Removal Assessment Report Kip Nelson Properties Site Kenosha, Kenosha County, Wisconsin.

Prepare for the U.S. Environmental Protection Agency, region 5, regarding removal assessment conducted by TN & Associates, Inc (TN&A), of properties by Kip Nelson, at Kenosha, Wisconsin.

000000204077

2003-05-30 00:00:00.0

WIN000508754

KIP NELSON/ABC SERVICES

PDF

PDF

TN & Associates, Inc (TN&A)

Administrative Record

Emergency response & Removal

text

Waste materials

Kip Nelson

Removal assessment

Properties

Environmental reporting

Midwest

TN & Associates, Inc (TN&A)

City of Kenosha

U.S. Environmental Protection Agency

2003-05-30

TN & Associates, Inc (TN&A)

City of Kenosha

U.S. Environmental Protection Agency

Copyright undetermined

eng

Kenosha, Wisconsin

PDF

EPA Region 5 Records Ctr.

204077

REMOVAL ASSESSMENT REPORT
KIP NELSON PROPERTIES SITE
KENOSHA, KENOSHA COUNTY, WISCONSIN

Prepared for:
U.S. ENVIRONMENTAL PROTECTION AGENCY
Region 5 Emergency Response Branch
77 West Jackson Boulevard
Chicago. IL 60604

TDD No.:
Date Prepared:
Contract No.:
Prepared by:
START Project Manager:
Telephone No.:
U.S. EPA Cm-Scene Coordinator:
Telephone No..

S05-0212-008
May 30. 2003
68-W-00-129
T N & Associates. Inc.

Raghu Nagam
(312)220-7000
Craig Thomas
(312)886-5907

T N & Associates, Inc.

Engineering and Science

CONTENTS

Section

Page

10

INTRODUCTION

1

20

SITE BACKGROUND

2

30

REMOVAL ASSESSMENT ACTIVITIES

6

31

SITE RECONNAISSANCE

6

311
3 12
3 I3
314

6
8
8
9

32

59 10 49™ STREET PROPERTY
6000 49™ STREET PROPERTY
5800 49™ STREET PROPERTY
5700 49™ STREET PROPERTY

9

SAMPLING ACTIVITIES

40

SAMPLE ANALYTICAL RESULTS

12

50

POTENTIAL SITE-RELATED THREATS

16

60

PROPOSED ACTIONS AND ESTIMATED COSTS

18

70

SUMMARY

19

Appendix

A
B
C

PHOTOGRAPHIC LOG
VALIDATED ANALYTICAL DATA PACKAGE
REMOVAL COST MANAGEMENT SYSTEM (RCMS) COST PROJECTION
FIGURES

Figure

1
2
3

Page

3
4
10

SITE LOCATION MAP
SITE FEATURES MAP
SAMPLING LOCATION MAP
TABLES

Table
1

Page
SAMPLE ANALYTICAL RESULTS

13

TDD S05-0212-008 (Kip Nelson Site)

1.0

INTRODUCTION

T N & Associates. Inc (TN&A). a subcontractor for the Tetra Tech EM Inc Superfund Technical
Assessment and Response Team (START), has prepared this remo\al assessment report in accordance
with the requirements of U S Em ironmental Protection Agenc\ (U S EPA) Technical Direction
Document (TDD) No S05-0212-008 The scope of this TDD \vas to conduct remo\ al assessment
activities at the Kip Nelson Properties (Kip Nelson) site in Kenosha. Kenosha Countv. Wisconsin
START was tasked to prepare a health and safety plan and a sampling plan, and to conduct a remo\ al
assessment, including air monitoring, drum and tank sampling, documentation of on-site conditions with
written logbook notes and a still camera (see Appendix A), analytical data \ alidation (see Appendix B).
and preparation of a removal assessment report

The removal assessment was performed in accordance with the National Oil and Hazardous Substances
Pollution Contingency Plan (NCP) as documented in Title 40 of the Code of Federal Regulations (CFR).
Section 300 415(b)(2), to evaluate site conditions and possible threats to human health, public \\elfare.
and the environment This report discusses the site background. remo\ al assessment activ ities. sample
analytical results, potential site-related threats, and proposed actions and estimated costs, and includes a
summary of the removal assessment Appendix A contains a photographic log of site activ Hies. Appendix
B contains the validated analytical data package for samples collected bv START, and Appendix C
contains Removal Cost Management Svstem (RCMS) cost projection

TDD S05-0212 008 (Kip Nelson Site)

2.0

SITE BACKGROUND

The Kip Nelson site comprises four salvage yard properties at 6000. 5910, 5800. and 5700 49th Street in
Kenosha, Kenosha County, Wisconsin (see Figure 1) The site properties at 6000. 5910. and 5800 49th
Street are contiguous, with no defining separation, and the property at 5700 49th Street is separated from
the rest of the site by a bulk fueling facility (see Figure 2) Kip Nelson ABC Sen ices conducted multiple
operations at the site, which included tank storage, recycling, and storage of waste drums, vehicles, tires.
waste petroleum products, tank sludge, and used ink

The responsible party (RP) is under a stipulation from the Wisconsin Department of Justice (WDOJ) to
remove wastes from the site The RP hired Environmental Innovations. Inc (El), to remove wastes from
the site El discusses the site activities in a letter dated October 30. 2002. addressed to Ms Shanna Laube
of the Wisconsin Department of Natural Resources (WDNR) In this letter. El indicates that all
nonfenced perimeter sections of the site would be fenced and that a limited excav ation of contaminated
soil at the 6000 and 5700 49th Street properties had been scheduled for October 31. 2002 The El letter
also indicates that all open drums and containers of liquids or wastes would be closed, covered, and
moved inside the building located at 6000 49th Street and that five large tanks were scheduled for cleanup
and disposal by November 6,2002

In a letter to WDOJ dated November 1. 2002. El indicates that a scrap dealer had removed approximately
75 percent of the scrap metal and vehicles from the 6000 49th Street property The letter also states that
on September 24. 2002, during the consolidation and staging of waste oils, two releases occurred Soil
and waste oil samples were collected, and results indicated that one spill area was hazardous while the
other w as nonhazardous El proposed an interim correctiv e action that inv oh ed soil excav ation.
sampling, and appropriate disposal The El letter also indicates that 5.516 gallons of waste oil was
removed from the 5910 49th Street property on October 4, 2002, 5,800 gallons of waste oil was removed
on October 25,2002. and 5,800 gallons of waste oil was removed on October 28, 2002 The El letter also
states that the waste oil from Tank 14 was disposed of as hazardous waste and that the water from this
tank was transferred to Tank 8, whose contents will be disposed of as hazardous waste The El letter
mentions 10 aboveground storage tanks (AST), including Tank 8, at the site that contain petroleum or
water and waste oil sludge The exact locations of these ASTs and the five large tanks that were to have
been removed bv November 6 are unknown

TDD S05-0212-008 (Kip Nelson Srte)

J

0L

,25Hi

»

KIP NELSON PROPERTY SITE
KENOSHA, WISCONSIN

S05-0212-008

NORTH
FIGURE 1
SITE LOCATION MAP

[ T N A Associates, Inc.
ource Modified from TerraSetver Kenosha Wisconsin 1976USGS
opographic Map

&A

Engineering and Science

f >TraTie7wthfl|6000 49lh St ^Plastic tanks |Metal

ml ding
5910 49th StreetTMlTanker truck

LEGJND

KIP NELSON PROPERTY SITE
KENOSHA, WISCONSIN

S05-0212-008
FIGURE 2
SITE FEATURES MAP

Site boundary

T N & Associates, Inc.

Engineering and Science
Source Modified from U S Geological Survey Aerial Phofogiaph of
Kenosha Wisconsin 2000 Terra Server

On December 18, 2002, El sent a letter to the City of Kenosha Fire Department indicating that all known
hazardous materials had been removed from the site and disposed of off site and that additional hazardous
materials not yet sampled for may be present on the site. Site materials removed by El were classified as
hazardous based on ignitability caused by solvents and, in a few cases, the presence of heavy metals (such
as lead and chrome).

WDNR requested U.S. EPA Region 5 Emergency Response Branch assistance on November 7, 2002. to
help evaluate and mitigate the threat posed by Kip Nelson ABC Services' operations at the site.
According to WDNR, removal activities are not proceeding in a timely manner because of the lack of
funds from the RP. WDNR's request letter indicates that on-site drums were leaking or overflowing;
tanks to be recycled were not intact, causing leaking of sludges and liquids; and soil staining from spills
was prevalent. Chlorinated compounds and high levels of metals have been identified in drum contents

and in site soil.

TDD S05-0212-008 (Kip Nelson Site)

3.0

REMOVAL ASSESSMENT ACTIVITIES

Removal assessment activities at the site included site reconnaissance and sampling activ ities Each
activity is discussed below

3.1

SITE RECONN \ISSA\CE

On February 26. 2002. U S EPA On-Scene Coordinators (OSC) Craig Thomas and Steven Farvan and
START conducted an on-site reconnaissance to document site conditions and determine potential
sampling locations at each of the four properties U S EPA and START were granted site access bv the
property owners to conduct this removal assessment The OSCs and START met with Mr Kip Nelson in
the metal building located at 5910 49th Street Mr Nelson informed the group that all drums contain oil
and that polychlonnated biphenyls (PCB) were never detected in samples collected from the drums
Mr Nelson, in reply to OSC inquiries, told the group that he would allow U S EPA investigators to
check his records to identify other potential RPs associated with the site At the end of this meeting, the
OSCs informed Mr Nelson that START would collect drum and tank samples and that he should not
allow disposal of any material without notifying U S EPA Reconnaissance observ ations at each
property are discussed below in the order of site reconnaissance inspection

3.1.1

591049 th STREET PROPERTY

The property at 5910 49* Street contains a concrete and a metal building Four 30-foot-long trailers were
located immediately northeast of the concrete building These trailers were filled with scrap, small
machinery. tools, and 55-gallon drums of unknown contents Some of these drums were emptv Another
trailer north of the concrete building contained 8 to 12 drums Two smaller trailers containing scrap
metal and small machinery were located northwest of the concrete building Prior to reconnaissance
activities, START calibrated the organic vapor air monitoring instrument, the total vapor analyzer (TVA1000), and the oxvgen, carbon monoxide, and combustible gas monitoring instrument (PhD Lite) The
TVA-1000 and PhD Lite instruments did not indicate anv readings above background levels

START did not conduct a reconnaissance of the concrete building because it was rented out and not
considered part of the Kip Nelson ABC Service operations

TDD S05-0212-008 (Kip Nelson Site)

The metal building is located west of the concrete building. Three fuel oil ASTs were located northwest
of the metal building. Two trailers approximately 60 feet long each were located north of the metal
building along the northern perimeter of the property. These trailers contained metal scrap. Several piles
of scrap and machinery were located next to these trailers. The real estate agent representing Mr. Kip
Nelson arrived on site and opened the service door to the metal building.

The metal building consisted of an office area in the southeast portion and a drum and warehouse area in
the remainder of the building. The metal building contained several rows of drums, typically five to six
in a row, along the entire length of the building. Over 150 drums, predominantly having a 55-gallon
capacity, were present in the building. A crew was operating a fork-lift to move drums. Inside the
building, the PhD Lite alarm started beeping, and carbon monoxide readings were as high as 40 parts per
million (ppm). At the OSCs suggestion, the other doors of the building were opened, the fork-lift engine
was shut off. and the air was vented out. The owner's consultant had moved all drums from the open
yard and staged them in the metal building and in the building located at 6000 49th Street property.

A small maintenance room in the southwestern corner of the metal building contained several small
5-gallon containers. Breathing zone air monitoring did not indicate any reading above background levels
in this room. Air monitoring using a TVA-1000 conducted by a red drum with an open bung indicated
over 200 ppm organic vapors. Air monitoring of another drum marked '"alcohol" indicated over
1,400 ppm organic vapors at the drum's bung opening.

After the building reconnaissance, U.S. EPA and START inspected the open yard north of the metal
building. A large trailer containing scrap metal and machinery and a huge rack containing machinery and
empty plastic drums were located along the northern perimeter of the northwestern portion of the
property. Immediately south of this trailer were four ASTs of unknown contents. Two small heating oil
tanks were located next to the western wall of the metal building, one at the northern end and one at the
southern end. A soil-stained area was observed next to the western wall of the metal building. Several
trucks and cars were also located in this area. Two 40-foot-long trailers containing drums and small
containers were located at the western perimeter of the property. Three ASTs and a pile of machine parts
and tires were located next to the trailers, and a tanker truck was located south of this pile. A truck
containing drums of unknown material was located southwest of the metal building and east of the gate
on 49* Street.

TDD S05-0212-008 (Kip Nelson Site)

6000 49 rh STREET PROPERTY

3.1.2

The property at this location contains one building located in the eastern portion of the propertv The
property entrance is through 49th Street by two gates, one of which is directlv south of the building A
dirt road encircles the building and connects the two gates The building contained about 30 rows of
drums, with each row typically containing three to six drums START estimated that over 150 to 200
drums were present in this building These drums occupied 75 percent of the building area The eastern
quarter of the building contained a split level area, with office space on the top level and several drums on
the bottom level The split-level roof appeared to have buckled and posed a potential health and safety
danger Breathing zone air monitoring readings were at background lev els in this building Air
monitoring for organic vapors of open drums indicated readings of 0 to 200 ppm

Two trailers located north of the building were filled with scrap metal and machinery In addition, several
empty drums were stacked north of the building Three plastic tanks were located northeast of the
building, and three ASTs were located northeast and west of the building An almost empty sludge tank
was located southeast of the building, and a visibly stained area was observed around this sludge tank
Two more ASTs were located at the southern property perimeter next to the west gate A trailer filled
with drums was located at the northwest corner of the property Two dumpsters containing soil and other
materials was located in the northwest portion of the property and was believed to have been left on site
by cleanup consultants conducting abatement actions at the property1 A tire pile containing scrap metal
was located in the southwest part of the property Metal and scrap piles were observed all over the
property'

3.1.3

5800 49'" STREET PROPERTY

The propertv at 5800 49th Street is an open vard containing two 40-foot-long trailers and one steel tanker
marked "ABC-T-6801 " The steel tank was estimated to be one-fourth to half full and to have a volume
of 2.000 to 3,000 gallons Of the two trailers, the north trailer contained over 100 5-gallon containers
marked "Anti Seize" and several chrome yellow containers marked ''flammable " The southern trailer
contained over 50 drums of 55-gallon capacity One drum was labeled "TMS Solvent-Fluorocarbon'' and
listed the manufacturer as E I Dupont in Wilmington. Delaware The trailer also contained 8 to 10
cartons of aerosol cans labeled "American Motors Touch-up "

TDD S05-0212-008 (Kip Nelson Site)

3.1.4

5700 49'" STREET PROPERTV

The property at 5700 49th Street contained several rail-car tankers in various stages of dismantlement
Some of the dismantled and cut open tanks contained oil or sludge Tanks labeled "26 East'" and ''27
East." had been cut open by the RP's cleanup contractor, and the tank contents had nearly overflowed,
posing potential spillage threats An- monitoring inside the tank indicated 5 to 10 ppm organic v apors

3.2

SAMPLING \CT\\ ITIES

START prepared a site sampling and analysis plan (SAP) that required the collection of drum and tank
samples from on-site locations and sample analysis for inorganic and organic compounds by a
commercial laboratory

START conducted drum sampling activities on February 26 and 27. 2003 Prior to the collection of drum
samples, START and the OSCs reviewed site reconnaissance information and identified potential drums
for sample collection On February 26, 2003, START donned "Level B" personal protective equipment
(PPE) and sampled drums in buildings located at the 6000 and 5910 49th Street properties (see Figure 3)
All drum samples were collected in laboratory-provided glass bottles using dedicated drum thieves

Drum samples D001 through D004 were collected from the building at 6000 49* Street Drum sample
DOO1 was collected from a blue 55-gallon plastic drum that had a reactive label on it The DOO1 sample
was liquid consisting of a clear brown top layer and a cloudy brown bottom layer Air monitoring of the
sample using the TV A-1000 indicated over 200 ppm organic vapors Drum sample D002 was collected
from a 55-gallon cream fiber drum with a liner labeled "Deoxidizer. Aluminum Cleaner" The D002
sample was a light-brown, single-phase, clear liquid Air monitoring of the sample using the TVA-1000
indicated over 10 ppm organic vapors Drum sample D003 was collected from a blue 55-gallon metal
drum labeled "propylene glycol" and "D004 " The D003 sample was a dark-brown, dense liquid Air
monitoring of the sample using the TVA-1000 indicated 10 to 100 ppm organic vapors Drum sample
D004 was collected from a 35-gaIlon green plastic drum marked "D002" and consisted of a dark-brown
liquid Air monitoring of the sample using the TV A-1000 indicated less than 5 ppm organic vapors

START then proceeded to the metal building at 5910 49th Street and collected drum samples D005
through D009 Drum sample D005 was collected from a 55-gallon black metal drum and consisted of a
dark-brown liquid Air monitoring of the sample using the TVA-1000 indicated over 200 ppm organic

n

TDD S05-0212-008 (Kip Nelson Site)

rs with scrap
achinery ,

Trailers with drums
27 East
tank
Northern trailer

T A

V'

\

T002

I
T003

1
T

26 East
tank

QD
DOS

006andD011
007
Drainage ditch

D008
D009

Tenant build p
(Concrete bui lding)

etal building

Southern trailer

D010

Office

Not part of site
operations
Tanker trailer

5910 49th Street

5700 49"1 Street

5800 49th Street

KIP NELSON PROPERTY SITE
KENOSHA, WISCONSIN

\ Stained soil
D001 Sample identification number

S05-0212-008
FIGURE 3
SAMPLING LOCATION MAP

i

erations

'

Drum storage areas

:TN T N & AaaoclateB, Inc.
Engineering and Science

10

vapors Drum sample D006 was collected from a 55-gallon black metal drum and consisted of a clear,
light-brown liquid Air monitoring of the sample using the TVA-1000 indicated ov er 400 ppm organic
vapors A duplicate sample of D006 was collected and labeled DO 11 Drum sample D007 was collected
from a 55-gallon black metal drum and consisted of a clear, light-brown liquid Air monitoring of the
sample using the TVA-1000 indicated over 1.400 ppm organic v apors Drum sample D008 w as collected
from a 55-gallon red metal drum and consisted of a two-phase, dark-brown liquid Air monitoring of the
sample using TVA-1000 indicated ov er 1.000 ppm organic \ apors Drum sample D009 w as collected
from a 55-gallon green plastic drum and consisted of a brown dense liquid Air monitoring of the sample
using the TVA-1000 indicated 200 to 300 ppm organic vapors

START sampling activities on February 27. 2003. included collection of samples from a tanker and a
drum from the 5800 49th Street property and from two rail-car tankers from the 5700 49th Street property
Specifically. START collected tanker samples TOO 1 through T003 and drum sample DO 10 The tanker
and rail-car samples were collected by dipping glass sample bottles directly into the liquid to be sampled
The drum sample was collected using a dedicated drum thief and laboratory-provided glass sample bottle
At 5800 49th Street, the tanker sample T001 consisted of a dense, oily black liquid Air monitoring of the
sample using the TVA-1000 indicated 25 to 50 ppm organic vapors START collected drum sample
DO 10 from the southern trailer at 5800 49th Street from a blue, 55-gallon metal drum marked "TMS
Solvent-Fluorocarbon " Drum sample DO 10 consisted of a clear brown liquid yielding a TVA-1000
reading of over 1,000 ppm organic vapors

At 5700 49* Street, sample T002 was collected from the rail-car tank marked "26 East " The sample
consisted of a dense, oily black liquid and was collected directly in the glass bottle by dipping the bottle
into the liquid through the opening on the side of the tank Air monitoring of the sample using the TVA1000 indicated 5 to 10 ppm organic vapors Sample T003 was collected from the rail-car tank marked
"27 East" at 5700 49th Street The sample consisted of a dense, oily black liquid Air monitoring using
the TVA-1000 indicated 5 to 10 ppm organic v apors

Key site features and sampling locations were photographed (see Appendix A) Drum and tank samples
were packaged and hand delivered to Great Lakes Analytical Services in Buffalo Grove, Illinois, on
February 27.2003 Sample analytical results are discussed in Section 4 0

TDD S05-0212-008 (Kip Nelson S'te)

4.0

SAMPLE ANALYTICAL RESULTS

START reviewed sample analytical data and supporting quality' assurance/quality control (QA/QC) data
provided by Great Lakes Analytical. The validated data package is included in Appendix B. Based on
START QA/QC data validation, the data are acceptable for use as qualified. Table 1 lists detected
analytes and their concentrations. Two drum samples (DOO 1 and D008) consisted of two-phase liquids,
requiring analysis of both layers. The analytical results of duplicate drum sample D011 were comparable
to results for original drum sample D006.

Analytical parameters were selected based on potential disposal requirements. All samples were tested
for pH and flashpoint except sample D011. which was not tested for pH. Samples T001 through T003
were also tested for percent chlorine composition. Samples D001 through D009 were analyzed for
reactive cyanide, reactive sulfide, PCBs, and toxicity characteristic leaching procedure (TCLP) volatile
organic compounds (VOC), TCLP semivolatile organic compounds (SVOC), and Resource Conservation
and Recovery Act (RCRA) metals. Sample DO 10 was analyzed for TCLP VOCs and SVOCs only.
Sample D011 was analyzed for TCLP VOCs, and sample T001 was analyzed for PCBs and TCLP VOCs
and SVOCs. Samples T002 and T003 were analyzed for TCLP metals and PCBs. Samples D001 and
D002 were also analyzed for TCLP pesticides and herbicides.

Benzene, trichloroethylene, tetrachloroethene, and methyl ethyl ketone were the most prevalent
contaminants detected. Potential site-related threats were evaluated in relation to the contaminants'
ignitability, corrosivity, and reactivity against criteria listed in 40 CFR, Parts 261.21,261.22, and 261.23,
respectively. Toxicity characteristics of site contaminants were evaluated against concentrations
summarized in 40 CFR. Part 261.24, Table 1. "Maximum Concentration of Contaminants for the Toxicity
Characteristic."

Analytical results of eight samples and one duplicate sample exceeded the TCLP concentrations of one or
more constituents listed in 40 CFR Part 261.24 Table 1, indicating hazardous waste characteristics.
Results for samples D001. D002, D007, D009, and T001 exceeded TCLP regulatory limits for benzene.
Analytical results for D009 and T001 exceeded TCLP regulatory limits for tetrachloroethene. Analytical
results for D002 and D006 exceeded TCLP regulatory limits for trichloroethylene. Analytical results for
D002, D006, and DO 11 exceeded TCLP regulatory limits for trichloroethylene. Analytical results for
D002 exceeded TCLP regulatory limits for heptachlor (and its epoxide). TCLP RCRA regulatory limits
were exceeded for the following metals: chromium in sample D003; selenium in samples D006 and

.~

TDD- S05-0212-008 (Kip Nelson Site)

TABLE 1
SAMPLE ANALYTICAL RESULTS
KIP NELSON PROPERTY SITE
KENOSHA, KENOSHA COUNTY, WISCONSIN
Sample Identification No.
Analytical Parameter

D001

D002

D003

D004

D005

D006

D007

D008

D009

DO 10

D011

T001

T002

T003

TCLP VOCs (mg/L)
9,770

238

ND

0.471

ND

ND

58.5

ND

187

ND

ND

1.05

NA

NA

Methyl ethyl kctone

ND

ND

ND

ND

ND

15.4J

ND

ND

ND

2.91 J

15.2 J

ND

NA

NA

Tetrachloroethene

ND

ND

ND

ND

ND

ND

ND

ND

66.2

ND

ND

7.10

NA

NA

Trichloroethylene

ND

142

ND

ND

ND

0.932

ND

ND

ND

ND

0.843

ND

NA

NA

ND

0.342

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

0.104

ND

0.258

ND

0.110

0.128

0.433

0.0710

ND

NA

NA

NA

ND

ND

Benzene

TCLP PESTICIDES! nig/kg)
Heptachlor
(and its epoxide)
TCLP METALS (mg/L)
Arsenic
Cadmium

ND

ND

0.4 15J

ND

ND

ND

ND

ND

ND

NA

NA

NA

ND

ND

Chromium

ND

ND

11.9

ND

ND

ND

ND

ND

ND

NA

NA

NA

ND

ND

0.000348

ND

ND

ND

0.000309

ND

ND

0.00123

000182

NA

NA

NA

ND

ND

0.185

0.0525

0.486

ND

ND

3.60

1.23

0.132

0.0625

NA

NA

NA

ND

ND

0.0850

0.0835

0.384

ND

0.0850

0.0900

ND

0.0835

0.0830

NA

NA

NA

ND

ND

1.92

0.0259

0.429

ND

0.0548

0.00821

0.0357

23.2

0.242

NA

NA

NA

0.184

0.227

Mercury
Selenium
Silver
Lead

13

TOP S05-0212-008 (Kip Nelson Site)

TABLE 1 (Continued)
SAMPLE ANALYTICAL RESULTS
KIP NELSON PROPERTY SITE
KENOSHA, KENOSHA COUNTY, WISCONSIN
Sample Identification No.
Analytical Parameter

D001

D002

D003

D004

D005

D006

D007

D008

D009

D010

D011

T001

T002

T003

PHYSICAL CHEMISTRY
596J

689J

1.89 J

637J

677J

761 J

696J

688J

703J

5 13J

NA

773J

590J

672J

Reactive Cyanide (mg/kg)

ND

0222

ND

ND

ND

ND

ND

ND

ND

NA

NA

NA

ND

ND

Reactive Sulfide (mg kg)

ND

ND

ND

ND

ND

ND

ND

10.0

ND

NA

NA

NA

ND

ND

Flashpoint (°F)

81.1

165

>220

149

>220

85. U

125

162

182

159

129 J

>220

>220

>220

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

0507

0504

0452

pH(SU)

Percent Chlorine (%)
Notes

Bolded results exceed the regulatory limits discussed in Section 4 0
J
mg/kg
mg/L
NA
ND
SU
TCLP
VOC

The analyte was detected The reported numerical values is considered estimated for quality control reasons
Milligram per kilogram
Milligram per liter
Not analyzed
Not detected at or above the reporting limit
Standard units
Toxicity characteristic leaching procedure
Volatile organic compound

14

TDD S05-0212-008 (Kip Nelson Site)

DOO7, and lead in sample D008 Drum sample D003 had a pH of 1 89 standard units (SU) and is
considered a corrosive liquid based on the criterion of less than 2 SU Drum sample D008 contained
10 (. mg/kg reactive sulfide and has a pH of 6 88 SU. therefore, it is considered a reactive liquid The
flashpoints of DOO 1, D006. D007. and D011 are below the minimum temperature of 140 °F and are
considered ignitable liquids

..

TDD S05-0208-010 (Kip Nelson Site)

5.0

POTENTIAL SITE-RELATED THREATS

Paragraph (b)(2) of 40 CFR Section 300.415 lists factors to be considered when dek.rmining the
appropriateness of a potential removal action at a site. Factors that are applicable to the site are discussed
below.

Actual or potential exposure to nearby human populations, animals, or the food chain from
hazardous substances or pollutants or contaminants. START sampling results indicate ignitable,
corrosive, reactive, and hazardous substances in drums inside the metal and 6000 49th Street buildings.
Personnel conducting various operations in the buildings could be exposed to these substances. One of
the buildings has an attached office space occupied by a tenant who could be exposed to hazardous
substances in case of a release. Drums containing hazardous substances are also located in several
unsecured trailers having unrestricted access.

The nature of hazardous substances and their potential exposure-related health effects are discussed
below. Inhalation of benzene, the most prevalent on-site contaminant detected, can cause drowsiness,
dizziness, and unconsciousness. Long-term benzene exposure affects bone marrow and can cause anemia
and leukemia. The Department of Health and Human Services (DHHS) has determined that benzene is a
known carcinogen. Long-term exposure to high levels of benzene in the air can cause leukemia and
cancer of blood-forming organs. Drinking or breathing high levels of trichloroethylene, which was also
detected on site, may cause nervous system effects, liver and lung damage, abnormal heartbeat, coma, and
possibly death. Breathing small amounts may cause headaches, lung irritation, dizziness, poor
coordination, and difficulty concentrating. Dermal contact with trichloroethylene for short periods may
cause skin rashes, headaches, lung irritation, dizziness, poor coordination, and difficulty concentrating.
Exposure to high levels of hexavalent chromium can damage the nose and cause cancer. Exposure to
very high concentrations of tetrachloroethylene can cause dizziness, headaches, sleepiness, confusion,
nausea, difficulty in speaking and walking, unconsciousness, and death. The DHHS has determined that
tetrachloroethylene may reasonably be anticipated to be a carcinogen. Tetrachloroethyiene has been
shown to cause liver tumors in mice and kidney tumors in male rats. Exposure to heptachlor and
heptachlor epoxide happens mostly from eating contaminated foods and milk, or skin contact with
contaminated soil. At high levels, they can cause damage to your nervous system. Heptachlor and
heptachlor epoxide are clearly toxic to humans and animals and can damage the nervous system. Lead,
which was detected in one sample at a concentration exceeding its screening criterion, can be inhaled in
workplace air or dust, ingested in contaminated foods, and imbibed through contaminated water. Lead
can damage the nervous system, kidneys, and reproductive system. Exposure to high levels can result in

16

TDD. S05-0208-010 (Kip Nelson Site)

neurological effects and brittle hair and deformed nails Occupational inhalation exposure may cause
dizziness, fatigue, irritation of mucous membranes, and respiratory effects

Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or other bulk storage
containers, that may pose a threat of release. Samples collected from some of the drums in the metal
and 6000 49th Street buildings and from the tanker and trailer located at 5800 49th Street contained
hazardous contaminants The drums, tanker, and trailer pose a threat of release because of the
deteriorating drum conditions and because the 5800 49th Street property is not secured

Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate
or be released. Trailers at the site contain hazardous substances in drums and other containers Hot or
severe weather conditions may damage the integrity of these trailers and the drums and containers inside
them, resulting in release of hazardous substances
Threat of fire or explosion. Drums in the metal and 6000 49th Street buildings contained liquids with
flash points below 140 °F, posing potential fire and explosion threats During the removal assessment, a
crew operated heavy machinery inside the building while the doors were closed Sparks from the engine
or from the tools room could result in a serious fire or explosion

Other situations or factors that may pose threats to public health or welfare of the United States or
the environment. The unsecured trailers, the tanker next to the road at 5800 49th Street, and several cutopen tanks at 5700 49* Street pose threats to public health or welfare from potential v andalism The
tanker at 5800 49th Street contains 2.000 to 3,000 gallons of hazardous liquid and can pose significant
threats to public health if v andals open the unsecured \ ah e on the tank Some of the cut-open tanks
contain liquids that could overflow as a result of small amounts of precipitation

The availability of other appropriate federal or state response mechanisms to respond to the
release. WDNR requested U S EPA Region 5 Emergency Response Branch assistance on November 7,
2002. to help evaluate and mitigate the threat posed bv Kip Nelson ABC Sen ices" operations at the Site
This request was made to U S EPA since WDNR did not have appropriate state response mechanisms to
respond to the release The request letter indicated that the drums on-site were leaking or ov erflowmg.
tanks to be recycled containing sludges or liquids were not intact causing leaking, and soil staining from
spills was prevalent

17

TDD S05-0208-010 (Kip Nelson Site)

60

PROPOSED ACTIONS AND ESTIMATED COSTS

Based on Section 5 0. U S EPA could undertake a removal action to abate potential site-related threats
from the presence of hazardous, flammable, and acidic substances present at the site The recommended
removal action would involve removing all hazardous and nonha/ardous liquids and transporting them to
a licensed disposal facihtv for treatment and/or fluid blending, as necessary Hazardous and nonhazardous
solids from drums and tanks would also be removed under this recommended removal action and
transported to a licensed disposal facility for appropriate treatment and disposal Lead-contaminated soil
may potentially be present on-site due to scrap operations, and would require proper characterization and
disposal

The cost for the recommended remov al action was projected using U S EPA's Remov al Cost
Management System (RCMS) software (see Appendix C) Transportation and disposal costs were quoted
by SET Environmental, Inc , located in Wheeling, Illinois The time frame for the completion of the
removal action is projected at 12 weeks, with 10-hour work days, 6 days a week The total cleanup
contractor cost for the removal action, including contingency and indirect costs is $ 800,661 76

jg

T

DD S05-0208-010 (Kip Nelson Site)

7.0

SUMMARY

On February 26 and 27. 2003. U.S. EPA OSCs Craig Thomas and Steven Faryan and START conducted
removal assessment activities at the Kip Nelson Property site in Kenosha, Wisconsin. Removal
assessment activities included a site reconnaissance and collection of 11 drum samples (including one
duplicate) and three tank samples. Samples were analyzed for TCLP VOCs, SVOCs, pesticides, and
RCRA metals and for flashpoint. pH. reactive sulfide. and percent chlorine. Sample analytical results
were compared to 40 CFR, Parts 261.21, 261.22, 261.23, and maximum allowable concentrations
pursuant to 40 CFR Part 261.24. Table 1. TCLP concentrations measured in a sample from one tank at
the 5800 49th Street property and several drum samples from the properties at 6000 and 5910 49th Street
exceeded the maximum allowable concentrations in 40 CFR, Part 261.24. Table 1. Analytical results of
drum samples from the properties at 6000 and 5910 49th Street also indicated ignitable, corrosive, and
reactive substances. Based on START removal assessment analytical results, the site meets the
requirements for a potential removal action to abate, prevent, minimize, stabilize, mitigate, or eliminate
the release or threat of release.

19

TDD S05-0208-010 (Kip Nelson Site)

APPENDIX A
PHOTOGRAPHIC LOG
(26 Pages)

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

1
Orientation: Not applicable
Wednesday, February 26, 2003
S05-0212-008
Date:
Site Name:
Kip Nelson Property
Raghu Nagam, START
Kenosha. Kenosha County, Wisconsin
Drum containing grease-like material in trailer north of concrete building at 5910 49* Street
property

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

Orientation: Southeast
Wednesday, February 26, 2003
Date:
S05-0212-008
Kip Nelson Property
Site Name:
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin
Several 5-gallon buckets located in trailer north of concrete building at 5910
49th Street property

A-l

Photograph No.:
TDD Number
Photographer
Location:
Subject:

Photograph No.:
TDD Number
Photographer.
Location:
Subject:

Orientation:
S05-0212-008
Date:
Raghu Nagam, START
Site Name:
Kenosha, Kenosha County, Wisconsin
55-gallon drum of unknown material in one of the four
building at 5910 49* Street property

East
Wednesday, February 26, 2003
Kip Nelson Property
trailers located north of concrete

Orientation: East
Date:
Wednesday, February 26, 2003
Site Name: Kip Nelson Property

S05-0212-008

Raghu Nagam. START

Kenosha, Kenosha County, Wisconsin
Flammable liquid in 55-gallon drums in one of the trailers north of concrete building at 5910
49* Street property

A-2

Photograph No.:
TDD Number
Photographer:
Location:
Subject:

5
Orientation: East
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha. Kenosha County, Wisconsin
View of scrap and machinery and 55-gallon drums in one of the trailers north of the concrete
building at 5910 49th Street property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

6
S05-0212-008
Raghu Nagam, START

Orientation: East
Date:
Wednesday, February 26,2003
Site Name: Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Gasoline cans in one of the trailers north of concrete building at 5910 49th Street property

A-3

Photograph No.'
TDD Number
Photographer
Location:
Subject:

Orientation: South
S05-0212-008
Wednesday, February 26, 2003
Date:
Raghu Nagam, START
Kip Nelson Property
Site Name:
Kenosha, Kenosha County, Wisconsin
Several aboveground storage tanks (AST) used for heating oil storage tanks, more ASTs
located just north of the metal building at 5910 49* Street property

Photograph No.
TDD Number:
Photographer
Location:
Subject:

8

Orientation: South
Date:
Wednesday, February 26, 2003
Site Name:
Kip Nelson Property

S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin
55-gallon drums staged in the metal building at 5910 49* Street property

A-4

Photograph No.
TDD Number
Photographer:
Location:
Subject:

Orientation: Northeast
S05-0212-008
Date:
Wednesday. February 26. 2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
55-gallon drums and small containers under the spht-level roof m the metal building at 5910
49* Street property

Photograph No.
TDD Number
Photographer
Location:
Subject:

10
S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin
Maintenance room in the metal building
Street property

A-5

Orientation: North
Wednesday, February 26. 2003
Date:
Site Name: Kip Nelson Property
stored with gasoline and paint cans at 5910 49th

Photograph No.:
TDD Number
Photographer:
Location:
Subject:

11
Orientation: South
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam. START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
55-gallon drums staged inside the building located at 6000 49* Street property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

12
S05-0212-008
Raghu Nagam, START

Orientation: Northeast
Date:
Wednesday, February 26,2003
Site Name:
Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Drum and evidence of past spills located in the building at 6000 49* Street property

A-6

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

13
Orientation: Not applicable
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Blue 55-gallon drum with "corrosive" sticker located in the building at 6000 49* Street
property

Photograph No.:
TDD Number
Photographer
Location:

14
S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin

Subject:

Orientation: Not applicable
Wednesday, February 26, 2003
Date:
Kip Nelson Property
Site Name:

3 5-gallon blue plastic drum with flammable/reactrve sticker on it located in the building at
6000 49* Street property

A-7

Photograph No.:
TDD Number
Photographer:
Location:
Subject:

15
Orientation: South
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site Name: Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Rusted drums located in the building at 6000 49* Street property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

16
Orientation: NA
Wednesday, February 26, 2003
S05-0212-008
Date:
Raghu Nagam, START
Site Name: Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Propylene glycol drum located in the building at 6000 49* Street property

A-8

Photograph No.:
TDD Number
Photographer
Location:
Subject:

17
Orientation: Southeast
S05-0212-008
Date:
Wednesday, February 26. 2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Drums staged above the split-level roof in the building at 6000 49* Street property.
Roof appeared structurally unsafe

Photograph No.:
TDD Number
Photographer
Location:
Subject:

18
Orientation: South
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site Name: Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Drums staged on the concrete floor and small containers on the racks next to the west
wall of building at 6000 49* Street property

A-9

Photograph No..
TDD Number:
Photographer:
Location:
Subject:

19
Orientation: Northwest
S05-0212-008
Date:
Wednesday, February 26. 2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Tires, scrap, dumpsters, and a trailer with drums located at 6000 49* Street property

Photograph No.'
TDD Number
Photographer
Location:
Subject:

20
Orientation: South
Wednesday, February 26, 2003
S05-0212-008
Date:
Kip Nelson Property
Raghu Nagam, START
Site Name:
Kenosha, Kenosha County, Wisconsin
Tires and stained soil at 6000 49* Street property

A-10

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

21
Orientation: South
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site Name: Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
55-gallon drums stored in the trailer located in the northwest corner of 6000 49* Street
property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

22
S05-0212-008

Orientation: South
Wednesday, February 26, 2003
Date:

Raghu Nagam, START

Site Name:

Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
drums stored in the trailer located in the northwest corner of 6000 49* Street property

A-ll

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

23
Orientation: Southwest
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site Name:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Fuel tank on 6000 49* Street property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

24
S05-0212-008
Raghu Nagam, START

Orientation: Southeast
Date:
Wednesday, February 26,2003
Site Name: Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Dumpsters and other scrap metal located next to the building on 6000 49* Street
property

A-12

Photograph No.:
TDD Number
Photographer:
Location:
Subject:

25
S05-0212-008
Raghu Nagam. START

Photograph No.:
TDD Number
Photographer
Location:
Subject:

26
S05-0212-008

Orientation: East
Date:
Wednesday, February 26, 2003
Site Name:
Kip Nelson Property

Kenosha. Kenosha County, Wisconsin
Drums in a trailer next to the fence on 5910 49* Street property

Orientation: Northwest
Wednesday, February 26, 2003
Date:

Raghu Nagam, START
Site Name: Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Sludge tank with visibly stained soil around it located east of the building at 6000 49*
Street property

A-13

Photograph No..
TDD Number:
Photographer
Location:
Subject:

27
S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin
Drums and 5-gallon containers located
property

Orientation: West
Date:
Wednesday, February 26.2003
Site:
Kip Nelson Property

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

28
Orientation: West
Wednesday, February 26, 2003
S05-0212-008
Date:
Kip Nelson Property
Raghu Nagam, START
Site:
Kenosha, Kenosha County, Wisconsin
AST, trailers, and empty drums in the northern Portion of 6000 and 5910 49* Street property

in the trailer east of the building at 6000 49* Street

A-14

Photograph No.:
TDD Number
Photographer
Location:
Subject:

29
Orientation: South
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
55-gallon drums and cartons of aerosol cans in the southern trailer on 5800 49* Street
property; one drum marked as "solvent"

Photograph No.:
TDD Number
Photographer
Location:
Subject:

30
Orientation: South
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
5-gallon containers marked "Anti-Seize" in the northern trailer at 5800 49* Street property

A-15

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

31
Orientation: South
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Scrap machinery and 5-gallon containers marked "Anti-Seize" in the northern trailer at 5800
49* Street property

Photograph No.:
TDD Number
Photographer
Location:
Subject:

32
Orientation: North
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Tanker marked "ABC-T-6601" at 5800 49* Street property; the tanker contained 2,000 to
3,000 gallons of waste oil with hazardous constituents

A-16

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

33
S05-0212-008

Orientation: East
Wednesday, February 26, 2003
Date:

Raghu Nagam, START

Site:

Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Rail car tankers cut open for oil removal located at 5700 49* Street property

Orientation: South
Wednesday,
Date:

34
S05-0212-008

Raghu Nagam, START
Site:
Kenosha, Kenosha County, Wisconsin
Rail car tanker located at 5700 49* Street property

A-17

February 26, 2003
Kip Nelson Property

rf*':?•••*-.rf*-.P*CI

Photograph No.:
TDD Number:
Photographer:
Location:
Subject:

. - *«'

35
S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin
Rail car tankers and machinery located

<?•*

Photograph No..
TDD Number
Photographer
Location:
Subject:

Orientation: North
Date:
Wednesday, February 26.2003
Site:
Kip Nelson Property
at 5700 49* Street property

"-•'"

36
S05-0212-008
Raghu Nagam, START

" <"* ,wl' •

Orientation: Northwest
Date:
Wednesday, February 26,2003
Site:
Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Northern and southern trailers located at 5800 49* Street property

A-18

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

37
Orientation: Southwest
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha. Kenosha County, Wisconsin
Two-phase liquid sample (D001) being collected from drum in the building at 6000 49* Street
property; analytical results indicate ignitable material

Photograph No.:
TDD Number
Photographer
Location:
Subject:

38
S05-0212-008
Raghu Nagam, START
Kenosha, Kenosha County, Wisconsin

Orientation: Not applicable
Date:
Wednesday, February 26.2003
Site:
Kip Nelson Property

Sample D002 collected from the building at 6000 49* Street property; analytical results
indicate hazardous volatile organic compound (VOC) constituents

A-19

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

39
Orientation:
North
S05-0212-008
Date:
Wednesday, February 26,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha. Kenosha County, Wisconsin
Sample D003 being collected from drum labeled "propylene glycol" at 6000 49* Street
property. Analytical results indicate chromium contamination

Photograph No.
TDD Number:
Photographer:
Location:
Subject:

40
Orientation:
Northwest
Wednesday, February 26, 2003
S05-0212-008
Date:
Kip Nelson Property
Raghu Nagam. START
Site:
Kenosha, Kenosha County, Wisconsin
Sample D004 being collected from drum at 6000 49* Street property

A-20

Photograph No..
TDD Number:
Photographer:
Location:
Subject:

41
Orientation:
Northwest
S05-0212-008
Date:
Wednesday. February 26,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Sample D005 being collected from 55-gallon drum located at 5910 49* Street property

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

42
Orientation:
North
S05-0212-008
Date:
Wednesday, February 26.2003
Raghu Nagam. START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Drum sample D006 being collected from drum at 5910 49* Street property; analytical results
indicate flammable material containing VOCs and metal contamination

A-21

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

43
Orientation:
Northwest
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Drum sample D007 being collected from drum at 5910 49* Street property; analytical results

indicate ignitable material contaminated with VOCs and metals

Photograph No.:
TDD Number
Photographer
Location:
Subject:

44
S05-0212-008

Orientation:
Date:

Northwest
Wednesday, February 26.2003

Raghu Nagam, START

Site:

Kip Nelson Property

Kenosha, Kenosha County, Wisconsin

Two-phase liquid sample D008 being collected from drum at 5910 49* Street property;
analytical results indicated VOC and metals contamination

A-22

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

45
Orientation:
Northwest
S05-0212-008
Date:
Wednesday, February 26, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha. Kenosha County, Wisconsin
Drum sample D009 being collected from green drum at 5910 49* Street property, analytical
results indicate VOC and metals contamination

Photograph No.:
TDD Number:
Photographer.
Location:
Subject:

46
S05-0212-008

Orientation:
Date:

South
Thursday, February 27, 2003

Raghu Nagam, START

Site:

Kip Nelson Property

Kenosha, Kenosha County, Wisconsin
Drum labeled "TMS Solvent-Fluorocarbon" located in southern trailer at 5800 49* Street
property

A-23

Photograph No.
TDD Number:
Photographer:
Location:
Subject:

47
Orientation:
South
S05-0212-008
Date:
Thursday, February 27, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
55-gallon drums and aerosol cans in the southern trailer at 5800 49* Street property

Photograph No.
TDD Number:
Photographer
Location:
Subject:

48
Orientation:
East
S05-0212-008
Date:
Thursday, February 27, 2003
Kip Nelson Property
Raghu Nagam. START
Site:
Kenosha, Kenosha County, Wisconsin
Aerosol cans labeled "Amencan Motors Touch-up" m the southern trailer located at 5800 49*
Street property

A-24

Photograph No.
TDD Number:
Photographer
Location:
Subject:

49
Orientation:
South
S05-0212-008
Date:
Thursday, February 27, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
5-gallon buckets labeled "chrome yellow" in the northern trailer at 6000 49* Street property

Photograph No.
TDD Number
Photographer
Location:
Subject:

50
Orientation:
Southeast
S05-0212-008
Date:
Thursday, February 27,2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
5-gallon buckets labeled "chrome yellow" with flammable sticker on it at 5800 49* Street
property

A-25

Photograph No.:
TDD Number
Photographer
Location:
Subject:

51
Orientation:
South
S05-0212-008
Date:
Thursday, February 27, 2003
Raghu Nagam, START
Site:
Kip Nelson Property
Kenosha, Kenosha County, Wisconsin
Sample DO 10 being collected from drum labeled "TMS Solvent-Fluorocarbon" in the
southern trailer at 5800 49* Street property; aerosol cans also visible

Photograph No.:
TDD Number:
Photographer
Location:
Subject:

South
52
Orientation:
Thursday, February 27, 2003
S05-0212-008
Date:
Kip Nelson Property
Raghu Nagam, START
Site:
Kenosha, Kenosha County, Wisconsin
Drums in the southern trailer at 5800 49* Street property

A-26

APPENDIX B
V A L I D A T E D A N A L Y T I C A L DATA PACKAGE
i 3 5 SheetM

TetraTech EM Inc.
26600 Telegraph Road, Suite 400 » Southfield, Ml 48034 » (248) 350-9694 » Fax (248) 223-99 1 1

MEMORANDUM

Date:

April 16, 2003

To:

Raghu Nagam, Project Manager, TN and Associates (TN)
•
Superfund Technical Assessment and Response Team (START) for Region 5

From:

Anne Troup, Chemist, (Tetra Tech EM Inc.) START for Region 5

Subject:

Data Validation for
Kip Nelson Properties Site
Kenosha, Wisconsin
Analytical Technical Direction Document (TDD) No, S05-0301-004
Project TDD No. S05-0212-008
Laboratory: Great Lakes Analytical Laboratories (GLA), Buffalo Grove, Illinois
Work Order No. B302323
Toxicity Characteristic Leaching Procedure (TCLP) Volatile Organic Compound (VOC),
TCLP Semivolatile Organic Compound (SVOC), TCLP Pesticides (Pesticides),
Polychlorinated Biphenyl (PCB), TCLP Herbicides (Herbicides), TCLP Metals, pH,
Reactive Cyanide, Reactive Sulfide, Flash Point, Percent Chlorine, and British Thermal Unit
(BTU) Analyses of Six Water, Six Liquid Waste, and Two Solid Waste Samples
1.0

INTRODUCTION

The Tetra Tech START for Region 5 validated TCLP VOC, TCLP SVOC, TCLP pesticides, PCB,
TCLP herbicides, TCLP metals, reactive cyanide, reactive sulfide, pH, flash point, percent chlorine and
BTU analytical data for six water, six liquid waste, and two solid waste samples. The samples were
collected during removal site evaluation activities conducted on February 26 and 27, 2003, at the Kip
Nelson Properties site in Kenosha, Wisconsin. Not every sample was analyzed for all the parameters.
The samples were analyzed under the above-referenced work order by GLA using U.S. Environmental
Protection Agency (U.S. EPA) SW-846 Methods 1311/8260B for TCLP VOC analysis; 1311/8270C for
TCLP SVOC analysis; 1311/8081A for TCLP pesticide analysis; 8082 for PCB analysis: 1311/8151A for
TCLP herbicide analysis; 1311/6010B for TCLP arsenic, barium, cadmium, chromium, selenium, and
silver analyses; 1311/7421A for TCLP lead analysis; 1311/7470A for TCLP mercury analysis; 9040B for

£j

contains recycled fiber and is recyclable

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
Page 2
pH analysis; 7.3.3 for reactive cyanide analysis; and 7.3.4 for reactive sulfide analysis. In addition, GLA
used American Society for Testing and Materials (ASTM) Method D93-85 for flash point analysis and
ASTM D808-90 for percent chlorine analysis. The BTU analysis was performed using ASTM Method
D240-92 by Sommer-Frey Laboratories, Inc., under subcontract to GLA.

The data were validated in general accordance with U.S. EPA's "Contract Laboratory Program National
Functional Guidelines for Organic Data Review" dated October 1999 and "Contract Laboratory Program
National Functional Guidelines for Inorganic Data Review" dated July 2002. Organic data validation
consisted of a review of the following quality control (QC) parameters: holding times, instrument
performance checks, initial and continuing calibrations, blank results, surrogate recovery results, matrix
spike and matrix spike duplicate (MS/MSD) results, laboratory control sample (LCS) results, internal
standard (IS) area counts, and target compound identification and quantitation. Inorganic data validation
consisted of a review of the following QC parameters: holding times, initial and continuing calibrations,
blank results, inductively coupled plasma (ICP) interference check sample results, LCS results, duplicate
sample results, MS/MSD results, and sample analytical result quantitation.

Section 2.0 discusses the results of the organic data validation, Section 3.0 discusses the results of the
inorganic data validation, and Section 4.0 presents an overall assessment of the data. The attachment to
this memorandum contains GLA's summary of analytical results as well as START'S handwritten data
qualifications where warranted.

2.0

ORGANIC DATA VALIDATION RESULTS

The results of START'S organic data validation are summarized below in terms of the QC parameters
reviewed. The data qualifier below was applied to the sample analytical results where warranted (see the
attachment).

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
Page 3
J - The analyte was detected. The reported numerical value is considered estimated for QC
reasons.

2.1

HOLDING TIMES

The samples were analyzed within the holding time limits of (1) 14 days to TCLP extraction and 14 days
from TCLP extraction to analysis for TCLP VOCs and (2) 14 days to TCLP extraction, 7 days from
TCLP extraction to preparative extraction, and 40 days from preparative extraction to analysis for TCLP
SVOCs, TCLP pesticides, and TCLP herbicides. Samples D003, D005, and D006 were extracted
beyond the method specified holding time of 14 days to preparative extraction but were analyzed within
the method specified holding time of 40 days from preparative extraction to analysis for PCBs. No
qualifications are warranted for the holding time exceedances because the target compounds are very
stable.

2.2

INSTRUMENT PERFORMANCE CHECKS

The bromofluorobenzene and decafluorotriphenylphosphine instrument performance checks met the QC
abundance criteria for the VOC and SVOC analyses, respectively. The chromatographic resolution was
adequate for the TCLP pesticide, PCB, and TCLP herbicide analyses.

2J

INITIAL AND CONTINUING CALIBRATIONS

All the initial calibration results were within QC limits, exhibiting high correlation coefficients or
acceptable relative standard deviations as required by the various methods. The percent difference (%D)
values for the continuing calibration results were acceptable for all detected target compounds.

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
Page 4
2.4

BLANK RESULTS

During the organic analyses, method blanks were run with each analytical batch in the proper sequence.
Method blanks were free of target compound contamination for the TCLP VOC, TCLP SVOC, TCLP
pesticide, PCB, and TCLP herbicide analyses.

2.5

SURROGATE RECOVERY RESULTS

All surrogate recoveries were within the laboratory-established QC limits with the following exceptions,
which were caused by interference from various nontarget compounds. Recoveries for the VOC
surrogate 4-bromofluorobenzene were slightly high and outside the laboratory-established QC limits for
sample D003. No qualification is warranted. In the SVOC analysis, recoveries for phenol-d6,
nitrobenzene-d5,2-fluorophenol, and 2-fluorobiphenol exceeded the QC limits in samples D001, D002,
D007, D008, and D009. The sample analytical results were all nondetects, so no qualifications are
warranted. In the pesticide analysis the recovery for tetrachloro-meta-xylene in sample D002 exceeded
the QC limits. No qualification is warranted. The recovery for 2,4-DCAA in sample D001 exceeded the
QC limits for the herbicide analysis. No qualification is warranted. In the PCB analysis, the surrogate
recoveries were within the QC limits specified by the laboratory.

2.6

MS/MSD RESULTS

MS/MSD samples were analyzed during the organic analyses. All recoveries were within laboratoryestablished QC limits with the following exception. In the VOC analysis, MS and MSD recoveries for
methyl ethyl ketone exceeded the QC limits. Positive sample results are qualified "J" for this compound
as estimated for QC reasons.

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
PageS
2.7

LCS RESULTS

An LCS was analyzed with the samples in each analytical batch. The LCS results were within QC limits
with the following exception. In the herbicide analysis, the recovery for the surrogate tetrachloro-metaxylene exceeded the QC limits. No qualification is warranted.

2.8

IS AREA COUNTS

The IS area counts were within the QC limits of -50 to +100 percent of those for the calibration standard.
The retention times for the ISs were within the QC limit of ± 30 seconds. IS area counts do not apply to
the TCLP pesticide, PCB, and TCLP herbicide analyses.

2.9

TARGET COMPOUND IDENTIFICATION AND QUANTITATION

A spot-check of the chromatograms for the TCLP VOC, TCLP SVOC, and TCLP pesticide analyses
confirmed the target compound identifications for the samples. No target compounds were detected in
the TCLP herbicide and PCB analyses.

3.0

INORGANIC DATA VALIDATION RESULTS

The results of START'S inorganic data validation are summarized below in terms of the QC parameters
reviewed. The data qualifier below was applied to the sample analytical results where warranted (see the
attachment).
•

J - The analyte was detected. The reported numerical value is considered estimated for QC
reasons.

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
Page 6
3.1

HOLDING TIMES

Samples were analyzed for TCLP metals within the holding time limits of 28 days for mercury and 6
months for metals other than mercury. Samples were analyzed within the holding time limits of 28 days
for percent chlorine and 14 days for reactive cyanide and reactive sulfide. The flash point and BTU
analytical methods do not stipulate a holding time. The methodology for pH analysis states that the
analysis should be performed "as soon as possible"; however, the laboratory did not perform this analysis
until March 6,2003, which was 8 days after laboratory receipt of the samples. Therefore, all pH results
are qualified "J" as estimated for QC reasons.

3.2

INITIAL AND CONTINUING CALIBRATIONS

All initial calibration results were within QC limits, exhibiting high correlation coefficients or appropriate
recoveries as required by the various methods. All continuing calibration results were also within QC
limits with the following exception. During the closing continuing calibration, silver exhibited an 89
percent recovery, which is just below the QC limit of 90 percent. No qualification is warranted for this
minor irregularity.

3J

BLANK RESULTS

Appropriate blanks such as initial calibration, continuing calibration, and preparation blanks were run with
each analytical batch. All blank results were within the QC limits specified by the laboratory.

3.4

ICP INTERFERENCE CHECK SAMPLE RESULTS

ICP interference check sample analyses were performed as required. All results were within QC limits.

Data Validation for
Kip Nelson Properties Site
Analytical TDD No. S05-0301-004
Project TDD No. S05-0212-008
Page 7
3.5

LCS RESULTS

An LCS was analyzed with each analytical batch. All the LCS results were within the QC limits
specified by the laboratory.

3.6

DUPLICATE SAMPLE RESULTS

A duplicate sample was not analyzed with the samples. However, sample D011 is a field duplicate of
sample D006. Metal analysis was not performed on sample D011. There was a 50 percent difference
between the flash point results for samples D006 and D011. Therefore, the flash point results for samples
D006 and D011 are qualified "J" as estimated for QC reasons.

3.7

MS/MSD RESULTS

MS/MSD samples were analyzed as required. All recoveries were within QC limits with the following
exception. The relative percent difference exceeded the QC limit for cadmium in the MS and MSD.
Therefore, all positive results are qualified "J" as estimated for QC reasons.

3.7

SAMPLE ANALYTICAL RESULT QUANTITATION

Analytical results were randomly spot-checked against raw data and extraction logs for the analyses.
The results checked were calculated correctly.

4.0

OVERALL ASSESSMENT OF DATA

Overall, the sample analytical data generated by GLA are acceptable for use as qualified.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI -1L
200 E. Randolph Suite 4700
Chicago EL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Reported:
03/18/03 13:52

ANALYTICAL REPORT FOR SAMPLES
Date Sampled

Date Received

Waste (L)

02/26/03 15:30

02/27/03 14:05

B302323-02

Waste (L)

02/26/03 15:35

02/27/03 14:05

D003, Bldg. 6000

B302323-03

Water

02/26/03 15:40

02/27/03 14:05

D004, Bldg. 6000

B302323-04

Waste (L)

02/2*6/03 16:10

02/27/03 14:05

D005, Bldg. 5910

B302323-05

Water

02/26/03 17:05

02/27/03 14:05

D006, Bldg. 5910

B302323-06

Water

02/26/03 17:10

02/27/03 14:05

37, Bldg. 5910

B302323-07

Water

02/26/03 17:15

02/27/03 14:05

t3fx)8, Bldg. 5910

B302323-08

Waste (L)

02/26/03 17:25

02/27/03 14:05

D009, Bldg. 5910

B302323-09

Waste (L)

02/26/03 17:30

02/27/03 14:05

T001, Tanker@5800

B3023 23-10

Waste (L)

02/27/03 09:20

02/27/03 14:05

T002, 26 East

B302323-11

Waste (S)

02/27/03 09:30

02/27/03 14:05

T003, 27 East

B302323-12

Waste (S)

02/27/03 09:35

02/27/03 14:05

D010, 5800 S. Trailer

B302323-13

Water

02/27/03 10:45

02/27/03 14:05

D011,DUPofD006

B3023 23-14

Water

02/26/03 17:10

02/27/03 14:05

Sample ID

Laboratory ID

Matrix

D001, Bldg. 6000

B302323-01

D002, Bldg. 6000

Great Lakes Analytical-Buffalo Grove

s\*^tf**

The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-02 1 2-008
Project Manager LisaGraczyk

Reported:

03/18/03 13:52

General Chemistry
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Method

Notes

Prepared

Analyzed

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
EPA9040B TV-^*3 4f
EPA 73.3
EPA 7.3.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
^>
EPA9040B T W -?•****
EPA 73.3
EPA 73.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
EPA9040B J V~**-^ '
EPA 7.3.3
EPA 7.3.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
EPA 9040B J
EPA 733
EPA 7.3.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
***
EPA9040B 3 V-^-* 3
EPA 73.3
EPA 7.3.4

DOOl, Bldg. 6000 (B302323-01) Waste (L) Sampled: 02/26/03 15:30 Received: 02/27/03 14:05
Flashpoint

PH

81.1
5.96

Reactive Cyanide
Reactive Sulfide

ND
ND

op

1

pH Units
0.0100
mg/1

6.50

it

3030076
3030065
3030080
3030078

D002, Bldg. 6000.(B302323-02) Waste (L) Sampled: 02/26/03 15:35 Received: 02/27/03 14:05

165
6.89

Flashpoint

PH
Reactive Cyanide
Reactive Sulfide

0.222

ND

op

1

pH Units
0.0100
mg/1
m

6.50

3030076
3030065
3030080
3030078

D003, Bldg. 6000 (B302323-03) Water Sampled: 02/26/03 15:40 Received: 02/27/03 14:05
Flashpoint

>220°F
1.89

pH

ND
ND

Reactive Cyanide
Reactive Sulfide

°F

1

pH Units
0.0100
mg/1

6.50

H

3030076
3030065
3030080
3030078

D004, Bldg. 6000 (B302323-04) Waste (L) Sampled: 02/26/03 16:10 Received: 02/27/03 14:05

149
637
ND
ND

Flashpoint

pH
Reactive Cyanide
Reactive Sulfide
D005, Bldg. 5910 (B302323-05) Water

1

6.50

11

3030076
3030065
3030080
3030078

H-fy>6 5 *

Sampled: 02/26/03 17:05 Received: 02/27/03 14:05

Flashpoint

>220 °F
6.77

PH

ND
ND

Reactive Cyanide
Reactive Sulfide

Great Lakes Analytical-Buffalo Grove
/ I "^^S*.

°F
pH Units
0.0100
mg/1

»J cH^"*-.-. T>. VVJ -*__

OF
pH Units
0.0100
mg/1

6.50

i*

1

3030076
3030065
3030080
3030078

The results m this report appfy to the samples analyzed in accordance -with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380Busch Parkway
Buffalo Grove, Illinois 60089
";
j

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-02 1 2-008
Project Manager LisaGraczyk

Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago PL, 60601

Reported:
03/18/03 13:52

General Chemistry
Great Lakes Analytical—Buffalo Grove
Result

Analyte
D006, Bldg. 5910 (B302323-06) Water

85.1 •
7.61
ND
ND

Dilution

Batch

Prepared

Analyzed

Method

—

Notes

°F
pH Units
0.0100
mg/1
6.50 " "

1
'
"
'

03/05/03
03%5/03
03/07/03
03/06/03

ASTMD93-85 T-y-9-*^ -^"
EPA9040B tTV-9— -3 ty
EPA 73.3
EPA 73.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTMD93-85
EPA9040B 3- V-?-03/#'
EPA 733
EPA 73.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03
03/06/03

ASTM D93-85
EPA9040B T-*J*g-e$ #f
EPA 73.3
EPA 73.4

03/05/03
03/05/03
03/05/03
03/05/03

03/05/03
03/05/03
03/07/03'
03/06/03

ASTM D93-85
EPA9040B T
EPA 733
EPA 7.3.4

03/06/03
03/05/03
03/05/03

ASTMD808.
ASTM D93-85
EPA9040B J" y-?*^*'-^"

3030076 03/05/03
3030065 03/05/03
3030080 03/05/03
3030078 03/05/03

Sampled: 02/26/03 17:15 Received: 02/27/03 14:05

.hpoint
]Wf
Reactive Cyanide
Reactive Sulfide
D008, Bldg. 5910 (B302323-08) Waste (L)
Flashpoint
pH
Reactive Cyanide
Reactive Sulfide
D009, Bldg. 5910 (B302323-09) Waste (L)
Flashpoint
pH
Reactive Cyanide
Reactive Sulfide

Units

Sampled: 02/26/03 17:10 Received: 02/27/03 14:05

Flashpoint .
pH
Reactive Cyanide
Reactive Sulfide
D007, Bldg. 5910 (B302323-07) Water

Reporting
Limit

125
636
ND
ND

°F
pH Units
0.0100
mg/1
6.50
"

1
"
"
"

3030076
3030065
3030080
3030078

Sampled: 02/26/03 17:25 Received: 02/27/03 14:05
162
6.88
ND
10.0

°F
pH Units
0.0100
mg/1
6.50
"

1
"
"
•

3030076
3030065
3030080
3030078

Sampled: 02/26/03 17:30 Received: 02/27/03 14:05
182
7.03
ND
ND

°F
pH Units
0.0100
mg/I
6.50
"

1
"
"
"

3030076
3030065
3030080
3030078

<Y -?-«'* XJr"

T"01, Tanker@5800 (B302323-10) Waste (L) Sampled: 02/27/03 09:20 Received: 02/27/03 14:05
J4. jint Chlorine
Flashpoint
pH

Great Lakes Analytical-Buffalo Grove

0.507
>220°F
7.73

0.100

%
°F
pH Units

1
"
"

3030106
3030076
3030065

03/06/03
03/05/03
03/05/03

The results m this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

-

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-02 1 2-008
Project Manager LisaGraczyk

Tetra Tech EMI - IL

j 200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

General Chemistry
Great Lakes Analytical— Buffalo Grove

-J
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

Notes

T002, 26 East (B302323-11) Waste (S) Sampled: 02/27/03 09:30 Received: 02/27/03 14:05
~ Percent Chlorine
^ Flashpoint
pH
_ Reactive Cyanide
Reactive Sulfide
"* T003, 27 East (B302323-12) Waste (S)

0.504
>220 °F
5.90
ND
ND

D010, 5800 S. Trailer (B302323-13) Water

— Flashpoint
pH
^DOll, DUP of D006 (B302323-14) Water
Flashpoint

Great Lakes Analytical-Buffalo Grove

1

3030106 03/06/03
3030076 03/05/03
3030090 03/06/03
3030081 03/05/03
3030079 03/05/03

03/06/03
03/06703
03/07/03
03/06/03

ASTMD808
ASTMD93-85
EPA9045C J" <-M-05 A,
EPA 7.3.3
EPA 7.3.4

03/06/03
03/05/03
03/06/03
03/05/03
03/05/03

03/06/03
03/05/03
03/06/03
03/07/03
03/06/03

ASTMD808
ASTMD93-85
EPA9045C ^ - 4 ^ - ^ >
EPA 73.3
EPA 73.4

03/05/03
03/05/03

03/05/03
03/05/03

ASTMD93-85
EPA9040B 3" </--7-«*3/a

03/05/03

03/05/03

ASTMD93-85

Sampled: 02/27/03 09:35 Received: 02/27/03 14:05

Percent Chlorine
Flashpoint
pH
Reactive Cyanide
Reactive Sulfide
-i

%
"F
pH Units
O.J30 mg/kg wet
n
6.50

0.100

0.452
>220 °F
6.72
ND
ND

0.100

%
°F
pH Units
0.130 mg/kg wet
6.50

1
"
•
"

3030106
3030076
3030090
3030081
3030079

Sampled: 02/27/03 10:45 Received: 02/27/03 14:05
159
5.13
Sampled: 02/26/03 17:10

129

°F
pH Units

1
"

3030076
3030065

Received: 02/27/03 14:05
3030076

The results m this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced m its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-02 1 2-008
Project Manager LisaGraczyk

Reported:
03/18/03 13:52

TCLP Metals by EPA 1311/6000/7000 Series Methods
Great Lakes Analytical—Buffalo Grove
Analyte

Result

D001, Bldg. 6000 (B302323-01) Waste (L)
Mercury
Arsenic
Jarium
Cadmium
Chromium
"'-'enium

ND
ND
ND
0.185
0.0850
1.92

)002, Bldg. 6000 (B302323-02) Waste (L)

0.0525
0.0835
0.0259

«ad
003, Bldg. 6000 (6302323-03) Water

Dilution

Batch

Prepared

Analyzed

Method

03/06/03
03/05/03

03/07/03
03f&6/03
i

EPA7470A
EPA6010B
it

Notes

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/I

I

3030087
3030063

It

M

N

W

H

H

"

"

"

I

t

.
.
•
.

M

M

n

N

N

N

It

•

If

"

.

H

H

It

QC

.
.

ii

03/07/03

EPA 7421

03/07/03

EPA 7470A

03/06/03
•
«

EPA6010B
"
»

N

It

.

It

"

"

GI3

Sampled: 02/26/03 15:35 Received: 02/27/03 14:05

ND
ND
ND
ND
ND

/fercury
Arsenic
Sari urn
Cadmium
'hromium
elenium
ilver

Units

Sampled: 02/26/03 15:30 Received: 02/27/03 14:05
0.000348
0.104

er
Wad

Reporting
Limit

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/1

1

3030087
3030063

•

U

m

U

N

•

»

M

03/06/03
03/05/03

.

N

it

.

n

m

m

»

U

N

N

It

M

H

"

03/07/03

EPA 7421

03/07/03
03/06/03
it

EPA 7470A
EPA6010B
n

QC

G13

Sampled: 02/26/03 15:40 Received: 02/27/03 14:05

!ercury
rsenic
arium
•*mium
ffenium
Iver

ead

Great Lakes Analytical-Buffalo Grove
'\tfX-«Av.J &A~~~~*-v^^.

ND
0.258

ND
0.415
11.9
0.486
0.384
0.429

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/I

1

.

.

3030087
3030063
.

03/06/03
03/05/03

«

it

•

n

n

ff

m

•»

n

N

M

N

it

v

n

n

N

•

It

n

" jf "^•1»

M

It

It

03/07/03

o'Sflyz
G13

EPA 7421

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Metals by EPA 1311/6000/7000 Series Methods
Great Lakes Analytical-Buffalo Grove
Reporting
Analyte

Result

Lnmt

Units

Dilution

Batch

Prepared

Analyzed

Method

03/06/03
03/06/03

03/07/03
03/f6/03

EPA7470A
EPA 6010B

Notes

D004, Bldg. 6000 (B302323-04) Waste (L) Sampled: 02/26/03 16:10 Received: 02/27/03 14:05

ND
ND
ND
ND
ND
ND
ND
ND

Mercury
Arsenic
Barium
— Cadmium
Chromium
- F " *uum

£«^_'
ll8f

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/1

1

3030087
3030089

ft

tt

M

M

rt

ft

ft

ft

n

»

"
"

ft

ft

ft

•

ft

H

•

ft

ft

*

N

It

03/07/03

EPA 7421

EPA7470A
EPA 6010B

I*

M

D005, Bldg. 5910 (B302323-05) Water Sampled: 02/26/03 17:05 Received: 02/27/03 14:05
Mercury
Arsenic
., Barium
Cadmium
• Chromium
Selenium
• Silver
Lead

0.000309
0.110

ND.
ND
ND
ND
0.0850
0.0548

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/I

1

3030087

03/06/03

3030063

03/05/03

03/07/03
03/06/03
It

ft

ft

N

M

It

ft

ft

W

N

It

ft

-

•

N

H

n

•

ft

tt

M

M

ft

•

N

n

03/07/03

EPA 7421

03/06/03
03/05/03

03/07/03
03/06/03

EPA7470A
EPA 601 OB

ft

ft

.
"

•

N

.

QC

G13

D006, Bldg. 5910 (B302323-06) Water Sampled: 02/26/03 17:10 Received: 02/27/03 14:05

ND

Mercury
Arsenic
Barium
C
'him

0.128

ND
ND
ND

C^Jum
Selenium
Silver
Lead

3.60
0.0900
0.00821

Great Lakes Analytical-Buffalo Grove

f

\ "^•"^V.

^J CS^**~*^*~ir*r*^

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/I

1

3030087
3030063

ft

*i

n

ft

fl

H

1

It

ft

n

n

H

n

n

n

ft

n

H

"

03/07/03

QC

•

G13

EPA 7421

The results m this report appfy to the samples analyzed m accordance with the chain of
custody document. This analytical report must be reproduced m its entirety

1380 Busch Parkway
Buffalo Grove, Illinois 60089
^
j

Project: Kip Nelson
Project Number: 505-02 1 2-008
Project Manager Lisa Graczyk

Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

~^

Email: info@glalabs.com
(847) 808-7766. FAX (847) 808-7772

Reported:
03/18/03 13:52

TCLP Metals by EPA 1311/6000/7000 Series Methods
Great Lakes Analytical—Buffalo Grove

—
-

Result

Analyte
D007, Bldg. 5910 (B302323-07) Water

Sampled: 02/26/03 17:15

Mercury
_, Arsenic
Barium
_ Cadmium
Chromium
-• Selenium
Silver
Lead

ND
0.433
ND
ND
ND
1.23
ND
0.0357

D008, Bldg. 5910 (B302323-08) Waste (L)

D009, Bldg. 5910 (B302323-09) Waste (L)

/ \ Wtft^

«J C^^«~^^-v^^_

Dilution

Batch

Prepared

Analyzed

Method

3030087
3030063

03/06/03
03/05/03

03/07/03
03^6/03

EPA7470A
EPA 6010B

.

.

Notes

Received: 02/27/03 14:05

0.000200
mg/1
0.0500
"
1.00
0.00500
.
0.100 "
0.0500
"
0.100 .
0.00500
.

1
"
'
.

It

QC
ft
H

.
.

.
.

.
.

'*•*'

03/07/03

EPA 7421

03/07/03
03/06/03

EPA7470A
EPA6010B

Received: 02/27/03 14:05

0.000200
mg/I
0.0500
"
1.00 .
0.00500
.
0.100 .
0.0500
.
0.0500
.
0.0550
"

I
"
.
.
.
.
.
11

3030087
3030063
.
.
.
.
.
"

03/06/03
03/05/03
.
.
.
.
»
"

"

QC
»
"
G13
03/07/03

EPA 7421

03/07/03
03/06/03

EPA7470A
EPA 601 OB

Sampled: 02/26/03 17:30 Received: 02/27/03 14:05
0.00182
ND
ND
ND
ND
0.0625
0.0830
0.242

Great Lakes Analytical-Buffalo Grove

Units

Sampled: 02/26/03 17:25
0.00123
0.0710
ND
ND
ND
0.132
0.0835
23.2

Mercury
Arsenic
_, Barium
Cadmium
-i Chromium
Selenium
- Silver
Lead

Mercury
_ Arsenic
Barium
. Cadmium
Chromium
Selenium
Silver
Lead

Reporting
Limit

0.000200
mg/I
0.0500
"
1.00 .
0.00500
.
0.100 .
010500
.
0.0500
.
0.00500
.

1
"
.
.
.
.
.
.

3030087
3030063
.
.
.
.
.
.

03/06/03
03/05/03
.
.
.
.
.
.

i*
"

u

^^^^

"
G13
03/07/03

EPA 7421

The results in this report apply to the samples analyzed m accordance with the cham of
custody document. This analytical report must be reproduced m its entirety.

GREAT
LAKES

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Reported:

03/18/03 13:52

TCLP Metals by EPA 1311/6000/7000 Series Methods
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

Notes

03/06/03
03/06/03

03/07/03
03*6/03

EPA 7470A
EPA6010B
.

T002, 26 East (B302323-11) Waste (S) Sampled: 02/27/03 09:30 Received: 02/27/03 14:05
Mercury
Arsenic
Barium
Cadmium
Chromium
J
'Tiium
r

ND
ND

ND
ND
ND
ND
ND

!feft

0.184

C.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

1

mg/1

H

>
«
.
•
•
ft

3030087
3030089

ft

ft

It

m

ft

•

p

ft

H

N

"

m

H

H

it

ft

ft

ft

»

n

ft

ft

n

n

it
"
N

N

03/07/03

EPA 7421

03/07/03
03/06/03

EPA7470A
EPA6010B

P003, 27 East (B302323-12) Waste (S) Sampled: 02/27/03 09:35 Received: 02/27/03 14:05
Mercury
Vrsenic
tarium
Cadmium
Chromium
elenium
ilver
«ad

ND
ND

ND
ND
ND
ND
ND
0327

Great Lakes Analytical-Buffalo Grove

•*• **~^**

0.000200
0.0500
1.00
0.00500
0.100
0.0500
0.0500
0.00500

mg/1

i

N

3030087
3030089
"

03/06/03
03/06/03

ft

N

M

M

N

It

"

N

n

•
it
.

•
.
•

"

m

It

ri

H

H

n

•

N

ft

"

•

"
"
"

ft

03/07/03

ft

M

EPA 7421

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

«J erA~Dorto S

1380 Buscn Parkway
Buffalo Grove, Illinois 60089
~
J

Project: Kip Nelson
Project Number 505-0212-00^
Project Manager Lisa Graczyk

Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

"^

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Reported:
03/18/0313:52

TCLP Volatile Organic Compounds by EPA Method 1311/8260B
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

QC

D001, Bldg. 6000 (B302323-01) Waste (L) Sampled: 02/26/03 15:30 Received: 02/27/03 14:05
Benzene
.^ Carbon tetrachloride
Chloro benzene
— Chloroform
1,2-Dichloroethane
-* 1,1-Dichloroethylene
Methyl ethyl ketone
" Tetrachloroethene
Trichloroethylene
Vinyl chloride

9770
ND
ND
ND
ND
ND
ND
ND.
ND
ND

50.0
50.0
50.0
50.0
50.0
50.0
250
50.0
50.0
50.0

mg/1

3030094

03/06/03

ft

ft

N

It

03/10/03

EPA8260B

it

ft

«

n

ft

ft

N

ft

ft

It

ft

ft

ft

H

It

It

0*

It

H
ft
ft

n
ft

If

ft

it

ft

M

ft

n

n

H

it

*

ft

it

M

n

K

tt

N

N

it

M

•

ft

it

98.2%
102%
95.6%
104%

Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane-d4
-" Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

500

74.5-129
69.2-137
75.5-130
64.9-123

Surrogate:
Surrogate:
Surrogate:
Surrogate:

Dibromofluoromethane
l,2-Dichloroethane-d4
Toluene-dS
4-Bromofluorobenzene

Great Lakes Analyticai-Buflalo Grove

y^"J trcjA^.

«J £^V-L

238
ND
ND
ND
ND
ND
ND
ND
142
ND

10.0
10.0
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0

it

"
"
"
"

QC

114%
121%
126%
122%

mg/I

100

3030094

03/06/03

03/11/03

EPA8260B

N

«

«

It

It

ft

M

•

n

n

n

•

»

v

M

n

•

i

it

it

a

ft

n

n

H

it
n

ft

ft

ft
tt

it

it

ft

n

H

•

•

N

•

n

N

ft

•

n

it

n

w

74.5-129
69.2-137
75.5-130
64.9-123

w

n

ft

: D002, Bldg. 6000 (B302323-02) Waste (L) Sampled: 02/26/03 15:35 Received: 02/27/03 14:05
Benzene
Carbon tetrachloride
Chloro benzene
_ Chloroform
1,2-Dichloroethane
i 1,1-Dichloroethylene
Methyl ethyl ketone
* Tetrachloroethene
Trichloroethylene
Vinyl chloride

Notes

"
"
"
"

The results m this report appfy to the samples analyzed in accordance with the chain of
custody document This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EM-IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Volatile Organic Compounds by EPA Method 1311/8260B
Great Lakes Analytical—Buffalo Grove
Analyte
D003, Bldg. 6000 (B302323-03) Water
Benzene
, Carbon tetrachloride
Chlorobenzene
- Chloroform
' 1,2-Dicnloroethane
•" 1 " Dichloroethylene
1 ^ j l ethyl ketone
^ 1 eJfachloroethene
Trichloroethylene
Vinyl chloride

Result

Reporting
Lnmt

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

0.300
0.300
0.300
0.300
0.300
0.300
1.50
0.300
0.300

"
"

0.150

.

92.2%
92.2%
96.4%
127%

5 D004, Bldg. 6000 (B302323-04) Waste (L) Sampled: 02/26/03 16:10

- Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane-d4
- Surrogate: Toluene-dS
Surrogate: 4-Bromofluorobenzene

Great Lakes Analytical-Buffalo Grove

S \ »"*-*Vv.

Dilution

Batch

Prepared

Analyzed

Method

Notes

Sampled: 02/26/03 15:40 Received: 02/27/03 14:05

Surrogate: Dibromofluoromethane
Surrogate: I ' ,2-Dichloroethane-d4
' Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
- 1,1-Dichloroethylene
Methyl ethyl ketone
J
"
-.hloroethene
T^fttoroethylenc
"* Vinyl chloride

Units

0.471
ND
ND
ND
ND
ND
ND
ND
ND
ND

0.300
0.300
0.300
0.300
0.300
0.300
1.50
0.300
0.300
0.150
91.8%
90.8%
97.8%
l63%

rag/I
.
"
.

150
»

QC

3030094 03/06/03
.
.
•

.

.

.
"

"

"

.

"

03/12/03
"

EPA8260B

»

"

n

.

"

"

"

.

74.5-129
692-137
75.5-130
64.9-123

"
"
"
"

Received: 02/27/03 14:05
mg/1
.
"
'
"
"
'
"
"
.
74.5-129
69.2-137
75.5-130
64.9-123

150
.

.

3030094
»

.

H
QC

03/06/03
.

.

03/12/03

EPA8260B

.

"
"
"
"

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@gJalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager: Lisa Graczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13 :52

TCLP Volatile Organic Compounds by EPA Method 1311/8260B
Great Lakes Analytical—Buffalo Grove
Analyte

Result

D005, Bldg. 5910 (B302323-05) Water
Benzene
„ Carbon tetrachloride
Chlorobenzene
- Chloroform
1 ,2-Dichloroethane
• 1,1-Dichloroethylene
Methyl ethyl ketone
Tetrachloroethene
Trichloroethylene
Vinyl chloride
Surrogate: Dibromofluoromethane
Surrogate: 1.2-DicUoroethane-d4
Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

Reporting
Limit

Surrogate;
Surrogate:
Surrogate:
Surrogate:

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND
ND
ND
ND
ND
15.4
ND
0.932

ND

Dibromofluoromethane
l,2-Dichloroethane-d4
Toluene-dS
4-Bromofluorobenzene

Great Lakes Analytical—Buffalo Grove
f \ *^-«V-

Dilution

Batch

Prepared

Analyzed

Method

Notes

QC

Sampled: 02/26/03 17:05 Received: 02/27/03 14:05
0.300
0.300
0.300
0.300
0.300
0.300
1.50
0.300
0.300
0.150
95.0%
94.0%
95.6%
100%

D006, Bldg. 5910 (B302323-06) Water Sampled: 02/26/03 17:10
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1 ,2-Dichloroethane
1,1 -Dichloroethylene
Methyl ethyl ketone
Tetrachloroethene
Trichloroethylene
Vinyl chloride

Units

«J f i ^ A ~ v ^ v _ w v » ^ .

0.300
0.300
0.300
0.300
0.300
0.300
1.50
0.300
0.300
0.150

94.4%
95.2%
100%
102%

mg/1

150

m

n

N

It

3030094

03/06/03

ft

ft

M

0
II

•

n

it

n

•

w

n

N

ft

it

*

rt

EPA8260B
ft

M

N

tt
N

M

ft

it

•

n

It

H

it

H

n

*

N

M

t

n

ft

«

ft

n

•

n

ft

N

74.5-129
69.2-137
75.5-130
64.9-123

ft

03/12/03

ft

*

It

a

W

n

"
"
"
"

QC

Received: 02/27/03 14:05
mg/1

3030094

03/06/03

03/12/03

N

.

150
n *

H

n

n

rt

n

it

ft

*

n

n

n

it

ft

It

ft

it

n

w

it

it

ft
M

N

n

n

n

N

H

It

ft

it

74.5-129
69.2-137
75.5-130
64.9-123

ft

H

ft

ft

ft
N

M

ft

H

M

it

M

rt

N

it

ft

•

EPA 8260B

ft

H

tt

_}

Ar T•/rn
*••*

i*

"
"
"
"

The results in this report appfy to the samples analyzed in accordance -with the cham of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago FL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Reported:
03/18/03 13:52

TCLP Volatile Organic Compounds by EPA Method 1311/8260B
Great Lakes Analytical—Buffalo Grove
Analyte
D007, Bldg. 5910 (B302323-07) Water
Benzene
.„ Carbon tetrachloride
Chlorobenzene
— Chloroform
1,2-Dichloroethane
~' ' " Oichloroethylene
j - j i ethyl ketone
~ TetrachloFoethene
Trichloroethylene
Vinyl chloride
Surrogate: Dibromofluoromethane
Surrogate: l,2-Dichloroethane-d4
* Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

Sampled: 02/26/03 17:15 Received: 02/27/03 14:05
58.5

ND
ND
ND
ND
ND
ND
ND
ND
ND

10.0
10.0
10.0
10.0
10.0

mg/1

10.0
50.0
10.0
10.0
10.0

100

QC

3030094

03/06/03

tt

ft

n

ft

It

ft

It

03/11/03

EPA8260B

0ft
ft

tt

tt
ft

ft

ft

N

tt

tt

H

H

tt

«

tt

ft

N

N

tt

K

tt

N

tt

ft

N

74.5-129
69.2-137
75.5-130
64.9-123

H

It

ft

tt

ft

N

ft

N

88.2%
95.8%
97.4%
94.4%

ft

H

•

tt

ft

ft

tt

tt

tt
tt

N

tt

ft

ft

"
"
"
"

D008, Bldg. 5910(8302323-08) Waste (L) Sampled: 02/26/03 17:25 Received: 02/27/03 14:05
Benzene
Carbon tetrachloride
Chlorobenzene
. Chloroform
1 ,2-Dichloroethane
• 1,1-Dichloroethylene
Methyl ethyl ketone
-.hloroethene
1 flweoroethylene
* Vinyl chloride
_ Surrogate: Dibromofluoromethane
Surrogate: 1,2-Dichloroethane-d4
~ Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

Great Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

G23, QC

50.0
50.0
50.0
50.0
50.0
50.0

mg/1

500

3030094

03/06/03

03/10/03

•

«

»

*

•

»

n

tt

n

H

•

it

tt

n

»

250

ft

ft

H

ft

tt

N

50.0
50.0
50.0

86.0%
91.8%
95.7%
106%

tt
tt

tt

H
ft

.

tt

M

tt

H

74.5-129
69.2-137
75.5-130
64.9-123

Notes

«

ft
N

ft
1

ft
•

«

n
H

ft

»

"
"
"
.

ft
tt

.

n
H

1

N

ft

EPA 8260B

N

It

N

tt

It

.

The results mthis report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
1847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager: LisaGraczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Volatile Organic Compounds by EPA Method 131178260B
Great Lakes Analytical—Buffalo Grove
Result

Analyte

Reporting
Limit

Units

D009, Bldg. 5910 (B302323-09) Waste (L) Sampled: 02/26/03 17:30
Benzene
,. Carbon tetrachloride
Chlorobenzene
— Chloroform
1 ,2-Dichloroethane
1,1-Dichloroethylene
Methyl ethyl ketone
~~ Tetrachloroethene
__ Trichloroethylene
Vinyl chloride

187
ND
ND
ND
ND
ND
ND
66.2
ND
ND

50.0
50.0
50.0
50.0

Batch

Prepared

Analyzed

Method

Received: 02/27/03 14:05
mg/I

500

3030094

03/06/03

»

ft

n

ft

it

tt

n

It

•

n

03/10/03

EPA8260B
ft

9a

ft

tt

n

ft

•

tt

n

tt

•

H

tt

•

n

250

tt

•

tt

tt

n

n

50.0
50.0
50.0

it

«

«

tt

«

M

M

n

tt

«

N

N

tt

W

B

tt

tt

N

ft

tt

H

tt

It

74.5-129
69.2-137
75.5-130
64.9-123

Surrogate:
Surrogate:
Surrogate:
Surrogate:

Dibromofluoromethane
l,2-DicUoroethane-d4
Toluene-dS
4-Bromofluorobenzene

3reat Lakes Analytical-Buflalo Grove

S \ "^-^V-

«J (fA*^~~-^_-vv~^_

1.05

ND
ND
ND
ND
ND
ND
7.10
ND
ND

1.00
1.00
1.00
1.00
1.00
1.00
5.00
1.00
1.00
1.00

81.4%
92.7%
103%
119%

QC

mg/1

10

3030094

03/06/03

03/12/03

EPA8260B

tt

M

N

tt

n

*

«

n

n

n

n

«

ft

N

M

n

tt

«

ft

W

N

ft

It

l>

n

M

it

tt

it

ft

n

H

tt

n

tt

a

R

N

n

n

H

n

ft

ft

it

n

ii

<t

tt

N

n

M

n

v

74.5-129
69.2-137
75.5-130
64.9-123

'^^ri

"
"
"
"

T001, Tanker@5800 (B302323-10) Waste (L) Sampled: 02/27/03 09:20 Received: 02/27/03 14:05
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1 ,2-Dichloroethane
1 , 1 -Dichloroethy lene
Methyl ethyl ketone
Tetrachloroethene
Trichloroethylene
Vinyl chloride

Notes
QC

50.0
50.0

91.6%
95.5%
98.0%
97.6%

Surrogate: Dibromofluoromethane
Surrogate: l,2-Dichloroethane-d4
~ Surrogate: Toluene-dS
Surrogate: 4-Bromofluorobenzene

Dilution

'^•H

"
"
"

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

^^

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Volatile Organic Compounds by EPA Method 1311/8260B
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

Notes

D010, 5800 S. Trailer (B302323-13) Water Sampled: 02/27/03 10:45 Received: 02/27/03 14:05
Benzene
„ Carbon tetrachloride
Chlorobenzene
— Chloroform
1 ,2-Dichloroethane
-1 * ' Oichloroethylene
»^^yl ethyl ketone
Tetrachloroethene
Trichloroethylene
Vinyl chloride

ND
ND
ND
ND
ND
ND
2.91
ND

ND
ND

Surrogate: Dibromofluoromethane
Surrogate: 1 ,2-Dichloroethane-d4
" Surrogate: Toluene-dS
Surrogate: 4-Bromofluorobenzene

0.300
0.300
0300
0.300
0.300
0300
1.50
0.300
0.300
0.150

QC

mg/1

150

3030094

03/06/03

03/12/03

•

M

n

n

WH

•

ft

ft

ft

•

It

ft

EPA8260B

ft

ft

It

N

»

H

ft

ft

It

It

ft

ft

M

N

ft

ft

ft

N

tt

H

ft

ft

N

it

n

N

n

it

N

N

N

n

n

n

•

ft

»

M

N

ft

87.0%
91.6%
96.0%
103%

74.5-129
69.2-137
75.5-130
64.9-123

ft

.

_

. Surrogate: Dibromofluoromethane
Surrogate: 1 ,2-Dichloroethane-d4
- Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene

Great Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
15.2
ND
0.843

ND

0.300
0.300
0.300
0.300
0.300
0.300
1.50
0.300
0.300
0.150

91.6%
93.0%
95.8%
101%

mg/1
tt

150
ft

3030094

N

ft

tt

H

N

It

It

N

«
ft

tt

•
N

W

ft

tt

•

74.5-129
69.2-137
75.5-130
64.9-123

QC
03/06/03

tt

s

03/12/03

ft

M

H

N

V

'T

"
"
"
"

D011, DUP of D006 (B302323-14) Water Sampled: 02/26/03 17:10 Received: 02/27/03 14:05
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1 ,2-Dichloroethane
* 1,1-Dichloroethylene
Methyl ethyl ketone
* '
'hloroethene
IfWHoroethylene
'' Vinyl chloride

,

-T- Lf'*}-*^

tt
tt

H

ft

•

EPA8260B
N

ft
ft

M

tt

tt

»

H

ft

B

it

t

ft

»

ft

ft

ft

•

M

M

M

n

ft

"
.
"
"

tt

.

T

*~r—

.

The results in this report appfy to the samples analyzed m accordance mth the chain of
custody document. This analytical report must be reproduced m its entirety.

&

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project Kip Nelson
Project Number 505-0212-008
Project Manager: LisaGraczyk

Tetra Tech EM - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

Polychlorinated Biphenyls by EPA Method 8082
Great Lakes Analytical—Buffalo Grove

~i

Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

03/11/03

03/11/03

EPA 8082

Notes

D001, Bldg. 6000 (B302323-01) Waste (L) Sampled: 02/26703 15:30 Received: 02/27/03 14:05
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
3
CB-1254
>CB-1260
Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

ND
ND
ND
ND
ND
ND
ND

7430
7430
7430
7430
7430
7430
7430
85.2%
85.5%

ug/kg

1

3030169

tt

tt

ft

ft

ft

ft

n

N

ft
ft

ft
tt

M

ft

ft

10-125
10-143

H

N

•

M

N

ft

N

ft

N

II

»

ft

H

H

It

H

ft

ft

n

9 It

" '

"

rf

^

if

O002, Bldg. 6000 (B302323-02) Waste (L) Sampled: 02/26/03 15:35 Received: 02/27/03 14:05
PCB-1016
- PCB-1221
PCB-1232
-1 PCB-1242
j PCB-1248
"" PCB-1254
PCB-1260
Surrogate: Tetrachloro-meta-xylene
~ Surrogate: Decachlorobiphenyl

ND
ND
ND
ND
ND
ND
ND

7350
7350
7350
7350
7350
7350
7350
80.6%
84.6%

ug/kg

1

3030169

03/11/03

03/11/03

R

R

tt

n

n

n

R

R

ft

n

n

•

«

n

n

tt

W

R

R

R

R

«

R

M

*

R

R

R

R

"

B

M

10-125
10-143

n

ft

n

n

tt

tt

EPA 8082
n

«
•
•
»
n

. D003, Bldg. 6000 (B302323-03) Water Sampled: 02/26/03 15:40 Received: 02/27/03 14:05
PCB-1016
' PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

Great Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
ND

50.0
50.0
50.0
50.0
50.0
50.0
50.0
68.9%
29.9%

ug/1

3030124

G12, G6

03/07/03

03/11/03

EPA 8082

10-110
10-140

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI-EL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

Porychlorinated Biphenyls by EPA Method 8082
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

03/11/03

03/11/03

EPA 8082

Notes

D004, Bldg. 6000 (B302323-04) Waste (L) Sampled: 02/26/03 16:10 Received: 02/27/03 14:05
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
P~TM254
I
1260

ND
ND
ND
ND
ND
ND
ND

7430
7430
7430
7430
7430
7430
7430

ug/kg

1

3030169

tt

it

tt

ft

M

tt

•t

»

«

R

tt

H

It

R

It

R

H

H

M

R

I.

It

.

tt

ft

R

R

It

H

ft

n

It

W

It

It

"

"

"

80.2%
25.9%

Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

01

.

10-125
10-143

"

D005, Bldg. 5910 (B302323-05) Water Sampled: 02/26/03 17:05 Received: 02/27/03 14:05
PCB-1016
•' PCB-1221
PCB-1232
- PCB-1242
PCB-1248
PCB-1254
PCB-1260

ND
NDND
ND
ND
ND
ND

50.0
50.0
50.0
50.0
50.0
50.0
50.0

ug/1

1

3030124

03/07/03

R

II

N

It

ft

R

R

N

N

tt

It

It

ft

ft

•

ft

M

R

R

tt

R

R

n

R

R

N

59.6%
40.1%

Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

G12, G6
03/11/03

EPA 8082
N
R

It
ft

ft

tt

ft

•

N

ft

it

n

it

»

10-110
10-140

n

. D006, Bldg. 5910 (B302323-06RE1) Water Sampled: 02/26/03 17:10 Received: 02/27/03 14:05
POM016
*P
'221
PfJto»f232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

Great Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
ND

50.0
50.0
50.0
50.0
50.0
50.0
50.0

66.8%
28.0%

G12.G6

ug/l

1

3030229

03/12/03

ft

N

ft

N

N

n

03/14/03
ft

EPA 8082
tt

-

"
"

n

ft

*

tt

«

R

It

H

R

n

ft

10-110
10-140

tt

M

H

ft

tt
M

ft
ft

N

n

it

n

*

it

n

it

H

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number: 505-0212-008
Project Manager. Lisa Graczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:

03/18/03 13:52

Polychlorinated Biphenyls by EPA Method 8082
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

03/11/03

03/11/03

EPA 8082

Notes

D007, Bldg. 5910 (B302323-07) Water Sampled: 02/26/03 17:15 Received: 02/27/03 14:05
PCB-1016
.. PCB-1221
PCB-1232
- PCB-1242
PCB-1248
- PCB-1254
PCB-1260

ND
ND

ND
ND
ND
ND
ND

7580
7580
7580
7580
7580
7580
7580

1

ft

It

«t

It

D008, Bldg. 5910 (B302323-08) Waste (L) Sampled: 02/26/03 17:25

ND
NDND
ND
ND
ND
ND

Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

7140
7140
7140
7140
7140
7140
7140
59.6%
47.7%

3030169

ft

•
•

"
ft

•

R

II

H

N

tt

n

H

H

U

N

tt

tt

N

It

It

it

n

it

it

R

t

"

n

if

n

I

"

10-125
10-143

76.7%
83.3%

Surrogate: Tetrachloro-meta-xylene
* Surrogate: Decachlorobiphenyl

PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260

ug/kg

>»•

rf

Received: 02/27/03 14:05
ug/kg

1

10-125
10-143

EPA 8082

3030169

03/11/03

03/11/03

ft

ft

It

tt

ft

ft

It

"

ft

N

0

ft

ft

N

H

N

tt

ft

"

"

tt

N

It

tt

»

n

tt

ft

H

n

D009, Bldg. 5910 (B302323-09) Waste (L) Sampled: 02/26/03 17:30 Received: 02/27/03 14:05
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

3reat Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
ND

7210
7210
7210
7210
7210
7210
7210
76.5%
92.0%

ug/kg

1

tt

tt

3030169

H

•

N
ft

tt

It

H

03/11/03

03/12/03

•

ft

EPA 8082

R

tt

n

"

"

"

«

N

N

N

•

M

n

•

»

N

tt

tt

tt

ft

ft

ft

*

a

It

tt

rt

it

ft

n

a

10-125
10-143

•

^

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email. mfo@glalabs com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number: 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

Polychlorinated Biphenyls by EPA Method 8082
Great Lakes Analytical—Buffalo Grove
Analyte
T001, Tanker@5800 (B302323-10) Waste (L)
PCB-1016
. PCB-1221
PCB-1232
- PCB-1242
PCB-1248
T
-1254
^,_--1260

Result

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

Notes

Sampled: 02/27/03 09:20 Received: 02/27/03 14:05
ND
ND
ND
ND
ND
ND
ND

7650
7650
7650
7650
7650
7650
7650
777%
564%

Surrogate. Tetrachloro-meta-xylene
., Surrogate: Decachlorobiphenyl

ug/kg
.
.
.
.
.

1
.
.
.
.
.

10-125
10-143

3030169 03/11/03
03/12/03
.
.
.
.
. . . .
.
.
.
.
.
.
.
.
.
.
.
.
"
.

.

EPA 8082

.

T002, 26 East (B302323-11) Waste (S) Sampled: 02/27/03 09:30 Received: 02/27/03 14:05
PCB-1016
PCB-1221
PCB-1232
PCB-1242
4 PCB-1248
' PCB-1254
PCB-1260

ND
NL>
ND
ND
ND
ND
ND

7080
7080
7080
7080
7080
7080
7080
930%
112%

Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl

ug/kg
.
.
.
.
.
.

1
.
.
.
.
.
.

10-125
10-143

3030169
.
.
.
.
.
.

03/11/03
.
.
.
.
.
.

03/12/03
.
.
.
.
.
.

EPA 8082

03/11/03
.
.

03/12/03
.
.

EPA 8082

"
"

T003, 27 East (B302323-12) Waste (S) Sampled: 02/27/03 09:35 Received: 02/27/03 14:05

p^-ioie
1221
PfcHfl232
PCB-1242
PCB-1248
PCB-1254
PCB-1260

Surrogate: Tetrachloro-meta-xylene
Surrogate. Decachlorobiphenyl

Great Lakes Analytical-Buffalo Grove
/~\

ND
ND
ND
ND
ND
ND
ND

7500
7500
7500
7500
7500
7500
7500
641%
682%

ug/kg
.
.
"
.
.
.
10-125
10-143

1
.
.

3030169
.
.

.
.
.

.
.
.

.
.
.

.
.
.

"
"

The results in this report apply to the samples analyzed m accordance with the chain of
custody document. This analytical report must be reproduced m its entirety

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago EL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project Kip Nelson
Project Number: 505-0212-008
Project Manager. LisaGraczyk

Reported:
03/18/03 13:52

TCLP Pesticides by EPA Method 1311/8081A
Great Lakes Analytical—Buffalo Grove
Analyte
D001, Bldg. 6000 (B302323-01) Waste (L)
Chlordane (tech)
indrin
leptachlor (and its epoxide)
gamma-BHC (Lindane)
Vlethoxychlor
[oxaphene

Result

Sampled : 02/26/03 15:30

ND
ND
ND
ND
ND
ND

Chlordane (tech)
'ndrin
[eptachlor (and its epoxide)
amma-BHC (Lindane)
lethoxychlor
oxaphene
urrogate: Tetrachloro-meta-xylene
urrogate: Decachlorobiphenyl

Great Lakes Analytical-Buffalo Grove

6.00
0.600
0.300
0.300
6.00
24.0

Units

Dilution

Batch

Prepared

Analyzed

Method

03/11/03
•„

EPA8081A

Notes

Received: 02/27/03 14:05
mg/kg

1

3030161

03/10/03

it

•

H

n

•

N

tt

n

ft

It

•

ft

ft

tt

ft

tt

ft

N

H

tt

H

ft

M

N

H

tt

•t

tt

78.0%
82.4%

Surrogate: Tetrachloro-meta-xylene
Surrogate: Decachlorobiphenyl
>002, Bldg. 6000 (B302323-02) Waste (L)

Reporting
Limit

28.2-110
10-124

H

n

tt

H

Sampled: 02726/03 15:35 Received: 02/27/03 14:05

ND
ND
0.342
ND
ND
ND

6.00
0.600
0.300
0.300
6.00
24.0

374%
85.7%

rag/kg
tt

1
tt

3030161

03/10/03

n

n

03/11/03
W

EPA8081A
tt

«

tt

ft

tt

tt

tt

ii

n

•

n

n

«

28.2-110
10-124

03/11/03
03/11/03

»

n

ft

H

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch ParkwayBuffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number: 505-0212-008
Project Manager: LisaGraczyk

Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

Units

D001, Bldg. 6000 (B302323-01) Waste (L) Sampled: 02/26/03 15:30
o-Cresol
m,p-Cresols
Cresol
- 1,4-Dichlorobenzene
2,4-Dinitrotoluene
" T xachloro benzene
achlorobutadiene
iK&achloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
.,

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

;ol

Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Great Lakes Analytical—Buffalo Grove

/ I *"*• *M*

«J £^A*

Prepared

Analyzed

Method

03/07/03

03/07/03

EPA 8270C

Notes

1

3030121

tt

It

It

tt

tt

»

ft

M

It

H

rt
n

W

ft

•

n

N

tt

it

n

n

it

ft

it

n

M

it

n

N

it

ft

n

it

M

H

n

it

m

M

N

tt

ft

ft
tt

ft

N

it

It

W

ft

"n

n

n

•

it

it

n

tt

ft

n

n

tt

it

n

n

N

n

it

n

n

m

10-110
10-110
10-113
10-110
10-116
10-181

tt
R

"
"
"
"
"
"

H
H

"

Sampled: 02/26/03 15:35 Received: 02/27/03 14:05

, ND

4|^)ichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol

mg/1

228%
154%
105%
85.3%
90.5%
ND
ND

o-Cresol
m,p-Cresols

Batch

Received: 02/27/03 14:05

47.1%

Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4
D002, Bldg. 6000 (B302323-02) Waste (L)

30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3

Dilution

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

30.3
30.3
30.3
30.3
30.3
30.3
30.3
30.3
"30.3
30.3
30.3
30.3
30.3

92.3%
78.6%
366%
107%
73.3%
92.1%

mg/1

1

3030121

«

H

.

03/07/03
»

03/10/03
M

EPA 8270C
R

R

R

R

.

R

M

"

»

"

"

"

"

R

It

R

R

R

H

ft

M

*

It

(t

.

R

It

R

R

R

R

R

R

R

R

R

R

R

R

R

R

R

R

H

R

R

R

It

.

R

It

R

.

«

"

R

R

R

R

R

.

R

R

R

R

R

R

10-110

-

10-110
10-113
10-110
10-116
10-181

"
"
"
"
"

H

"

"

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EM-IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number: 505-0212-008
Project Manager LisaGraczyk

Reported:
03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Result

Analyte

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

03/10/03

EPA8270C

Notes

D003, Bldg. 6000 (B302323-03) Water Sampled: 02/26/03 15:40 Received: 02/27/03 14:05
o-Cresol
- m,p-Cresols
Cresol
— 1,4-Dichlorobenzene
2,4-Dinitrotoluene
" Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
,„ Nitrobenzene
Pentachlorophenol
_. Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND-

Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
_ Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
, Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

200
200
200
7.50

Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Great Lakes Analytical-Buffalo Grove

f \ *V<""1»

••J C^^-«"-*-W-N«.

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

1

3030141

03/10/03

H

«

n

n

n

it

*

ft
it

*

0.200
0.200
0.500
3.00
2.00

it

it

ft

n

tt

tt

ft

tt

n

ft

it

tt

tt

H

tt

•

ft

n

n

»

M

n

n

n

w

tt

•

tt

it

H

n

ft

ft

tt

n

N

it

it

•

100

9

n

»

•

H

H

n

400

ft

n

n

n

N

n

2.00
0. 0400 %
19.2%
41.2%
44.8%
49.0%
51.6%

N

N

it

n

M

ft

"

"

200
200
200
7.50
0.200
0200
0.500
3.00

100
100
5.00
400
2.00
23.8%
14.5%
44.8%
41.6%
54.4%
50.8%

10-110
10-110
10-113
10-110
10-116
10-181

ft

"

^ _^

tt

tt

5.00

~ D004, Bldg. 6000 (B302323-04) Waste (L) Sampled: 02/26/03 16:10
o-Cresol
m,p-Cresols
Cresol
1 ,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
' Pentachlorophenol
Pyridine
" 2,4,5-Trichlorophenol
2,4,6-Trichlorophenol

mg/I

tt

L

"
"
"
"

Received: 02/27/03 14:05
mg/1

1

3030141

n

n

n

03/10/03

N

M

n

n
N

tt

ft

M

n

ft

n

H

H

H

N

rt

n

tt

03/10/03

EPA8270C

it

n

it

R

n

it

n

n

^^M
^BP

.
tt

ft

tt

N

it

n

H

n

it

n

it

M

N

It

H

tt

H

It

10-110
10-110
10-113
10-110
10-116
10-181

ft

n

tt
•
tt

n

n

tt

n

n

ft
tt

M

N

H
tt

It

ft
tt

"
"
"
"
"

The results in this report appfy to the samples analyzed in accordance with the cham of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago PL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: K'o Nelson
Project Number 5C >-0212-008
Project Manager LLaGraczyk

Reported:
03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Analyte

Result

D005, Bldg. 5910 (B302323-05) Water
o-Cresol
, m,p-Cresols
Cresol
- 1,4-Dichlorobenzene
2,4-Dinitrotoluene
I
•'Chlorobenzene
}
chlorobutadiene
~ He^chloroethane
5 Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4
D006, Bldg. 5910 (B302323-06) Water
o-Cresol
m.p-Cresols
"C
1
1 .^..^Chlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
- Hexachloroethane
Nitrobenzene
• Pentachlorophenol
Pyridine
" 2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Great Lakes Analytical-Buffalo Grove

f

\

"^ *M-i

*J CAA—^-, -tt. y^,-,,

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

03/10/03

03/10/03

EPA8270C

Notes

Sampled: 02/26/03 17:05 Received: 02/27/03 14:05

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND-

200
200
200
7.50

mg/1

1

H

H

N

ft

ft

"

•

tt

0.200
0.200
0.500
3.00
2.00

100
5.00
400
2.00
25.2%
15.9%
48.8%
48.4%
56.8%
56.0%

3030141

*•
ft

it

It

it

•

«

n

ft

It

n

tt

tt

ft

ft

it

ft

n

n

ft

n

N

N

ft

ft

N

M

It

.

N

N

•

n

n

H

H

it

•

N

n

tt

ft

tt

K

n

N

tt

ft

ft

ft

It

K

tl

It

n

u

n

N

„

10-110
10-110
10-113
10-110
10-116
10-181

•

*

"

"

rt

tt

n

H

"
It

It

rt

H

n

it

n

it

Sampled: 02)76/03 17:10 Received: 02/27/03 14:05

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
29.7
77.2%
76.4%
54.8%
90.3%
68.3%
82.3 %

mg/1

1

3030121

N

•

ft

03/07/03
ft

03/07/03
tt

EPA8270C
N

H

N

•

tt

tt

ft

ft

n

It

tt

ft

ft

n

H

•

tt

It

ft

n

ft

ft

N

H

tt

ft

ft

M

ft

ft

ft

ft

N

tt

tt

H

ft

H

•

N

tt

•

N

N

it

tt

H

ft

N

N

•

M

M

N

n

ft

N

«

tt

n

n

n

n

•

K

n

n

tt

10-110
10-110
10-113
10-110
10-116
10-181

„
H

It

It

n

it

tt

n

H

It

If

H

n

it

it

it

it

tt

it

n

The results m this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced m its entirety.

1380Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Analyte
D007, Bldg. 5910 (B302323-07) Water
o-Cresol
-, m,p-Cresols
Cresol
- 1,4-Dichlorobenzene
2,4-Dinitrotoluene
' Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
„ Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
J Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Result

Reporting
Limit

Sampled: 02/26/03 17:15

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
125%
80.0%
784%
93.6%
79.0%
85.2%

Units

Dilution

Batch

Prepared

Analyzed

Method

Notes

03/07/03

03/10/03

EPA8270C

Received: 02/27/03 14:05
mg/I

1

.

R

R

»

*R

R

H

R

R

R

R

R

R

R

H

R

R

tt

R

R

R

R

R

H
H

'

3030121

R

R

R

H

It

R

H

R

R

R

N

.

R

H

R

R

R

R

H

H

R

R

*

R

H

.

R
R

R

.

H

R

R

R

R

R

R

H

a

R

R

R

R

R

H

10-110
10-110
10-113
10-110
10-116
10-181

"
"
"
"
"
"

^.^^

R
R

"

H

"

H

D008, Bldg. 5910 (B302323-08) Waste (L) Sampled: 02/26/03 17:25 Received: 02/27/03 14:05
o-Cresol
m,p-Cresols
' Cresol
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol

Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Great Lakes Analytical-Buffalo Grove

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
30.0
116%
82.2%
460%
118%
81.0%
88.8%

mg/1

1

tt

ft

3030121

03/07/03

tt

03/10/03

tt

ft

EPA8270C
tt

ft

it

K

it

it

n

tt

n

M

n

it

it

tt

•

n

it

»

n

it

tt

it

ft

H

tt

H

tt

ft

•

ft

ft

it

n

tt

n

^^

tt

M

.
R

R

H

H

R

R

R

R

R

R

R

R

R

R

R

R

R

R

R

R

It

R

R

R

"
"
"
"
"
"

"

"

H

"
"

H
H

10-110
10-110
10-113
10-110
10-116
10-181

.

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager Lisa Graczyk

Tetra Tech EMI-IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:

03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Analyte

Result

Reporting
Limit

D009, Bldg. 5910 (B302323-09) Waste (L) Sampled: 02/26/03 17:30
o-Cresol
„ m,p-Cresols
Cresol
- 1,4-Dichlorobenzene
2,4-Dinitrotoluene
ichlorobenzene
ichlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

ND
ND
ND
ND
ND
ND '

ND
ND
ND
ND
ND
ND
ND

Units

Dilution

Batch

Prepared

Analyzed

Method

3030121 03/07/03

03/10/03

EPA8270C

Received: 02/27/03 14:05

29.7

mg/1

1

29.7
29.7
29.7
29.7
29.7

'
.
.
'
"

.
.
.

.
.

.
.

•*
.
.

297
29.7
29.7
29.7
29.7
29.7
29.7

.
"
"
.
"
.
.

.

.

.

.

.
.

.
.

.
.

777%
79.8%
400%

70-770
10-110
10-113

"
"
"

101%

10-110

n

10-116
10-181

"
"

70.7%
87.9%

o-Cresol
m.n-Cresols

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

•>!
!HB0ichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

Great Lakes Analytical-Buffalo Grove

/~~\ w-oL,-

J c^v^.

.
.
"

"
n

Sampled: 02/27/03 09:20 Received: 02/27/03 14:05
3030141

.
.

•

T001, Tanker@5800 (B302323-10) Waste (L)

200
200
200
7.50
0.200
0.200
0.500
3.00
'2.00

Notes

03/10/03

H
H

n

mg/I

1

03/10/03

.
"
.
.
.
.

.

.

.

.

.
.
.
.

.
.
.
.

.
.
.
.

.
.
.
.

5.00

.

.

.

.

.

400
2.00

.

.

.

.

.

EPA8270C

100

23.4%
14.3%
50.8%
50.4%
57.6%
54.0%

10-110
10-110
10-113
10-110
10-116
10-181

"
"
"
"
"
"

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced m its entirety.

GF.1AT
1380Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI-L
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/03 13:52

TCLP Semivolatiles by EPA Method 1311/8270C
Great Lakes Analytical—Buffalo Grove
Analyte

Result

D010,5800 S. Trailer (B302323-13) Water
o-Cresol
.^ m,p-Cresols
Cresol
— 1,4-Dichlorobenzene
2,4-Dinitrotoluene
' * Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
-" 2,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol
" Surrogate: Phenol-d6
Surrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl
Surrogate: 2,4,6-Tribromophenol
Surrogate: p-Terphenyl-dl 4

3reat Lakes Analytical—Buffalo Grove
y^ wAc.

J <>X-~s~*^^->_

Reporting
Limit

Units

Dilution

Batch

Prepared

Analyzed

Method

EPA8270C

Notes

Sampled: 02/27/03 10:45 Received: 02/27/03 14:05

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND-

200
200
200
7.50
0.200
0.200
0.500
3.00
2.00

mg/1

1

3030141

03/10/03

03/10/03

it

ft

rt

it

*

ft

ft

tt

ft

ft

n

N

n

M

n

ft
»
n

tt

ft

n

N

n

N

M

N

n

n

n

H

it

ft

n

tt

it

ft

it

tt
ft

ft
N

N

ft

,

n

N

n

n

n

100

N

n

n

n

R

H

5.00

it

«

n

n

n

ft

400

It

K

,.

2.00

It

tt

it

n

n

ft

11.2%
19.3%
56.4%
54.8%
62.4%
59.2%

10-110
10-110
10-113
10-110
10-116
10-181

^_

»
tt

it

n

n

n

it

tt

tt

n

u

n

n

It

It

n
It

tf

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.

^

1380 Busch Parkway
Buffalo Grove, Illinois 60089

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager LisaGraczyk

Tetra Tech EMI -IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Reported:
03/18/0313:52

TCLP Herbicides by EPA Method 1311/8151A
North Creek Analytical - Bothell
Analyte
D001, Bldg. 6000 (B302323-01) Waste (L)

2,4-D
2,4,5-TP (Silvex)

Result

•

J-TP (Silvex)

Surrogate: 2,4-DCAA

Great Lakes Analytical-Buffalo Grove

/l**~tr(i-

Units

Dilution

Batch

Prepared

Analyzed

Method

03/11/03
-

03/13/03
• .

EPA8151A

Notes

Sampled: 02/26/03 15:30 Received: 02/27/03 14:05
ND
ND

Surrogate: 2,4-DCAA
D002, Bldg. 6000 (B302323-02) Waste (L)

- Reporting
Limit

3.32
3.54
143%

Sampled: 02/26/03 15:35
ND
N D

3.32
3.54

91.9%

mg/I
'

1
.

24-135

3C11018
.
"

"

H

S-04

Received: 02/27/03 14:05
mg/1
.

1
.

3C11018
.

03/11/03
.

03/13/03
.

EPA8151A

24-135

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This anafytical report must be reproduced in its entirety.

1380 Busch Parkway
Buffalo Grove, Illinois 60089
Tetra Tech EMI - IL
200 E. Randolph Suite 4700
Chicago IL, 60601

Email: info@glalabs.com
(847) 808-7766 FAX (847) 808-7772

Project: Kip Nelson
Project Number 505-0212-008
Project Manager: Lisa Graczyk

Reported:
03/18/03 13:52

Notes and Definitions
>220

>220 °F

G12

The reporting limits have been elevated due to low sample volume.

G13

The recovery of this analyte in the check standard is below the method specified acceptance criteria.

G23

The sample was diluted due to the presence of high concentrations of non-target analytes.

G6

This sample was extracted past the method specified holdtime.

QC

The result for one or more quality control measurements associated with this sample did not meet the laboratory and/or source
method acceptance criteria.

S-04

The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect

DET

Analyte DETECTED

:ND

Analyte NOT DETECTED at or above the reporting limit

MR

Not Reported

dry

Sample results reported on a dry weight basis

RPD

Relative Percent Difference

•

Great Lakes Analytical-Buffalo Grove Wisconsin DNR Certification Lab ID: 999917160
Great Lakes Analytical—Buffalo Grove NELAP Primary Accreditation: Illinois #100261
Great Lakes Analytical—Buffalo Grove NELAP Secondary Accreditation: New Jersey #IL001
Great Lakes Analytical-Oak Creek, WI Wisconsin DNR Certification Lab ID: 341000330

Great Lakes Analytical-Buffalo Grove
/ \ **~ «A-t.

«J e^^^^^-v^-^.

The results in this report appfy to the samples analyzed in accordance with the chain of
custody document. This anafytical report must be reproduced in its entirety.

A Subsidiary of Sommer-Frey Laboratories, Inc.
Great Lakes Analytical Laboratories
Attn: Andy Johnson

Received Date: 3/4/03

1380 Busch Parkway

Report Date: 3/5/03

Buffalo Grove, IL 60089

P.O. Number 1458

- Analytical Results
Lab#: 03A1326-001
Test
BTU Per Pound

Test
BTU Per Pound

Sample ID.

LOD
50

Sample ID:

LOQ Analysis Date
160
3/5/03

By
Method
HTM
D240

Flag
1

LOQ Analysis Date
160
3/5/03

By
Method
HTM
D240

Flag
1

LOQ Analysis Date
160
3/5/03

By
Method
HTM
D240

Flag
1

B302323-11

Result Units
16435 BTU/Lb

Lab#: 03A1326-003

FLAG
1

B302323-10

Result Units
18750 BTU/Lb

Lab#: 03A1326-002

Test
BTU Per Pound

Sample ID:

LOO
50

B302323-12

Result
Units
10810 BTU/Lb

LOD
50

Comment
All laboratory QC requirements were met for this sample

Gary G. Geipel „
Senior Analyst
6125 West National Avenue, P.O. Box 14513, Milwaukee, Wisconsin 53214
(414)^75-6700 » FAX: (414) 475-7216 ° www.sflabs.com
Toll-Free: (800) 300-6700
, n~_» „!

i , „(,„,..-+„„,

nonr n' Msmrai Po«;o! rrr<=<!

Certified Laboratory £241249360 «

APPENDIX C
REMOVAL COST MANAGEMENT SYSTEM
REMOVAL COST PROJECTION
(16 Sheets)

PROJECTION SUMMARY BY TASK REPORT

Page 1

KipNelsonERRS
Contract Number: 68-S5-9802

Prime Contractor: Earth Tech, Inc.
Start Date: 07/01/2003

End Date: 12/31/2003

Administrative
Total
Personnel

28,864.00

Equipment

2,520.00

Other Costs

630.00

Total

32,014.00

Demolition
Total
Personnel

0.00

Equipment

20,550.00

Other Costs

210.00

Total

20.760.00

Disposal
Total
Personnel

3,280.00

Equipment

7,230.00

Other Costs

10,500.00

Total

21,010.00

haz liquid
Total
Personnel

0.00

Equipment

0.00

Other Costs

22,837.50

Total

22,837.50

Personnel

8,100.00

Equipment

23,220.00

Other Costs

87,574.20

Total

118,894.20

Health & Safety
Total

Non-haz liquid
Total
Personnel

0.00

Equipment

0.00

Other Costs

3,675.00

Total

3,675.00

(

Prime Contractor:
Earth Tech, Inc.

KIPNELSONEKRS
'rejection Detail By Task Report

rage 1
Contract Number:
68-S5-9802

ADMINISTRATIVE
$32,014.00
PERSONNEL

$28,864.00
Quantity

Reg Mrs/Day

OT Mrs/Day

Days

Reg Rate

OT Rate

Total

1

8

2

82

32.00

48.00

28,864.00

RCMS#

Days

Total

Computer-Portable PC

Quantity
1

Daily Rate

07023020

Office-Equipped/8x40

02055043

1

15.00
20.00

72
72

1,440.00

Quantity

Cost

Total

3

200.00

630.00

Description
Field Cost Admin.
EQUIPMENT
Description

OTHER COSTS
Description

$2,520.00
1,080.00

$630.00

Phone

DEMOLITION
$20,760.00
PERSONNEL

$0.00
Quantity

Reg Hrs/Day

OT Hrs/Dav

Days

Reg Rate

OT Rate

Total

0

0

0

0.00

0.00

0.00

0.00

RCMS#

Quantity

Daily Rate

Days

Total

Cutting Torch
Drum-Crusher

07033010

Shears-Boom attachmnt/large

03070012

1

10.00
200.00
750.00

40
20
21

800.00

03027010

2
1

Description

EQUIPMENT
Description

OTHER COSTS
Description
Tools

$20,550.00

4,000.00
15,750.00

$210.00
Quantity
1

Cost

Total

200.00

210.00
DISPOSAL
$21,010.00

PERSONNEL
Description

$3,280.00
Quantity

Reg Hrs/Day

OT Hrs/Dav

1

8

0

Days
10

RCMS#

Quantity

Daily Rate

Days

Total

08001020

1

100.00

15

1,500.00

T&D Coordinator
EQUIPMENT
Description
Acid-2 inches

Reg Rate
41.00

$7,230.00

OT Rate

Total

0.00

3,280.00

OTHER FIELD COSTS DETAIL REPORT

Pace 1

KipNelsonERRS
Contract Number: 68-S5-9802

Prime Contractor: Earth Tech, Inc.
Total
Analysis
Bottled Water
Disposal
Electrical

10,500.00
945.00
120,487.50
630.00

Equipment

3,150.00

Fuel

6,615.00

Lodging
Materials/Supplies
PerDiem
Personal Protection
Phone
Shipping
Tools
Transportation
Totals

54,600.00
3,780.00
25,200.00
2,419.20
630.00
1,575.00
210.00
47,512.50
$278.254.20

- vr-'T:: •••: "*•

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^
S401
Chemist
S401
Chemist
Clean-Up Techniciar S203
Computer Operator S408
Construction Inspect} S308
Construction Inspect S308
S310
Electrician
S409
:ngmeer
S409
Engineer
S409
zngmeer
S409
Engineer
Engineer
S409
S409
Engineer
S409
Engineer
Engineer/Civil
S415
Engineer/Civil
S415
Engineer/Civil
S415
Engineer/Electrical S411
Engineer/Structural S412
Equipment Operator S205
Field Clerk/Typist
S210
Field Cost Admin
S213
Foreman
S110
S420
Geologist
S425
Hydrogeologist
Ind Hygienist/Safety S430
Laborer / Non 40 Hr S230
Program Manager S510
Project Manager
S130
Radiation Specialist S445
Response Manager S105
Response Manager S105
Response Manager S105
Response Manager S105
S450
Site Safety
T&D Coordinator
S520
S220
Truck Driver
>«&HW'*£*" '"**:

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Earth Tech, Inc.

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08001020
«J Air Blower-Portable / 300 CFM
07001010
Air Blower-Portable / 3000 CFM
07001012
-7 Analyzer-Hazcat System
04006035
i Attachment-Grappler Demolition
03000022
—
Attachment-Grappler Drum/Hydrau
03000026
_ Attachment-HoRam-Hydraulic
03000035
Backhoe-CASE 580
03001010
„ Backhoe-CASE 680L
03001020
Backhoe-Extendahoe
03001030
- Boat-14/16ft
07015020
Boat-21 ft
07015030
- Boat-26-30 tt
07015035
Boat-Motor > 50 HP
07015043
Boat-Motor >100 HP
07015045
Boat-Motor 10 to 50 HP
07015042
Boom
01001010
- Boom-Harbor 12-1 Sin Skirt
09005010
Boom-Harbor 6-1 2in Skirt
09005005
Box-1 ton
01003010
Box-2 ton
01003020
' Bulldozer-CASE 1550
03010040
Bulldozer-CASE 450/550
03010010
Bulldozer-CAT D8
03010060
Car-Passenger
01009010
Centrifugal-2 inch
08012020
Centrifugal-3 inch
08012030
Centrifugal-4 inch
08012040
Compactor-Cat 81 5
03015010
Compactor-CAT CS323C ROLLER VI 03015015
Compactor-CAT CS433C ROLLER VI 03015020
Compactor-Sheepsfoot Attach.
03015030
Compressor/ Air-> 200 CFM
07021020
Compressor / Air-185 CFM
07021010
Computer-CAD
07023025
Computer-Portable PC
07023020
Cutting Torch
07033010
Decon-8x25
02020020
Decon-With Showers 8x40
02020040
Decon-Without Showers 8X40
02020041
Diving-Hard Hat Shallow
07036010
Diving-Scuba
07036005
Double Diaphram-Teflon 2 inch
08018026
Double Diaphram-Teflon 3 inch
08018036
08018046
Double Diaphram-Teflon 4 inch
Drum-Crusher
03027010
Dump-Articulated
01015010
01015042
Dump-Fixed box 10/20 yds
03030040
Excavator-CASE 688
Excavator-CAT 225B LC
03030065
Excavator-CAT EL180/Long Reach
03030056
Excavator-Gradall/Wheeled
03030033
33035014
Forklift-Telescopic
Fume Hood-Vented
M049020
Generator-350 KW
37051060
Generator-5 KW
37051005
Generator-50 KW
37051040
Hose-Discharge / 2m
3705501 1
Hose-Discharge / 3in
(37055012
Hose-Discharge / 4in
(37055013

Earth Tech, Inc Disposal
Earth Tech, Inc
Earth Tech, Inc
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Earth Tech, Inc. Demolition
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Page: 1 of 3

100 OC3
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150.00
200.00
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100.00
20000
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0

0

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1500.00
000
0.00
480.00
000
4800.00
0.00
0.00
0.00
0.00
000
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

8100.00
0.00
000
0.00

8100.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

1080.00
800.00
0.00
0.00

6300.00
0.00

0.00
0.00
1500.00
0.00
4000.00
0.00
31500.00
0.00
000
0.00
0.00
18000.00
0.00
000
0.00
0.00
300.00
0.00
0.00

.

Z&i'jZtJi^rr >,>£ipNelscjnERRS - Equipment --, ;-

"

-'- •

j task' Code ff ^.i^itis M^&jrs <oQuaritiJ >
Hose-Fire 100 ft
07055021 Earth Tech, Inc
15.00
, Hose-Suction 2in
07055031 Earth Tech, Inc
500
Hose-Suction 3in
07055032 Earth Tech, Inc I
5.00
— Hose-Suction 4in
07055033 , Earth Tech, Inc
500|
Lighting-Conventional
07067010 , Earth Tech, Inc
5.00
" Lighting-Explosion Proof
07067020 Earth Tech, Inc
4000
Lighting-Light Plant
07067030 Earth Tech, Inc.
1 20.00 j
Loader/Track-CAT 943 1 .5 cyd
03055030 Earth Tech, Inc.
350.00
Loader/Track-CAT 973 3 cyd
03055060 Earth Tech, Inc.
soo.oo;
Loader/Wheel-CASE 721 2.5 cyd
03060040 Earth Tech, Inc
450.00
Loader/Wheel-CAT 950E 3 5 cyd
03060050 Earth Tech, Inc
500 OOi
Lowboy-20 ton
02045020 i Earth Tech, Inc.
75.00)
Lowboy-30 ton
02045030 Earth Tech, Inc.
100.001
Lowboy-50 ton
02045050 i Earth Tech, Inc.
120.00
Lowboy-9ton
02045010 Earth Tech, Inc.
5000
Meter/Monitor-Aerosol/Miniram
'05001040 Earth Tech, Inc.
50.00!
Meter/Monitor-Aersol/Ram
'05001041 , Earth Tech, Inc. j
150.00
Meter/Monitor-Alpha Meter
'05001032 ' Earth Tech, Inc.
40.00
Meter/Monitor-Beta Gamma Meter LU ; 05001 033 , Earth Tech, Inc.
40.00!
' ' '^r/Monitor-Explosion/Oxygen
,05001012 Earth Tech, Inc. Health & Safety
50.00
r/Monitor-HNu (PID)
105001020 ' Earth Tech, Inc.
70.00
- fflPfer/Monitor-OVA (FID)
05001025 Earth Tech, Inc. Health & Safety
1 25.00 j
Office-Equipped/8x40
i 02055043 , Earth Tech, Inc. Administrative
20.00
Oil-Oleophilic Recovery
< 07073020 Earth Tech, Inc.
0.00
Oil-Skimmer Heads
' 07073040 , Earth Tech, Inc.
30.00
Pickup-2 wheel drive
01036010 ' Earth Tech, Inc. Transportation
60.00
Pickup-4 wheel drive
01 036020 • Earth Tech, Inc.
70.00!
Pool-1 0,000 gallons
,06039030 Earth Tech, Inc.
100.00
Pool-20,000 gallons
06039045 ; Earth Tech, Inc.
100.00
Pool-50,000 gallons
i 06039050 ' Earth Tech, Inc.
300 00 1
PPE-Level A / Suit
05005040 Earth Tech, Inc.
150.00
PPE-Lvl B/SCBA/Low Pres
' 05005051 Earth Tech, Inc. Sampling
5.00 1
Radio-Handheld
05015010 • Earth Tech, Inc. i Health & Safety
5.00!
Radio-Portable Base
05015020 ' Earth Tech, Inc j Health & Safety
5.00
Response-Emergency
01039020 Earth Tech, Inc. i
100.00
Road Tractor
' 01 04201 0 Earth Tech, Inc
80.00!
Scales
07085010 Earth Tech, Inc.
75.00
'per
'03065020 Earth Tech, Inc.
700.00!
i^^er-Self Loader
,03065010 Earth Tech, Inc.
1100.00
750 00 1
Shears-Boom attachmnt/large
'03070012 'Earth Tech, Inc. Demolition
<
Shears-Boom attachmnt/small
,03070010 Earth Tech, Inc
10000
Skid Unit-Vacuum/1 500 gal
1 0206701 0 , Earth Tech, Inc.
150.001
200.00 1
Skimmer-Drum 1 0-20 bbls/hr
'; 0901 5005 Earth Tech, Inc.
Skimmer-Oleophillic 20-30
09015020 Earth Tech, Inc.
40.00 '
Skimmer-Rope (200 gal/hr)
109015010 Earth Tech, Inc
30.00
150.00'
Skimmer-Weir/Suction Skimpac
09015045 Earth Tech, Inc.
40.00
Skimmer-Wier/Suction 10-50
09015035 Earth Tech, Inc.
60.00!
Stakebed/Flatbed-1 ton
;01045010 'Earth Tech, Inc. ;
90.00
Stakebed/Flatbed-2 ton
,01045020 Earth Tech, Inc.
Steam Jenny
07090020 Earth Tech, Inc. I Disposal
80.00
:
2000
Storage-Approx. 20
ft.
02070010 Earth Tech, Inc. '
25.00
Storage-Approx. 40
ft.
02070020 Earth Tech, Inc.
40.00
Trash-2inch
08054010 Earth Tech, Inc
50.00
Trash-3 inch
08054015 Earth Tech, Inc.
Trash-4 <nch
08054020 Earth Tech Inc
80 00
Uni Loader-Barrel grappler atta
03095035 .Earth Tech, Inc. Transportation
50.00i
Uni Loader-Forks Attachment
03095025 Earth Tech, Inc. Transportation
25.00 '
Uni Loader-w/ bucket
'03095010 Earth Tech, Inc. 'Transportation
1 00.00 1
Vacuum-3800 gallons / Dump
01051038 Earth Tech, Inc. ,
120.001
Van-Passenger
01054030 Earth Tech, Inc.
75 00 i
Page: 2 of 3

0
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0
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0.00
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0.00
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0.00
0.00
000
360000
0.00
9000 00
1440.00
0.00
000
4920.00
000
0.00
0.00
0.00
0.00
450.00
2160.00
2160.00
0.00
0.00
0.00
0.00
0.00
15750.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
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1500.00
750.00
7200.00
0.00
0.00

1
0
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0
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0
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6
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1
1
0
0

Water Laser-LO-Pressure Single
Water Laser-MED-Pressure Single
Welder-Unit

'07096004
07096008
,07097010

Earth Tech, Inc
Earth Tech, Inc.
Earth Tech, Inc

2500J
4000
5000

Page. 3 of 3

°L

000
0.00
000

~j$jl&&$3$^£^v^*** '~x '-' .- ': KipNelsonERRS - dther Field Costs
t^i^^^^^2^i''*^"i"^ **

IVQuaritit; I '^ir
A-iafATS
- Jotal
Amouni
^' -iX i- *' ;.p !~ ..
v

Analysis
Bottled Water
Disposal
Disposal
Disposal
Electrical
Equipment
Fencing
Fuel
nventory
Lodging
Materials/Supplies
'erDiem
Personal Protection
Personnel
Phone
Repairs
Security
Shipping
T — |S

spoliation
'fWRsportation
Transportation

Earth Tech, Inc
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.
Earth Tech, Inc.

Disposal
Health & Safety
haz liquid
Non-haz liquid
Non-haz solids
Health & Safety
Operations
Equipment
Health & Safety
Health & Safety
Health & Safety
Health & Safety
Administrative

Sampling
Demolition
laz liquid
•Jon-haz liquid
vlon-haz solids

400.00
300.00
0.75
0.60
1860
200.00!
1000.00
0.00 1
1.75
000
6500!
50 00 1
3000J
32.00
O.OOl
200.00
0.00
0.00
150.00
200.00
0.12
0.10
8.35

25
3
25000
5000
5000
3
3
0
3600
0
800
72
800
72
0
3
0
0
10
1
25000
5000
5000

Page: 1 of 1

5
5
5
5
5
5
5,
5
5
5
5
5
5
5
5
51
5
5'
5
5
5'
5'
5

1050000
945.00
19687.50
3150.00
97650 00
630.00
3150.00
0.00
6615.00
0.00
54600.00
3780.00
25200.00
2419.20
0.00
630.00
0.00
0.00
1575.00
210.00
3150.00
525.00
43837.50

Disposal 43%

4% Analysis

7% Other
Lodging 20%

17% Transportation
PerDiem 9%

PROJECTION SUMMARY REPORT
Govt TetraTech EMI STARTS Kip Nelson
Prime Contractor: TetraTech EMI
STARTS

Contract Number: 68-W-00-129
.' End Date: 12/30/2003

Start Date: 07/01/2003

Total
Personnel

$119,682.25

Equipment

2,970.00

Other Costs

30,175.25
Total

Site Contingency
Indirect

15%
10%
Total With
Contingency and
Indirect

Comments:

$152.827.50
22,924.13
17,575.16

$193.326.79

PROJECTION SUMMARY BY TASK REPORT

Page 1

Govt TetraTech EMI STARTS Kip Nelson
Prime Contractor: TetraTech EMI
STARTS

Contract Number: 68-W-00-129
End Date: 12/30/2003

Start Date: 07/01/2003
Administrative
Total

Other Costs

59,632.40
0.00
0.00

Total

59,632.40

Personnel
Equipment

Health & Safety
Total
Personnel

37,142.72

Equipment

0.00

Other Costs

1,343.75

Total

38,486.47

Mobilization/Demob
Total
Personnel

0.00

Equipment

0.00

Other Costs

27,326.50

Total

27.326.50

Report
Total
Personnel

12,173.30

Equipment

0.00

Other Costs

0.00

Total

12.173.30

Sampling
Total
Personnel

10,733.83

Equipment

2,430.00

Other Costs

0.00

Total

13,163.83

Transportation
Total
Personnel

0.00

Equipment

540.00

Other Costs

1,505.00

Total

2.045.00

GOVT TETRATECH EMI STARTS KIH NELSON
""rejection Detail By Task Report
/

Prime Contractor:
TetraTech EMI STARTS

Kage 1
Contract Number:
68-W-00-129

ADMINISTRATIVE
$59,632.40
PERSONNEL
Description
START
EQUIPMENT
Description

OTHER COSTS
Description

$59,632.40
Quantity

Reg Hrs/Dav

OT Hrs/Dav

Days

Reg Rate

OT Rate

Total

1

8

2

100

6934

0 00

59,632 40

RCMS#

Quantity

Daily Rate

Days

Total

0

0 00

0

0 00

Quantity

Cost

Total

0

000

000

$0.00

$0.00

HEALTH & SAFETY
$38,486.47
PERSONNEL
Description

$37,142.72
Quantity

Reg Hrs/Dav

OT Hrs/Day

Days

Req Rate

OT. Rate

Total

1

8

2

82

56 62

000

37,14272

RCMS#

Quantity

Daily Rate

Days

Total

0

0 00

0

0 00

Quantity

Cost

Total

25

5000

1,34375

START
EQUIPMENT
Description

OTHER COSTS
Description

$0.00

$1,343.75

Materials/Supplies

MOBILIZATION/DEMOB
$27,326.50
PERSONNEL
Description

EQUIPMENT
Description

OTHER COSTS
Description
Fuel

$0.00
Quantity

Reg Hrs/Dav

OT Hrs/Day

Days

Reg Rate

OT Rate

Total

0

0

0

0 00

0 00

0 00

0 00

RCMS#

Quantity

Daily Rate

Days

Total

0

0 00

0

0 00

Quantity

Cost

Total

400

1 80

77400

$0.00

$27,326.50

OTHER FIELD COSTS DETAIL REPORT

Page 1

Govt TetraTech EMI STARTS Kip Nelson
Prime Contractor: TetraTech EMI

Contrac{ N(jmber 68.w.00.129

Total
Fuel
Lodging

774.00
18,167.50

Materials/Supplies

1,343.75

PerDiem

8,385.00

Transportation

1,505.00

Totals

$30,175.25

•»? V* *

\Qovt TetraTech EMI STARTS Kip Nelson - Other Field Costs
IllJtctor* , ,; .Task Code

'-

-

- -Cosl Quantity
1

1

G/A"/,

Analysis
TetraTech EMI STAIj
OOO
O
0
Bottled Water
TetraTech EMI STAfi
000
O1
0
Decon
TetraTech EMI STAll
ooo
ol
o
~ Disposal
TetraTech EMI STAIJ
000
0
0
Electrical
TetraTech EMI STAIJ
;
OOOi
0
0
TetraTech EMI STAIj
* Equipment
000
0
0
Fencing
TetraTech EMI STAll
OOOl
0'
0
Fuel
TetraTech EMI STAli Mobilization/Demj
1 so'
400i
75
Inventory
TetraTech EMI STA?
OOOI
0
0
Lodging
TetraTech EMI STAIJ Mobilization/Dem
65 00
260
75
Materials/Supplies TetraTech EMI STAIj Health & Safety
5000
25
75
PerDiem
TetraTech EMI STAIJ Mobilization/Demi
3000!
260'
75
Personal Protection TetraTech EMI STAli
000
0
0
Personnel
TetraTech EMI STAIJ
OOOI
0
0
Phone
TetraTech EMI STAI;
000
O1
0
Repairs
TetraTech EMI STAFi
OOOl
Ol
0
Security
TetraTech EMI STAIj
000
Ol
0
Shipping
TetraTech EMI STAI|
oooj
oj
o
Subctr/Consultant TetraTech EMI STAI
000
0
0
T
TetraTech EMI STAI
000
Oi
0
"L^portation
TetraTech EMI STAR Transportation
700 OO 1
2
75
TetraTech EMI STAfj
Travel
ooo
o!
o
Treatment
TetraTech EMI STAIJ
OOO!
ol
0
Utilities
| TetraTech EMI STAll
OOOt
01
0
^SaiSSIS^^^S^^^ftWf5^••5JMBM»Sl»H*tt.l'.lrf|^|^Myi|

Page 1 of 1

Total Amouni
000
000
000
000
000
000
000

77400
OOOJ
1816750
134375
8385 00
000
000

OOOI
000
000
000
000
000
150500
000
000
000

$30,17525

Page: 1 of 1

PROJECTION SUMMARY REPORT
KipNelsonERRS
Contract Number: 68-S5-9802

Prime Contractor: Earth Tech, Inc.

End Date: 12/31/2003

Start Date: 07/01/2003

Total
Personnel

$215,540.00

Equipment

139,140.00

Other Costs

278,254.20
Total

$632.934.20

Site Contingency

15 %

94,940.13

Indirect

10%

72,787.43

Total With
Contingency and
Indirect
Comments:

$800.661.76