Site Assessment Report for Frost Manufacturing Company

Report done by Ecology and Environment, Inc, for Environmental Protection Agency, in regards to site conditions and threats of human health and environment, at the Frost Manufacturing Company, in Kenosha, Wisconsin.

254394

1997-01-27 00:00:00.0

WID006090286

Frost Manufacturing Company

PDF

Ecology and Environment, Inc.

Site assessment

Administrative Record

text

Human health

Environment

Frost Manufacturing Company

Environmental reporting

Midwest

Environment, Inc. (E & E)

Environmental Protection Agency

City of Kenosha

2019-01-27

Environment, Inc. (E & E)

Environmental Protection Agency

City of Kenosha

Copyright undetermined

eng

Kenosha, Wisconsin

PDF

OOOC.O ",

EPA Region 5 Records Ctr.

254394

SITE ASSESSMENT REPORT
FOR
FROST MAlVfUFACTURING COMPANY
KENOSHA, KENOSHA COUNTY, WISCONSIN
TDD: S05-9606-022
PAN: 6N2201SI

^mmf

January 27, 1997

Prepared for:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Emergency and Enforcement Response Branch
77 West Jackson Boulevard
Chicago, Illinois 60604

"tu*

M. //rnJL,^^^

Prepared by:

Date: / - 2 7 - 9 >

dine. START Project Manager
Reviev.ed by: \ i \ ^ ^ r ) ' ^ ' - ?^.. c ' ^ - - ^
Lr. MJ Ripp. S T A ^ / A s s i s t ^ t PProgram Manager

Date: j J u h ^ L ^

Appnn^ed by:

Date: / / 6 ^ /^'^
Thomas Kouns. STAT^T Program Manaeer

• colony and environnjent, inc
intpr-nationai Specialists m the Environmerit

\ 3

33 North Dearborn Street. Chicago, Illinois 60602
Tel 312/578-9243. Fax: 312/578-9345

Table of Contents

Section

1
2

3
4
5
6

Page

Introduction
Background
2.1 Site Description
2.2 Site History
Site Assessment
Analytical Results
Discussion of Potential Threats
Proposed Removal Actions

Appendix
A
B
C

Photodocumentation
Analytical Results
Cost Estimates

1-1
2-1
2-1
2-2
3-1
4-1
5-1
6-1
Page
A-1
B-1
C-1

List of Figures

Figure
2-1
2-2
3-1

Page
Site Location Map
Site Features Map
Sample Location Map

2-6
2-7
3-3

ni

List of Tables

Table
4-1
4-2
4-3
4-4

Page
Cyanide, pH, and Total Metals Analytical Results
TCLP Metals Analytical Results
Volatile Organic Compounds Analytical Results
Semivolatile Organic Compounds Analytical Results

IV

4-2
4-3
4-4
4-5

1. Introduction

The United States Environmental Protection Agency (U.S. EPA) has tasked the Superfund
Technical Assessment and Response Team (START) contractor Ecology and Environment, Inc.
(E & E), under Technical Direction Document (TDD) S05-9606-022 to assess site conditions and
threats to human health and the environment at the Frost Manufacturing Company (FMC) site, located
in Kenosha, Kenosha County, Wisconsin.

1-1

2. Background

2.1 Site Description
The FMC site is located at the southeast corner of the intersection of 14th Avenue and 65th
Street, 6523 14th Avenue, in Kenosha, Kenosha County, Wisconsin. The geographic coordinates of
the site are: latitude 42°34'29.1"N; longitude 87°49'36.4"W (Figure 2-1). The site is comprised of
4.75 acres of land, with an adjacent 0.41 acres used for parking. Currently, the site is an inactive
plumbing supply manufacturer.
The site is comprised of the brass foundry building, located on the northwest portion of the
site; the main plant building where the plating operations and production processes occurred, located
south of the foundry building; four underground storage tanks (USTs) for fuel oil, three located in the
alley east of the main plant and one located south of the brass foundry building; a carport located
between the brass foundry building and the main plant building; and three storage sheds and a garage,
located east of the main plant building and west of the Union Pacific Railroad (UPRR) (formerly the
Chicago and Northwestern Railroad).

The brass foundry building is in good condition and all

equipment has been removed from the building, leaving several pits. The brass foundry building
consisted of six main areas: a core department, a grinding department, a mold department, a link belt
shakeout, a melt department, and a boiler room (Figure 2-2).
The main plant building was constructed of brick, with the exception of the steel warehouse
addition on the southern end of the building. The new addition contained a warehouse area, the
wastewater pretreatment system, the treatment area, product storage, and loading docks. The
northern part of the main plant building contained the production process area and offices. The
production process area consisted of an annealing furnace, metal drawing machines, a plating area, an
eiectropolish and stripping area, and a buffing process area. The roof in several areas of the older
parts of the main plant building leaked during precipitation events. Pieces of ceiling insulation from
several areas of the older parts of the main plant building had fallen to the floor.

2-1

Three sheds and a garage were located along the eastern side of the site. The southernmost
shed is constructed of wood. The next two sheds to the north were constructed of steel and concrete.
The sheds were used to store old equipment and had some equipment, parts, and miscellaneous
containers. All sheds were in fair condition. The garage was located to the north of the sheds and is
constructed of concrete block. The garage was used to store foundry material and was empty, except
for a dismantled engine (Figure 2-2).
The site is bordered by the UPRR line to the east, 14th Avenue to the west, 65th Street to the
north, and Becker Inc., property to the south. The site topography is relatively flat. The site is
located in a residential/heavy industrial area. The population of Kenosha is 80,352 persons according
to the 1990 U.S. Census. The City of Kenosha relies on Lake Michigan for its water supply. The
Wisconsin Department of Natural Resources (WDNR) records indicate that there are no water supply
wells on the site. There are no known potable water supplies in the area.

2.2 Site History

The FMC site has been in use since 1902, as a manufacturer of plumbing supplies, primarily
copper tubing. The company operating the facility was incorporated in the State of Wisconsin
November 3, 1902, as F.P. Incorporated, and administratively dissolved June 18, 1996. The last
annual report filed by the company was for 1993.
The brass foundry building was used by the City of Kenosha as the City garage and repair
shop from 1941 through 1955. It is not known what the building was used for prior to 1941. FMC's
brass foundry building was in use from 1956 until 1991, for the manufacture of leaded brass parts.
In September 1991, the leaded brass foundry ceased operations. WDNR records indicate that
approximately 1,120 cubic yards of foundry sand were generated at the site between 1986 and 1991.
The remainder of the main facility (plating) has been inactive since 1994. FMC manufactured
copper tubing, chrome-plated plumbing trim, swimming pool deck equipment, and leaded-brass
castings. In 1987, a wastewater pretreatment system was completed to meet federal pretreatment
standards for metal finishing under the Code of Federal Regulations (CFR) 443.
Products manufactured at the FMC site consisted of plumbing fittings and fixtures, brass
goods, specialized plumbing fittings, heat exchanger fittings, and swimming pool components. In
1980, FMC manufactured 550,000 square feet per year (sq ft/yr) chrome plating; 700 sq ft/yr hard
chrome plating; 440,000 sq ft/yr electropolishing; 50,000 sq ft/yr bright dipping; 550,000 sq ft/yr
2-2

nickel plating; and 550,000 sq ft/yr copper plating. The processes employed in the manufacturing of
these products included chrome plating, hard chrome plating, electropolishing, bright dipping, nickel
plating, and copper plating. Raw materials used in the manufacturing of these products were: brass
tube, sheet brass, brass ingot, copper tube, stainless steel tube, and stainless steel sheet. Chemicals
utilized in the manufacturing processes included: sulfuric acid, hydrochloric acid, nitric acid,
phosphoric and sulfuric acid (Batelle #2067), potassium cyanide, chromic acid, nickel chloride, nickel
sulfate, boric acid, and prepared cleaners (Oxy-prep #176, #157, #274, #293; Udylite).
The facility was a large quantity generator of hazardous wastes regulated under the Resource
Conservation and Recovery Act (RCRA) and notified the U.S. EPA on May 4, 1981. The U.S. EPA
hazardous waste generator identification number for FMC was WID006090286. Hazardous wastes
generated on site were foundry sand and buffing dusts; which are considered D008 lead from the
leaded-brass foundry, and F006 wastewater treatment sludges from electroplating operations. Other
generated hazardous waste included spent solvents.
A large quantity generator inspection was conducted by WDNR on September 24, 1984, at
the facility.

On October 16, 1984, FMC received a Notice of Noncompliance. Deficiencies

included failure to mark containers with accumulation start dates, waste manifests without facility
identification number, lack of weekly inspection of containers for leaks and defects, no written
Contingency Plan and emergency procedures, and no program to train employees in the handling of
hazardous wastes and emergencies.
On February 13, 1985, WDNR representatives met with the FMC officials to discuss progress
on the Notice of Noncompliance. WDNR requested a plant layout figure be added to the
Contingency Plan and that the employee training program still needed to be implemented. On April
11, 1985, WDNR submitted a letter notifying FMC that all required corrections had been made and
the company was in compliance.
On October 31, 1988, a large quantity generator inspection of the FMC facility was conducted
by WDNR. FMC received a Notice of Noncompliance. On December 13, 1988, WDNR notified
FMC that the required corrections were made and the facility was in compliance.
On September 28, 1993, a large quantity generator inspection of the FMC facility was
conducted by WDNR. As a result of the inspection, FMC received several Notices of
Noncompliance.

2-3

On October 6, 1993, WDNR conducted a second inspection to collect samples of the foundry
sand. WDNR collected two samples of the foundry sand; the first sample was collected near the
south blowmatic molder, and the second sample was collected near the eastern end of the building by
the shaker area. Both samples were analyzed by the Wisconsin State Laboratory of Hygiene for
Toxicity Characteristic Leaching Procedure (TCLP) lead. Both sample results were 37 micrograms
per liter (^g/L) TCLP lead. The samples were split with FMC. FMC had their samples analyzed for
TCLP lead by CBC Environmental Laboratories (CBC) of Oak Creek, Wisconsin. The CBC
analytical result for the shakeout area was 37 ;ng/L and the south blowmatic molder sample result was
28 /ig/L.

The analyses confirmed that the waste foundry sand is a hazardous waste (D008), due to

TCLP lead results greater than 5 /^g/L. FMC estimated that approximately 20 cubic yards of waste
foundry sand was present in the foundry building. The foundry sand was removed during closure
activities of the foundry building.
To comply with the WDNR closure performance standards, S.NR685.05 (1), May 1994,
FMC contracted the services of Sigma Environmental Services, Inc. (Sigma), to prepare a Closure
Plan for the brass foundry building. The Closure Plan for the brass foundry building was completed
during September of 1994. WDNR approved the Closure Plan of the brass foundry building on
February 2, 1995. During closure activities of the foundry building, 15 cubic yards of D008
hazardous wastes were collected and shipped to the Chemical Waste Management stabilization facility
located in Menomonee Falls, Wisconsin.
The plating facility has been inactive since late 1994. According to a former FMC employee
interviewed by WDNR, Mr. Lanctote, the automatic plating line was installed in 1957, replacing an
older manual plating system. Waste from plating tank clean-out was sent with used drums (1" depth
of waste in each drum) for disposal, and the wastewater went through a pretreatment system prior to
discharge to the sanitary sewer. In December of 1985, FMC discontinued the use of cyanide in the
plating operations. Mr. Lanctote confirmed the locations of the plating, plating chemical storage,
polishing, press machine and maintenance, pipe bending, inspection, warehouse, and wastewater
pretreatment system areas.
As of June 30, 1996, FMC owed the County of Kenosha $190,557 in back property taxes.
The City and County of Kenosha, in cooperation with WDNR, have selected the FMC site as part of
the WDNR Brownfields Environmental Assessment Pilot (BEAP) program. The BEAR program goal
for FMC is to investigate the potential contamination and help bring the property back into productive
commercial or industrial use, or to develop the property into a multi-use area.
2-4

On May 16, 1996, the Kenosha Fire Department responded to a fire at the FMC facility.
Vandals had set fire to the office area of the main plant building. The offices were extensively
damaged by the fire.
On May 20, 1996, representatives from the Wisconsin Division of Health (WDH), Bureau of
Public Health, WDNR, Kenosha County Health Department, and the City of Kenosha visited the
FMC site to determine possible health threats posed by the abandoned facility in a residential
neighborhood. WDH observed evidence of people trespassing by climbing the fence on the eastern
side north shed by the railroad and/or by climbing through an open shed window. Trespassers
entered the main plant by using a swimming pool ladder to access the plant roof, and another pool
ladder from the roof to access an open area in the plant.
Chemical hazards were also observed by WDH at the FMC site. In several areas in the main
plant, greenish powdered chemicals had been spilled. Barrels of what appeared to be plating waste
had been tipped onto the floor. In another room, vandals had opened a valve on an oil tank, which
created a slippery oil-covered floor. A number of barrels with unknown contents were observed
throughout the buildings. The plating area had plastic coverings over areas where plating operations
occurred.
Physical hazards were noted by WDH at the FMC site. The foundry building contained
several pits with dimensions of 4 feet wide and 4 feet deep. The main plant contains several sumps
with standing water. In the plating area there were sumps containing standing liquids.
Inlialation exposure is an issue at the FMC site. Air quality problems may occur from the
spilled plating wastes. Personnel in the WDNR investigation group noted an odor of sulfuric acid. A
recent fire in the office area left the odor of smoke. No odors were noted outside of the buildings.
Ingestion exposure is also a potential concern. The threat of trespassers coming into contact
with contaminants and unknowingly ingesting the contaminants could be a problem.
On June 17, 1996, WDNR requested that the U.S. EPA Region 5 Emergency Response
Branch conduct a removal assessment for a time-critical removal action at the FMC site. A joint site
reconnaissance was conducted on July 2, 1996, by U.S. EPA On-Scene Coordinator (OSC) Rey
Rivera and WDNR representative John Burnett.

2-5

Quadrangle Location

ecology and environment, inc.
Region 5 - Superfund Technical Assessment and Response Team
33 North Dearborn, Chicago, Illinois 60602
FIGURE *

Site Location Map

2-1

Frost Manufacturing Company

1:24,000

CITY

Kenosha
Wisconsin
SOURCE u.S.G.S. Topographic Map, 7.5' Series
Kenosha. Wisconsin Quadrangle
2-6

REVISED

S05-9606-022
1958

12IL

2-7

3. Site Assessment

START member John Nordine and U.S. EPA OSC Rey Rivera mobilized to the FMC site on
July 24, 1996, to conduct a site assessment. Keith Lesniak of U.S. EPA, John Burnett from WDNR,
and Sharon Krewson from the City of Kenosha, participated in the site assessment. The site
assessment included the collection of nine samples (four liquid and five solid), air monitoring, and
photodocumentation. The weather was partly cloudy, 80° F, and the wind was from the northwest at
10 miles per hour. The weather changed to rain in the afternoon.
A site safety meeting was conducted and hazards associated with the FMC site were
discussed. A site reconnaissance was conducted to observe site conditions and determine sample
locations (Figure 3-1). During this site reconnaissance, site features were photographed (Appendix
A). Air monitoring was conducted using a 10.2 eV HNU photoionization detector (PID) for
screening organic vapors. Organic vapor readings monitored throughout the site with the HNU were
either below or at the background level of 1 part per million (ppm). Sampling activities were
conducted in Level B protective equipment.
During the reconnaissance, nine sample locations were marked and numerous observations
were made. Two transformer areas were located on the east side of the main plant. All utilities at
the FMC site had been turned off by the City of Kenosha. Four USTs were located by their stand
pipes, three in the alley east of the main plant and one south of the brass foundry building.
According to WDNR file information, one UST capacity was 20,000 gallons, two were 8,000
gallons, and one was of unknown capacity.
Several areas of the FMC site showed signs of vandalism. The lock on the foundry building
door had been pried off. Windows were broken in all of the buildings. In the alley behind the main
building, several 55-gallon drums had been tipped over, releasing their contents to a storm drain.
Most of the sheds showed signs of vandalism; anything left in the sheds had been thrown to the
ground. In the boiler room, vandals had opened several 55-gallon drums of "Benzene Oil", which
released the oil onto the floor and into a floor drain. A yellow powder had been spilled on the floor
3-1

by the entrance to the plating area. In a room near the annealing furnace, two white poly 55-gallon
drums had been tipped over; the first drum contained a bright green liquid and solid with a pH of 0
standard units (S.U.). The remaining drum contained a grey semi-solid material. Vandals had set
fire to the office area of the plant.
Equipment used for sampling activities included trowels and disposable bailers and spoons.
All equipment was decontaminated prior to use. Equipment was scrubbed with a solution of Alconox
and rinsed with distilled water. The equipment was thoroughly rinsed with distilled water and air
dried. Site entry equipment did not indicate any readings above background levels during the
collection of environmental samples.
Samples designated by "V" were collected from sumps; samples designated by "S" were
collected from solids; samples designated by "D" were collected from 55-gallon drums; and the
sample designated by "A" was suspected of containing asbestos. Sample VI was a liquid collected a
sump located in the new water treatment area. Three samples, V2, SI, and S2, were collected from
the plating area; sump Sample V2 was collected from liquid in the plating room sump, solid Sample
SI was collected from a yellow powder spilled on the plating rooin floor, and Sample S2 was
collected from green solids near the floor grating system in the plating room. Samples S3, S4, Dl,
and D2 were collected from a room where thirty 55-gallon drums were stored; Sample S3 was
collected from a green solid spilled from an overturned white 55-gallon poly drum; Sample S4 was
collected from a grey semi-solid white material spilled from an overturned white 55-gallon poly drum;
Sample Dl was collected from a dark green liquid in an 55-gallon poly drum, with a field pH test of
0; and Sample D2 was a black liquid collected from a 55-gallon poly drum, with a field pH test of 10
to 11. Asbestos Sample Al was collected from pieces of tile that had fallen from the ceiling near the
annealing furnace.
All on-site activities concluded after the completion of sampling activities. The samples were
picked up by a courier from VOC Analytical, who delivered the samples to the laboratory, VOC
Analytical, of Naperville, Illinois. An Office of Solid Waste and Emergency Response QA level II
data package was requested under analytical TDD S05-9607-807.
Analytical results were received on August 9, 1996. All of the samples were analyzed for
total RCRA metal and TCLP metals concentration. Samples SI, S2, S3, Dl, and D2 were analyzed
for pH; Sample S4 was analyzed for cyanide; Samples VI and V2 were analyzed for volatile organic
compounds; and Samples VI, V2, S4, Dl, and D2 were analyzed for semivolatile organic
compounds.
3-2

65lh Street

Gate

I
I

Brass foundry
Shed]

,

1—1
Garage

Carport

Machine shop

_r
Recieving

<

Gate

30 Drums

•3

^

Storage

Alleyway

Pipe bending

oo
Office

1^

UST's

19 Drums O O O
- - - - r
Boiler

\
3 <
S >

Finished stock
storage and
packing

17 Drums

idder to roof

• |

3

•

H:

I

Q9.

Press room
Barrel
washing

19 Dliums
1

Shed
Dregreasing

Plating area
Yellow powder spill

,
(^
2 Drums
Shed

irransformeri
Polishing i

Sump

>

D
33 DwHjis___Lad<ler
to| roof

O O lo.U

Storage

Inspection

I I
gallon
Baghouse

Old water treatment area
Loading dock

O Acid tanks

Shed
5 Drums
15 Drums

New water treatment building

oo
15,|X)0
gallon

Warehouse
Sump
Gate

South parking area

Legend
— VI
•

-

Dl

Drum Sample

•X- SI

Solid Sample

A

Asbestos Sample

A1
-

-

O O

Sump Sample

O

ecology and environment, inc.
Superfiind Technical Assessment and Response Team
33 North Dearborn, Suite 900, Chicago, Illinois 60602
nCUREf

Sample Location Map

3-1
SCALE

Frost Manufacturing Company

Not to Scale

Defmed Area
Fence
Drums

1

Gate

TTID

Kenosha

Wisconsin

Ecology and Environment, Inc.

3-3

S05-9606-022
September 26, 1996

4. ANALYTICAL RESULTS

The sample results are presented in Tables 4-1, 4-2, 4-3, and 4-4. The TCLP chromium
concentrations detected in Samples S3 and Dl exceeded the regulatory requirements of 5 milligrams
per liter (mg/L). Samples S2, S3, and Dl exhibit the characteristic of corrosivity, with a pH below
2. The validated QA/QC analytical package is included in Appendix B.

4-1

Table 4-1
CYANIDE, pH, and TOTAL METALS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
Parameter
Sample
Identification

Cyanide
(mg/kg)

pH
(S.U.)

Arsenic
(mg/kg)

Barium
(mg/kg)

Cadmium
(mg/kg)

Chromium
(mg/kg)

Lead
(mg/kg)

Mercury
(mg/kg)

Selenium
(mg/kg)

Silver
(mg/kg)

SI

NA

4.5

13

270

3.8

1,600

700

BDL

BDL

1.4

S2

NA

1.0

14

49

BDL

3,500

130

BDL

BDL

BDL

S3

NA

0.0

46

1.5

BDL

6,900

50

0.18

BDL

1.3

S4

BDL

NA

15

43

BDL

4,000

950

BDL

BDL

BDL

Dl

NA

0.0

BDL

BDL

BDL

9,000

BDL

BDL

BDL

BDL

D2

NA

8.0

BDL

0.24

BDL

19

1.2

0.0041

BDL

BDL

Key:
NA = Not analyzed.
BDL = Below detection limit.
mg/kg = Milligrams per kilogram.
S.U. — Standard units.

Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9606-022.

Table 4-2
TCLP METALS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
Parameter

Sample Identification

Chromium
(mg/L)

Lead
(mg/L)

SI

0.35

BDL

S2

0.60

NA

S3

400

NA

S4

BDL

BDL

Dl

9,000

NA

D2

NA

NA

Key:
NA = Not analyzed.
BDL = Below detection limit.
mg/L = Milligrams per liter.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9606-022.

4-3

Table 4-3
VOLATILE ORGANIC COMPOUNDS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
(units = Mg/kg)
Sample Identification
Parameter

VI

V2

2-Butanone

0.13

BDL

Chloroform

0.0060

BDL

4-Methyl-2-pentanone

0.080

BDL

Toluene

0.080

BDL

Styrene

0.0090

BDL

Key:
Mg/kg = Micrograms per kilogram.
BDL = Below detection limit.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9606-022.

4-4

Table 4-4
SEMIVOLATILE ORGANIC COMPOUNDS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
(units = liglkg)
Sample Identification
Parameter
bis(2-Ethylhexyl)plnhalate
di-n-Octyl phthalate

VI

V2

S4

Dl

D2

2,300

BDL

4.5

130

BDL

240

BDL

BDL

BDL

BDL

Key:
/xg/kg = Micrograms per kilogram.
BDL = Below detection limit.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9696-022.

4-5

5. DISCUSSION OF POTENTIAL THREATS

Conditions present at the FMC site that warrant an appropriate removal action as set forth in
paragraph (b) (2) of Section 300.415 of the National Oil and Hazardous Substances Contingency Plan
(NCP) are:

Actual or potential exposure to nearby human populations, animals, or the food
chain from hazardous substances or pollutants or contaminants. The FMC site is
located in an industrial and residential area. The industrial buildings are surrounded
by a chain-link fence; however, this is not sufficient to prevent access by children,
animals, and vandals. Elevated concentrations of TCLP chromium were detected in
Samples S3 and Dl at 400 and 9,000 mg/L, respectively. Chromium is a cumulative
toxicant, and the human exposure conditions of most concern are long-term exposure
to elevated levels in the diet. Samples S2, S3, and Dl, which had pH levels of 1.0,
0.0, and 0.0, respectively, exhibit the characteristic of corrosivity as defined by
paragraph (a)(1) of 40 CFR Section 261.21 of the NCP; it is aqueous and has a pH of
less than or equal to 2 or greater than or equal to 12.5; or paragraph (2), a solid
waste that exhibits the characteristic of corrosivity has the EPA Hazardous Waste
Number of D002.
Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or
other bulk storage containers, that may pose a threat of release. Samples
collected during the site assessment indicate that hazardous materials are present on
site. Approximately eighty-four 55-gallon drums, two 30-gallon drums, fourteen 5gallon buckets, three 1-gallon pails, and 11 sumps were found on site. Sample
results of some of the drum and vat contents indicate the presence of plating wastes.
Several open 55-gallon drums of flammable liquids, acids, and unknown contents
were observed in the main plant building and in some of the sheds on site. The
drums pose a potential threat of release. There are three USTs located in the alley
east of the main plant building and one UST located south of the brass foundry
building that were used for fuel oil storage.
The UST capacities are two at 8,000 gallons, one at 28,000 gallons, and one
tank of unknown volume. The tanks were not sampled during the assessment.

5-1

•

Weather conditions that may cause hazardous substances or pollutants or
contaminants to migrate or be released. The roof of the facility leaks during
precipitation events; therefore, the possibility exists that sumps, pits, and drums that
were open could overflow due to events of heavy precipitation. Freezing
temperatures during winter months may cause a rupture of containers at the site,
resulting in a release.

•

The threat of fire or explosion. The office area of FMC was set on fire by vandals
on May 16, 1996. Should another fire occur, the potential for a rupture of an on-site
drum or container exists. The resulting release would pose health risks to nearby
residents.

•

The unavailability of other appropriate Federal or State response mechanisms to
respond to the release. This factor supports the proposed actions at FMC because
WDNR or local officials do not have the necessary resources to respond to an
emergency situation.
Based on the analytical results and site conditions, mitigative actions are necessary at the

FMC site to abate potential and imminent threats to human health and the environment posed by
hazardous conditions present at the site.

5-2

6. PROPOSED REMOVAL ACTIONS

The preferred removal action to mitigate threats associated with the FMC site consists of offsite treatment and disposal of liquid and solid wastes, and disposal of nonhazardous solid wastes at a
landfill. The removal actions described in this report directly address actual or threatened releases of
hazardous substances, pollutants, or contaminants at the facility which may pose an imminent and
substantial endangerment to public health and safety, and to the environment. The removal action at
the FMC site would include consolidating and staging debris; conducting sampling and compatibility
testing on all drums, tanks, pits, sumps, and miscellaneous containers; conducting bulk testing;
bulking all large wastestreams; preparing composite samples and submitting the samples for disposal
bids; transporting waste off site to disposal facilities; conducting soil and concrete sampling; and
excavation and disposal of contaminated soil and concrete, if necessary. An estimate for conducting a
removal action at the FMC site totalling $1,020,507 was prepared using the Removal Cost
Management System (RCMS) Cost Projection Module, version 4.2 (Appendix C). The following
assumptions were made when preparing the estimate:

The project will be conducted in phases, the first of which will include preparation of
a site safety plan, mobilization of personnel and equipment, container sampling,
compatibility and bulk testing, waste consolidation, disposal bidding, and a concrete
and soil extent of contamination (EOC) study. This phase is expected to take
approximately 60 working days. The second phase will include excavation of any
contaminated soil and concrete, and transportation and disposal of all wastestreams.
A total of 30 working days will be required for this phase.
The Emergency Response Cleanup Services (ERCS) contractor rates will be used for
cleanup contractor personnel and equipment costs.
ERCS contractor personnel will consist of one response manager, one
foreman/equipment operator, one field clerk, and five laborers. The START
contractor will include one geologist. One U.S. EPA OSC will be on site at all times.

6-1

Wastestreams will include acidic liquids; base/neutral liquids; debris, including
concrete (contaminated and noncontaminated); combustible liquids; and RCRA-empty
containers.
Volumes for liquid wastes were based upon a worst-case scenario, assuming all tanks,
drums, and pits were full.
All plating waste will be shipped to disposal facilities for treatment. The mixed acids
wastestream (9,500 gallons) will be shipped in bulk to Clean Harbors in Cincinnati,
Ohio, at a unit cost of $0.65 per gallon and a transportation charge of $1,500 per load
(2 loads). Base/neutral liquids (2,000 gallons) will be shipped in bulk to Heritage in
Indianapolis, Indiana, at a unit cost of $0.75 per gallon, and a transportation cost of
$1,300 per load (1 load). Combustible liquids (76,000 gallons) will be shipped in
bulk to Heritage in Lemont, Illinois, at a unit cost of $0.60 per gallon, and a
transportation cost of $500 per load (15 loads).
Concrete and soil volumes were estimated using the plating area of the building
(30,000 square feet) with an excavation depth of 6 inches. An additional 25%
contingency was added to account for soil contamination beneath the concrete. Based
upon file information, this cost estimate assumes that contaminated soil contains
chromium and lead, which would require treatment prior to landfilling. It is assumed
that the concrete and soil will be transported to the Chemical Waste Management
(CWM) Adams Center Landfill for treatment and disposal at a cost of $100 per cubic
yard and $1,500 per load for transportation.
Nonhazardous debris and RCRA-empty drums is assumed to be a special waste. A
total volume of 60 cubic yards was assumed to be transported to a permitted local
landfill at a cost of $20 per cubic yard and a transportation cost of $200 per load.

6-2

Appendix A

Photodocumentation

A-1

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sign on building face "Frost Co. Founded 1902."

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: North gate of Frost Manufacturing Company. Note the gate is locked, but still accessible.

L

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: North side of the brass foundry building along 66th Street.
iQ^DCDCZ^ C 3 '

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The west front of the brass foundry building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the west side of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the loading dock area of the main plant building

L

^g/ggumg^tiigtmmm^mmmmmmm

^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southeast
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the southwest end of the main plant building.

^

••H

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The south gate was located along 14th Avenue. Note that access is possible even with the
gate locked.

J

^
|i»w I

iw

0i'

«g

r*

^ r

'M0

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Northeast
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The southeast end of the brass foundry building.

:M

*

P
tx

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The north gate was located on 14th Avenue.

^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the fence along 14th Avenue.

}.
Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southeast
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the second gate along 14th Avenue.

'C^sass^i

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The parking area south of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity BSmm Photographer: J. Nordine
Subject: The southeast gate to the alley was open at the time of the site assessment.

«|e-^'^5

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35inm Photographer: J. Nordine
Subject: A view of the alley to the north.

IN H
JJMVn

^

1

1

m
Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Three 55-gallon drums that have been tipped over in the alley on the east side of the main
plant building. The drums spilled an oily liquid onto the concrete and into a drain in the alley. Note
the large electrical transformers in background.

'1

'T.!
IH.^ i l l

. 1

t

*B.-

I
7-^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
|
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: 3,000-gallon vertical tank labeled "acid" located on the east side of the main plant building.
«HA»

rfm^

alwi^M » mJt^mtm^mm'

IPI
1
\

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: 2,500-gallon horizontal tank labeled "acid" located on the east side of the main plant
building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The pool ladder used to gain access to the roof of the main plant building.

11* '-^ ^ ^ n ^SB 9 t & '

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: A second pool ladder used to gain access to the roof of the main plant building.

Ill
/ ,»

rf-

•'-,{'•} , ' y f \ M ^ ' ^ - V

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Two large transformers located on the east side of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Eighteen 55-gallon drums of unknown contents located in a shed east of the main plant
building.

p
,i

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The north side of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Unknown
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Thirty 55-gallon drums located in the main plant. Three of the drums had been tipped over
by vandals, spilling the drums' contents.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Seventeen 55-gallon drums and four 5-gallon pails located in the old water treatment area of
the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Unknown
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: 55-gallon drum labeled "Protopet White No. IS, White Petroleum USP Case# 8009-03-8.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Unknown
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: One of several pits filled with unknown liquids in the main plant.

r

dBHHtfflilii
Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Friable material fallen from the ceiling located near the annealing furnace. Sample Al was
collected from this material.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Up
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Friable ceiling material located above the annealing furnace.

"'TsJfiui—^ * » • * ! -

••
*

J

g.«j/ j & f f « w ^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the south side of the plating area.

I?

Bm
Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the north side of the plating area.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the northeast side of the plating area.

• 1i s

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Northwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: White substance that was spilled on the plating room floor.

^HHSSS m^^g

1

ppRMiiiiiiiiiiiqiiqq

^

^R
1• <
Wr 3
^ F Ml

•V/

'

1

i^

^T

^K^I^^^BLV

^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Bright green liquid spilled from piping in the plating room.
(E3D QiD CSS> <S& C 9 fSEi S S - ^ 9 OS) € S QEO <SSi ^S> 4E> (SS) ^E> ' ^ i ^ ^ ^ ^ (

<4il

! i '

'<-

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Down
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sump located in the plating room. Sample V2 was collected from the liquid in the sump.

^ '

ilBBBBBBfeaigt

.t.^t-»t-!;!

aesis

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample SI collected from a yellow powder that had been spilled near the plating room.

\fK

'•^m-

Site: Frost Manufacturing Company Date: 7-24-96 Direction: —
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample S2 was colllected fiom plating solids from the raceways in the plating room.
I c - J t " ^ " i C ^ ^ ^J-r- * C S b ) ^--—^ f -LSi

^ ^ ^ • V ' ''^:

't?^ ' % •

Site: Frost Manufacturing Company Date: 7-24-96 Direction: —
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample S4 was collected from solids that spilled from a drum.

ik

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample Dl was collected from a liquid in this drum.

B I I

•vV^

•

-:u)i(K^

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample D2 was collected from a liquid from this drum.

Appendix B
Analytical Results

B-1

ecology and eevlroHiMBenntlg niiic<
International Specialists in the Environment
33 North Dearborn Street
Chicago, Illinois 60602

Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 11, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Inorganic Data Quality Review for Toxicity
Characteristic Leaching Procedure (TCLP) Chromium and
Lead, Frost Manufacturing, Kenosha, Kenosha County,
Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD ,S05-9607-807
Analytical PAN-6UAG01TA

The data quality assurance (QA) review of four solid samples
collected from the Frost Manufacturing site is,complete. The
samples were collected on July 24, 1996, by ,the Superfund
Technical Assessment and Response Team (START) contractor.
Ecology and Environment, Inc. (E & E ) . The samples were
submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846
Methods 1311 and 6010.
Sample Identification
START
Identification No.
SI
S2
S3
S4

recycled paper

Laboratory
Identification No.
L9328-1
L9328-2
L9328-3
L9328-4

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
TCLP Chromium, Lead
Page 2
Data Qualifications:
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, and analyzed
on August 16, 1996. This is within the 6-month holding
time limit.
II.

Calibration;
Initial Calibration;

Acceptable

Recoveries for the initial calibration verification were
within 90 to 110%, as required.
Continuing Calibration;

Acceptable

All analytes included in the continuing calibration
verification standard were within 90 to 110%, as required.
III.

Blanks;

Acceptable

Calibration and preparation blanks were analyzed with each
analytical batch. No target analytes were detected in the
blanks.
IV.

Overall Assessment of Data For Use:

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

AUG 2 2 1956
Ecology & Environment, Inc.
Our Qiialiiy Control h Your Quality Assurance

Client #: CHI-96-031103
Address: Ecology and Environment,Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-1

Sample Description:
Label: SI
Date Sampled: 07/24/96
Time Sampled: 00:00
Date Received: 07/25/96
Collected By: Client

GN2201; J05-9607-807
Relog of L8736

Parame'ter

Results

Units

0.35
BDL

[chromium
Lead

mg/1
mg/1

Reportable
Detect
Limit

Method

1311/6010
1311/6010

0.010
0.050

Extr.
Date

08/14/96 08/16/96
08/14/96 08/16/96

BDL = Below Detection Limits
* CompoufKls are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
OAP# 900376G
SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SO CERTiK 96031

NC CERT# 444

TN CERT# 02985
ELPAT# 13801
VA CERT# 00395
MA CERT# M-FL449

CT CERT# PH-0122

ND CERT# R - U 8

HRS# E86240,86356

CA CERT# 1-1068
AZ CERT# AZ0529

Analysis
Date
Analyst

R e s p e c t f u l l y subi

Mariner Fernande
Laboratory Director

USAGE CERT
L9328-1

V.O.C. Analytical Laboratories, Inc.
710 East Ogden Avenue, Suite #104, Naperville, Illinois 60563-8603 • Phone: (708) 355-8VOC(8862) • Fax: (708) 355-8915

SH
SH

Client #:
Address:

Sample

CHI-96-031103
Ecology and E n v i r o n m e n t , I n c .
I l l W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : D a v i d Hendren

Page:
Date:
Log # :

Page 1 of
08/19/96
L9328-2

1

Description:
Label:
Date Sampled:
Time S a m p l e d :
Date Received:
C o l l e c t e d By:

GN2201; J 0 5 - 9 6 0 7 - 8 0 7
R e l o g of L8736

Parameter
XCLF H e t a l s
Chromium

Results
0.60

Units
mg/1

Method

Reportable
Detect
Limit

1311/6010

0.010

S2
07/24/96
00:00
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

08/14/96 08/16/96

BDL = Below Detection L i m i t s
* Compounds are Screened Only, with an estimated detection l i m i t .
A l l analyses were performed using EPA, ASTM, USGS, or Standard Methods.
A l l analyses were performed w i t h i n EPA holding times unless otherwise noted.
QAP# 900376G
SUB HRSiy 86122,86109,E86048
SC CERT# 96031
TN CERT# 02985
ELPAT# 13801
VA CERT# 00395
MA CERT# M-FL449

HRS# E86240,86356
ADEM ID# 40850
NC CERTlV 444
CT CERT# PH-0122
CA CERT# 1-1068
AZ CERT# AZ0529
USACE CERT

Respectfully

submitted.

Marino
Laboratory Director

ND CERT# R-148

L9328-2

V.O.C. Analytical Laboratories, Inc.

SH

Client #: CHI-96-031103
Address: Ecology and Environment,Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-3

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

GN2201; J05-9607-807
Relog of L8736

Parameter
XCIJ» » 6 t a l s
Chromium

Results

400

Units

mg/1

Reportable
Detect
Limit

Method

1311/6010

S3
07/24/96
00:00
07/25/96
Client

Extr.
Date

0.010

08/14/96 08/16/96

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection l i m i t .
A l l analyses were performed using EPA, ASTM, USGS, or Standard Methods.
A l l analyses were performed w i t h i n EPA holding times unless otherwise noted.
QAP# 900376G
SUB HRS# 86122,86109,E86048
SC CERT# 96031
TN CERT# 02985
ELPAT# 13801
VA CERT# 00395
MA CERT# M-FL449
ND CERT# R-148

HRS# E86240,86356
ADEM ID# 40850
NC CERT# 444
CT CERT# PH-0122
CA CERT# 1-1068
AZ CERT# AZ0529
USACE CERT

Laboratory

Director

L9328-3

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analyst

SH

C l i e n t # : CHI-96-031103
A d d r e s s : E c o l o g y and E n v i r o n m e n t , I n c .
I l l W. J a c k s o n B l v d .
C h i c a g o , I L 60604
A t t n ; D a v i d Hendren

P a g e : P a g e 1 of
Date: 08/19/96
Log # : L9328-4

1

Sample D e s c r i p t i o n :
L a b e l : S4
Date Sampled: 07/24/96
Time S a m p l e d : 0 0 : 0 0
Date Received: 07/25/96
C o l l e c t e d By: C l i e n t

GN2201; J 0 5 - 9 6 0 7 - 8 0 7
R e l o g of L8736

Parameter
XCLP. U e t a l s
Chromium
Lead
BDL = Below D e t e c t i o n

Results

Units

BDL
BDL

mg/1
mg/1

Reportable
Detect
Limit

Method

1311/6010
1311/6010

0.010
0.050

Extr.
Date

Analysis
Date
Analyst

08/14/96 08/16/96
08/14/96 08/16/96

Limits

* Compounds a r e Screened O n l y , w i t h an e s t i m a t e d d e t e c t i o n

limit.

A l l a n a l y s e s were p e r f o r m e d u s i n g EPA, ASTM, USGS, o r S t a n d a r d Methods.
A l l a n a l y s e s were p e r f o r m e d w i t h i n EPA h o l d i n g t i m e s u n l e s s o t h e r w i s e n o t e d .
QAP# 900376G

HRS# E86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SC CERT# 96031

NC CERTDf 444

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 13801

CA CERT# 1-1068

VA CERT# 00395

AZ CERT# AZ0529

MA CERT# M-FL449

USACE CERT

Respectfully

submitted.
/

Marijpo Fe^nand©^ ®
Laboratory D i r e c t o r

ND CERT# R-148

L9328-4

V.O.C. Analytical Laboratories, Inc.

SH
SH

ecology and enviroiMmeinitt9 nmc.
International Specialists in the Environment
33 North Dearborn Street

Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 2, 1996

TO;

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT;

Organic Data Quality Review for Volatile Organic
Compounds, Frost Manufacturing, Kenosha, Kenosha
County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of two liquid waste
samples collected from the Frost Manufacturing site is complete.
The samples were collected on July 24, 1996, by the Superfund
Technical Assessment and Response Team (START) contractor.
Ecology and Environment, Inc. (E & E ) . The samples were
submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
8240.
Sample Identification
START
Identification No.

Laboratory
Identification No,

VI
V2

L8736-1
L8736-2

Data Qualifications:
I.

Sample Holding Time:

Acceptable

The samples were collected on July 24, 1996, and analyzed
on July 31, 1996. This is within the 14-day holding time
limit.

recycled paper

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
VOA
Page 2
II.

Gas Chromatography/Mass Spectrometry (GC/MS) Tuning;
Acceptable
GC/MS tuning to meet ion abundance criteria using
bromofluorobenzene (BFB) were acceptable and samples were
analyzed within 12 hours of BFB tuning.

III.

Calibrations;
• Initial Calibration;

Acceptable

A five-point initial calibration was performed prior to
analysis. All average response factors were greater than
0.05. The percent relative standard deviations (%RSDs)
between response factors were less than 30% for all
detected target compounds.
• Continuing Calibration;

Acceptable

The percent differences of the response factors were less
than 25%, as required for detected target compounds.
IV.

Blank;

Acceptable

A method blank was analyzed with the samples. No target
compounds or contaminants were detected in the blank.
V.

Internal Standards:

Acceptable

The areas of the internal standards in the samples were
within -50% to •H00% of the associated calibration check
standard. The retention time of the internal standard was
within the 30-second control limit.
VI.

Compound Identification;

Qualified

The mass spectra of detected target compounds was not
provided by the laboratory; therefore, all reported
compound have been qualified "N".
VII.

Additional QC Checks;

Acceptable

The recoveries of the surrogates used in the samples and
blank were within laboratory-established guidelines.

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
VOA
Page 3
VIII. Overall Assessment of Data for Use:

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April
1990), Data Validation Procedures, Section 5.0, VOAs By
GC/MS analysis. Based upon the information provided, the
data are acceptable for use, with the above-stated
qualifications.
Data Qualifiers and Definitions;
N - Presumptive evidence of presence of material.

ecology and envirommenntt^ ImCo
International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602

Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 2, 1996

TO;

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH;

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Organic Data Quality Review for Semivolatile
Organic Compounds, Frost Manufacturing, Kenosha,
Kenosha County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and one
solid waste samples collected from the Frost Manufacturing site
is complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor. Ecology and Environment, Inc. (E & E ) . The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
8270.
Sample Identification
START
Identification No.
VI
V2
S4
Dl
D2

recycled paper

Laboratory
Identification No.
L8736-1
L8736-2
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
SVOA
Page 2
Data Qualifications;
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, extracted on
July 31, 1996, and analyzed on August 2, 199 6. Sample S4
was analyzed on August 7, 1996. This is within the 14-day
holding time limit, from collection to extraction and 40day limit from extraction to analysis.
II.

Gas Chromatography/Mass Spectrometry (GC/MS) Tuning;
Acceptable
GC/MS tuning to meet ion abundance criteria using
decafluorotriphenylphosphine (DFTPP) were acceptable and
samples were analyzed within 12 hours of DFTPP tuning.

III.

Calibrations:
• Initial Calibration;

Qualified

A five-point initial calibration was performed prior to
analysis. All average response factors were greater than
0.05 except benzidine; therefore, the nondetect values for
this compound have been flagged "R", as required. The
percent relative standard deviations (%RSDs) between
response factors were less than 3 0% for all detected target
compounds.
• Continuing Calibration:

Acceptable

The percent differences of the response factors were less
than 25%, as required for detected target compounds.
IV.

Blank;

Acceptable

A method blank was analyzed with the samples. No target
compounds or contaminants were detected in the blank.
V.

Internal Standards;

Acceptable

The areas of the internal standards in the samples were
within -50% to -(-100% of the associated calibration check
standard. The retention time of the internal standard was
within the 30-second control limit.

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
SVOA
Page 3
VI.

Compound Identification;

Qualified

The mass spectra of detected target compounds were not
provided by the laboratory; therefore all reported
compounds have been qualified "N".
VII.

Additional QC Checks;

Acceptable

The recoveries of the surrogates used in the samples and
blank were within laboratory-established guidelines.
VIII. Overall Assessment of Data for Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April
1990), Data Validation Procedures, Section 4.0 BNAs By
GC/MS analysis. Based upon the information provided, the
data are acceptable for use, with the above-stated
qualifications.
Data Qualifiers and Definitions;
N - Presumptive evidence of presence of material.
R - The sample results are rejected (analyte may or may not
be present) due to gross deficiencies in quality control
criteria. Any reported value is unusable. Resampling
and/or reanalysis is necessary for verification.

ecology and envirosisiffieinitt^ Imc.
International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM;

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH;

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Inorganic Data Quality Review for Resource
Conservation and Recovery Act (RCRA) Metals, Frost
Manufacturing, Kenosha, Kenosha County, Wisconsin

REFERENCE;

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and four
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor. Ecology and Environment, Inc. (E & E ) . The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 84 6
Methods 6010 and 7471.
Sample Identification
START
Identification No.
VI
V2
SI
S2
S3
S4
Dl
D2

recycled paper

Laboratory
Identification No.
L8736-1
L8736-2
L8736-4
L8736-5
L8736-6
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
RCRA Metals
Page 2
Data Qualifications:
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, and analyzed
on July 27 to 29, 1996. Analysis for mercury was performed
on July 16, 1996. This is within the 6-month (28 days for
mercury) holding time limit.
II.

Calibration;
Initial Calibration;

Acceptable

Recoveries for the initial calibration verification were
within 90 to 110% (80 to 120% for mercury), as required.
The correlation coefficient for mercury exceeded 0.995.
Continuing Calibration;

Acceptable

All analytes included in the continuing calibration
verification standard were within 90 to 110% (80 to 120%
for mercury), as required.
III.

Blanks;

Acceptable

Calibration and preparation blanks were analyzed with each
analytical batch. No target analytes were detected in the
blanks.
IV.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

ecology and envir€)iim©iml

HmCo

International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602

Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 2, 1996

TO;

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH;

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT;

Miscellaneous Data Quality Review for pH and
Asbestos, Frost Manufacturing, Kenosha, Kenosha
County, Wisconsin

REFERENCE;

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and four
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor. Ecology and Environment, Inc. (E & E ) . The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
9045 and EPA method 150.1.
Sample Identification
START
Identification No.
VI
V2
SI
S2
S3
S4
Dl
D2

recycled paper

Laboratory
Identification No.
L8736-1
L8736-2
L8736-4
L8736-5
L8736-6
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
pH, Asbestos
Page 2
Data Qualifications:
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, and analyzed
on August 7, 1996. The Office of Solid Waste and Emergency
Response (OSWER) Directive 9360.4-01 (April 1990) does not
provide holding times for these parameters.
II.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Data Validation Procedures,
Section 9.0, Generic Data Validation Procedures. Based
upon the information provided, the data are acceptable for
use.

ecology and efiivir^Hiimsinntg.nimc,
International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE;

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT;

Inorganic Data Quality Review for Cyanide, Frost
Manufacturing, Kenosha, Kenosha County, Wisconsin

REFERENCE;

Project TDD S05-9606-022 Analytical TDD S05-9607-807
Project PAN 6N2201SIXX Analytical PAN 6UAG01TA

The data quality assurance (QA) review of two liquid and one
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor. Ecology and Environment, Inc. (E & E ) . The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Method 3 3 5.3.
Sample Identification
Laboratory
Identification No,

START
Identification No.
VI
V2
S4

L8736-1
L8736-2
L8736-7

Data Qualifications;
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, and analyzed
on August 7, 1996. This is within the 14-day holding time.

recycled paper

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
Cyanide
Page 2
II.

Calibration;

Acceptable

The correlation coefficient of the initial calibration
curve exceeded 0.995. Recoveries of continuing
calibrations were within 85-110%.
III.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

Our Quality Control Is Your Quality Assurance

C l i e n t #: CHI-96-031104
A d d r e s s : E c o l o g y and E n v i r o n m e n t
E c o l o g y and E n v i r o n m e n t
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : , D a v e Hendren

P a g e : Page 1 of 6
Date: 08/09/96
Log # : L 8 7 3 6 - 1

Sample D e s c r i p t i o n :
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:

J05-9607-807

C o l l e c t e d By:

Parameter

N-Nitrosodimethylamine
niline
henol
is(2-Chloroethyl)
Ether
2-Chlorophenol
, 3-Dichlorobenzene
,4-Dichlorobenzene
enzyl alcohol
1,2-Dichlorobenzene
-Methylphenol
is {2-Chloroisopropyl)
Ethe
N-Nitrosodi-n-propylamine
^-Methylphenol
Blexachloroethane
«itrobenzene
Isophorone
-Nitrophenol
,4-Dimethyl Phenol
i s (2-Chloroethoxy) Methane
Benzoic Acid
-Nitrosodiethylamine
,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
•1 -Chioroani1ine

K
1
t

t

f

I
I
I

Results

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

Units

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

Reportable
Detect
Limit

190
160
250
170
170
260
180
220
280
120
880
290
210
220
170
230
210
110
150
2000
280
260
130
230
670

VI Sump-H20
07/24/96
1 3 :30
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

V.O.C. Analytical Laboratories, Inc.
710 East Ogden Avenue, Suite #104, Naperville, Illinois 60563-8603 • Phone: (708) 355-8VOC(8862) • Fax: (708) 355-8915

Treat

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Parcuneter

exachlorobutadiene
-Chloro- 3 -Methylphenol
-Methylnaphthalene
2-Methylnaphthalene
exachlorocyclopentadiene
,4,6-Trichlorophenol
2,4,5-Trichlorophenol
^-Chloronaphthalene
ft-Nitroaniline
•Dimethylphthalate
2,6-Dinitrotoluene
^^cenaphthylene
•3-Nitroaniline
^^cenaphthene
Dibenzofuran
, 4-Dinitrotoluene
,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
luorene
-Chlorophenyl-phenylether
4-Nitroaniline
^,6-Dinitro-2-Methylphenol
w-Nitrosodiphenylamine
Hizobenzene
4-Bromophenyl-phenylether
ilpha-BHC
iexachlorobenzene
^ Pentachlorophenol
gamma-BHC
•seta-BHC
Jphenanthrene
Anthracene
delta-BHC
fcarbazole
•leptachlor

f
f

f

t

I
I
I

Label
Date Sampled
Time Sampled
Date Received
Collected By

J05-9607-807

Results

Units

(cont inued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

190
120
120
260
340
210
500
100
220
150
220
170
1000
120
130
2000
2000
2000
910
100
100
2000
2000
190
120
210
150
160
1000
140
210
120
160
140
1000
210

VI Sump-H20 Treat
07/24/96
13:30
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Parameter

Results

s

t

i-n-butylphthalate
Idrin
luoranthene
Heptachlor Epoxide
benzidine
^yrene
Endosulfan I
^ , 4 ' -DDE
•Jieldrin

Bl,4'-DDD
Endosulfan II
ndrin Aldehyde
ndrin
utylbenzylphthalate
Endosulfan Sulfate
» , 4 ' -DDT
K n d r i n Ketone
Benzo(a)anthracene
3,3'-Dichlorobenzidine
hrysene
,2-Diphenylhydrazine
Bis(2-Ethylhexyl)Phthalate
J3i-n-octyl phthalate
M e n z o (b) f luoranthene
•benzo(k)fluoranthene
Benzo(a)pyrene
•Endeno(1, 2,3 -c,d)pyrene
B)ibenzo(a,h)Anthracene
^ e n z o (g, h, i) perylene
PCB 1016
•>CB 1221
|pCB 1232
PCB 1242
^ C B 1254
ftcB 1260
B:hlordane

(

t

I
I
I

V
Label: VI Sump-H20
Date Sampled: 07/24/96
Time Sampled: 13:30
Date Received: 07/25/96
Coll e c t e d B y : C l i e n t

J05-9607-807
7

Units

(cont Lnued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL g.
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
2300 ro
ug/1
240 t J
ug/1
BDL
ug/1
BDL
ug/1
ug/1
BDL
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
ug/1
BDL
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

160
220
150
240
2000'
120
340
370
230
220
1100
1600
200
120
130
210
1000
120
480
150
110
600
240
590
200
100
520
690
520
6000
6000
6000
6000
6000
6000
2000

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Treat

Analysis
Date
1^nalji

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address:
Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 4 of 6
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Parameter

i[iiii;?^i$:ii;i:|^<$|i£li§ii^
oxaphene
i l u t i o n Factor

f
f

rsenic
arium
Cadmium
^hromium
Kead
mercury
Selenium
ilver

I

Dichlorodifluoromethane
•ithanol
H:hlorome thane
vinyl Chloride
Bromomethane
B:hloroethane
Brrichlorofluoromethane
Acrolein
J.,1-Dichloroethene
Bicetone
Hodomethane
Carbon Disulfide
ethylene Chloride
crylonitrile
irans-l,2-dichloroethene
1,1-Dichloroethane
inyl Acetate
-Butanone
Chloroform
1,1,1-Trichloroethane
B:arbon Tetrachloride
Ifcenzene

K

f
I
I
I

Label
Date Sampled
Time S a m p l e d
Date Received
C o l l e c t e d By

J05-9607-807

Results

Units

(continued)
BDL
ug/1
100

BDL
5.4
BDL
540
57
0.11
BDL
BDL

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.13 ^»
0.0060»^
BDL
BDL
BDL

Method

Reportable
Detect
Limit

VI Sump-H20
07/24/96
13 :30
07/25/96
Client

Extr.
Date

Treat

Analysis
Date
Analyst

3510/8270
3510/8270

4000

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245.2
3010/6010A
3010/6010A

10
1 0
1 0
1 0
1 0
0 10
i 0
1 0

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

V.O.C. Analytical Laboratories, Inc.

0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050

Page: Page 5 of 6
Date: 08/09/96
Log #: L8736-1

Client #: CHI-96-031104.
Address:
Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren
Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time S a m p l e d :
Date Received:
C o l l e c t e d By:

J05-9607-807

Parameter

Results

Units

Method

Reportable
Detect
Limit

VI S u m p - H 2 0
07/24/96
13 : 3 0
07/25/96
Client

Extr.
Date

Treat

Analysis
Date
Analyst

(continued)

t

, 2-Dichloroethane
richloroethene
J., 2 -Dichloropropane
Dibromomethane
romodichloromethane
-Chloroethylvinyl Ether
Cis-1,3-Dichloropropene
4-Methyl-2-pentanone
oluene
rans-1,3-Dichloropropene
Ethyl Methacrylate
, 1, 2 -Trichloroethane
-Hexanone
ibromochloromethane
Chlorobenzene
thylbenzene
otal Xylenes
btyrene
Bromoform
is-1,4-dichloro-2-butene
,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
J^rans-1,4-dichloro-2-butene
KTBE
ML ,1,1,2-Tetrachloroethane
Cis-1,2-Dichloroethene
•iTe trachloroethene
B L ,2-Dibromoethane
~L,2-Dibromo-3-Chloropropane
Dilution Factor

f

t

K

C
t

Cyanide

i
I
I
I

BDL
BDL
BDL
BDL
BDL
BDL
BDL
0 . 0 8 0 r»
0.080 N
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0 . 0 0 9 0 t^
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1.0

BDL
3 .0

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
^ mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

mg/1

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

335.3
150.1

V.O.C. Analytical Laboratories, Inc.

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050
0050

0 010
0 10

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

08/07/96 08/07/96
08/07/96 08/07/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

I NO
INC

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 6 of 5
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results

Parameter
SjSjii^iJSlllliiifei^

Units

Method

Reportable
Detect
Limit

VI Sump-H20 Treat
07/24/96
13 : 3 0
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

t inued)

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900375G

HRS# E86240,86356

SUB HRS# 86122,86109,E86046

ADEM ID# 40850

SC CERTS 96 031

NC CERT# 444

TN CERT# 02985

CT CERTS PH-0122

ELPAT# 13801

CA CERTS 1-1068

VA CERT# 00395

Respectfully submittec

(

MA CERT# M-FL44 9

AZ CERTS AZ0529

ND CERTtt R-14 8

USACE CERT

V.O.C. Analytical Laboratories, Inc.

L8736-1

P a g e : Page 1 of 6
Date: 08/09/96
Log # : L8736-2

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren
Sample Description:
6N2201
KJ5100

L a b e l : V2 S u m p - P l a t i n g
Date Sampled: 07/24/96
Time S a m p l e d : 1 4 : 0 0
Date Received: 07/25/96
C o l l e c t e d By: C l i e n t

J05-9607-807

Results

Fnits

N-Nitrosodimethylamine
•Aniline
•Phenol
•eis(2-Chloroethyl) Ether
2-Chlorophenol
•l,3-Dichlorobenzene
•l,4-Dichlorobenzene
Benzyl a l c o h o l
1,2-Dichlorobenzene
B2-Methylphenol
BBis (2-Chloroisopropyl) Ethe
N-Nitrosodi-n-propylamine
—4-Methylphenol
Riexachloroethane
Hfitrobenzene
Isophorone
-Nitrophenol

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

,4-Dimethyl Phenol
i s (2-Chloroethoxy) Methane
Benzoic Acid
•j-Nitrosodiethylamine
^2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
•l-Chloroaniline

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

L

Parameter

Method

Reportable
Detect
Limit

Extr.
Date

Analysis
Date
1^nar

?:iiD|j|\!i?|i:i||i;i|aig|^

t
I
I
I

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
16
25
17
17
26
18
22
28
12
88
29
21
22
17
23
21
11
15
200
28
26
13
23
67

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of 6
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

V2 Sump-Plating
07/24/96
14:00
07/25/96
Client

Reportable
Detect

Parameter

Results

S e m i v o l a t i l e Organic Compoundss
•ilexachlorobutadiene
ft-Chloro-3-Methylphenol
^-Methylnaphthalene
2-Methylnaphthalene
Bfeexachlorocyclopentadiene
1^ , 4 , 6 - T r i c h l o r o p h e n o l
2,4,5-Trichlorophenol
2-Chloronaphthalene
ft-Nitroaniline
ft)imethylphthalate
2,6-Dinitrotoluene
HAcenaphthylene
•B -Nitroaniline
^cenaphthene
Dibenzofuran
, 4-Dinitrotoluene
,4-Dinitrophenol
4 -Nitrophenol
Diethylphthalate
luorene
-Chioropheny1-phenyle t h e r
4-Nitroaniline
^ , 6-Dinitro-2-Methylphenol
•J-Nitrosodiphenylamine
ift.zobenzene
4-Bromophenyl-phenylether
«l p h a - B H C
Biexachlorobenzene
^entachlorophenol
gamma-BHC
•seta-BHC
^henanthrene
Anthracene
delta-BHC
•Tarbazole
Bleptachlor

f
K

I
I
I

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
• ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Limit

Date

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

Date

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

1\nal

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of 6
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Parameter

Results

S
S e m i v o l a t i l e O r g a n i c Compounds
i-n-butylphthalate
Idrin
luoranthene
Heptachlor Epoxide
|feenzidine
Wbyrene
Endosulfan I
4,4'-DDE
ieldrin
,4'-DDD
Endosulfan I I
n d r i n Aldehyde
ndrin
utylbenzylphthalate
Endosulfan S u l f a t e
M , 4 ' -DDT
K n d r i n Ketone
^ e n z o (a) a n t h r a c e n e
3,3'-Dichlorobenzidine
hrysene
,2-Diphenylhydrazine
Bis(2-Ethylhexyl)Phthalate
^ i - n - o c t y l phthalate
M e n z o (b) f l u o r a n t h e n e
W e n z o (k) f l u o r a n t h e n e
Benzo(a)pyrene
« [ n d e n o ( 1 , 2, 3 ~c, d ) p y r e n e
w i b e n z o ( a , h) A n t h r a c e n e
^ e n z o (g, h , i ) p e r y l e n e
PCB 1016
•>CB 1221

(

t

(

t

P>CB 1232
PCB 1242
PCB 1254
CB 1260
hlordane

t
I
I
I

Label: V2 Sump-Plating
Date Sampled: 07/24 /96
Time Sampled: 14:00
Date Received: 07/25/96
Coll ected By: Client

J05-9607-807
7

Units

(COE tinued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL R
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
ug/1
BDL
ug/1
BDL
BDL
ug/1
ug/1
BDL
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
ug/1
BDL
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

Extr.
Date

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
48
15
11
60
25
59
20
10
52
69
52
600
600
600
600
600
600
200

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604 ,
Attn: Dave Hendren

Page: Page 4 of
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Parameter
:|liiipi|S^||ii'i|||ii;^^^^^^
rfoxaphene
• d i l u t i o n Factor
•Dichlorodifluoromethane

Ipthanol
Chloromethane
Vinyl Chloride
^Bromomethane
B;;hloroethane
Trichlorofluoromethane
^^.crolein
ll,1-Dichloroethene
^^cetone
lodomethane
•Carbon D i s u l f i d e
wlethylene Chloride
Acrylonitrile
Trans-l,2-dichloroethene
HI,1-Dichloroethane
J v i n y l Acetate
2-Butanone
^Uhloroform
HI,1,1-Trichloroethane
Bbarbon T e t r a c h l o r i d e
Benzene
•|L,2-Dichloroethane
•rrichloroethene
^ , 2-Dichloropropane
Dibromomethane
|feromodichloromethane
^2-Chloroethylvinyl Ether
Cis-1,3-Dichloropropene
4-Methyl-2-pentanone
oluene
rans-l,3-Dichloropropene

t
I
I
I

Label:
Date Sampled:
Time S a m p l e d :
Date Received:
C o l l e c t e d By:

J05-9607-B07

Results

Units

Method

Reportable
Detect
Limit

V2 S u m p - P l a t i n g
07/24/96
14 :00
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

(continued)
BDL
10

ug/1

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

1 0
1 0
1 0
1 0
1 0
1 0
1 0
10
1 0
1 0
1 0
1 0
4 0
10
1 0
1 0
1 0
1 0
1 0
1 0
1 0
1 0
1 0
1 0
-1 0
1 0
1 0
1 0
1 0
1 0
1 0
1 0

07/31/96
07/31/96
07/31/96
.07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

V.O.C. Analytical Laboratories, Inc.

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Client #: CHI-96-031104
Address:
Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 5 of
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Parameter

V o l a t i l e O r g a n i c Compounds
• e t h y l Methacrylate
•L,1,2-Trichloroethane
^-Hexanone
Dibromochloromethane
•::hlorobenzene
Kthylbenzene
T o t a l Xylenes
Styrene
romoform
is-1,4-dichloro-2-butene
1,1,2,2-Tetrachloroethane
^,2,3-Trichloropropane
•Trans-l,4-dichloro-2-butene
^TBE
1,1,1,2-Tetrachloroethane
•:is-l,2-Dichloroethene
•Tetrachloroethene
1,2-Dibromoethane
1,2-Dibromo-3-Chloropropane
B^ilution Factor

t

f

'yanide

L a b e l : V 2 S u m p - P l a t in g
Date Sampled: 07/24/96
Time Sampled: 14:00
Date Received: 07/25/96
Coll ected B y : Client

J05-9607-807
7

Results

(continued)
BDL
BDL
BDL
BDL
BDL
. BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1.0

BDL

Units

Method

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240.
5030/8240
5030/8240

mg/1

335.3

Reportable
Detect
Limit

Extr.
Date

Analysis
Analyst
Date

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

0.010

08/07/96 08/07/96

V.O.C. Analytical Laboratories, Inc.

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

INO

Page: Page 6 of 6
Date: 08/09/96
Log #: L8736-2

client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren
Saimple Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Units

Method

Reportable
Detect
Limit

V2 Sump-Plating
07/24/96
14 : 0 0
07/25/96
Client

Extr.
Date

IliSiiiiiiilsiJilll^giijii^
BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAPS 900376G

HRSS E86240,86356

SUB HRS# 86122,86109,E86D48

ADEM IDS 40850

SC CERTS 96031

NC CERTS 444

TN CERTS 02985

CT CERTS PH-0122

ELPATS 13801

CA CERTS 1-1068

VA CERTS 00395

AZ CERTS AZ0529

MA CERTS M-FL44 9

USACE CERT

<r^

pectfully s

Marino FernandeJ
Laboratory Director
L8736-2

ND CERTS R-148

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analyst

Our Quality Control Is Your Quality Assurance

Client #: CHI-96-031104
Address: Ecology & Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: David Hendren

Page: Page 1 of 1
Date: 08/08/96
Log#: L8736-3

Sample Description:

Label: Al
Date Sampled: 07/24/96
Time Sampled: 14:10
Date Received: 07/25/96
Collected By:
Client

Bulk Asbestos ID

Extraction Date: 07/30/96
Analysis Date: 07/30/96

Description

Present

Method

Homogeneous
sample

% Cellulose

% Nonfibrous
Material

% Fibrous Glass

Color

Ceiling tile

no

EPA-600/PLM

No

20-25%

70-75%

2-5%

cream

Respectfijlly submitted.

Marino Fernandez
Laboratory Director

V.O.C. Analytical Laboratories, Inc.
710 East Ogden Avenue, Suite #104, Naperville, Illinois 60563-8603 • Phone: (708) 355-8VOC(8862) • Fax: (708) 355-8915

C l i e n t #: CHI-96-031104
A d d r e s s : Ecology and Environment
E c o l o g y and E n v i r o n m e n t
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave Hendren

P a g e : Page 1 of
Date: 08/09/96
Log # : L8736-4

1

Sample D e s c r i p t i o n :
6N2201
KJ5100

Parameter
ietals
Arsenic
^arium
•Tadmium
Chromium
Lead
•Mercury
Kelenium
Silver

I

Label :
D a t e Sampled .:
Time Sampled .:
D a t e :R e c e i v e d .:
C o l l e c t e d By•:

J05-9607-807

Results

Units

13
270
3.8

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

1600
700
BDL
BDL
1.4

4.5

•H

Reportable
Detect
Limit

Method
3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A
9045

SI Y e l l o w Powder
07/24 / 9 6
14:00
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

1.0
1.0

0.10

08/07/96 08/07/96

0.10

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G

HRS# £86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850 •

SC CERT# 95031

NC CERT# 444

TN CERT# 02 985

CT CERT# PH-0122

ELPAT# 13801

CA CERT# 1-1068

VA CERT# 00395

AZ CERTft AZ0529

MA CERT# M--FL449

USACE CERT

Marino" Fernandez^ «
Laboratory Director

ND CERT# R~14 8

V.O.C. Analytical Laboratories, Inc.

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

5.0
1.0
1.0
1.0
1.0

JK
JK
JK
JK
JK
JK
JK
JK

INO

C l i e n t #: CHI-96-031104
Address:
E c o l o g y and E n v i r o n m e n t
E c o l o g y and E n v i r o n m e n t
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave H e n d r e n

P a g e : Page 1 of 1
Date: 08/09/96
Log # : L 8 7 3 6 - 5

Sample D e s c r i p t i o n :
6N2201
KJ5100

Parameter

Arsenic
^arium
•Tadmium
Chromium
Lead
U^ercury
•Selenium
Silver

t

L a b e l : S2 P l a t i n g Room FL
D a t e Sampled : 0 7 / 2 4 / 9 6
Time Sampled : 1 4 : 1 5
Date Received : 07/25/96
C o l l e c t e d By : C l i e n t

J 0 5 - 9 6 0 7 - 8 0 77

Results

Units

14
49
BDL

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

3500
130
BDL
BDL
BDL

Method

Reportable
Detect
Limit

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

Extr.
Date

Analysis
Date
Analyst

10
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

0.10

08/07/96 08/07/96

5.0
1.0
1.0
1.0
1.0

0.10

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

eneral chemistry
1.0

9045

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding.times unless otherwise noted.
QAP# 900376G

HRS# E86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SC CERT# 96031

NC CERT# 444

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 138 01

CA CERT# 1-1068

VA CERT# 00395

AZ CERT# AZ0529

MA CERT# M-FL449

USACE CERT

Marino Fernandez
Laboratory Director
L8736-5

ND CERT# R-148

V.O.C. Analytical Laboratories, Inc.

INO

P a g e : Page 1 of
Date: 08/09/96
Log # : L8736-6

C l i e n t #: CHI-96-031104
Address:
E c o l o g y and E n v i r o n m e n t
E c o l o g y and E n v i r o n m e n t
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave Hendren
Sample D e s c r i p t i o n :
6N2201
KJ510 0

Label:
Date Sampled:
Time Sampled:
Date Received:
Coll ected By:

J 0 5 - 9 6 0 7 - 8 0 77

Parameter
Arsenic
•barium
ftladmium
^Thromium
Lead
•Mercury
Kelenium
Silver

I

Results

46
1.5
BDL
6900
50
0.18
BDL
1.3

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

0.00

S3 Drum S p i l l
07/24/96
15:00
07/25/96
Client

Reportable
Detect
Limit

Extr.
Date

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5.0
1.0
5.0
1.0
1.0
0.10
10
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

9045

0.10

08/07/96 08/07/96

Method

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G

HRS# E86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SC CERT# 96 031

NC CERT# 4 44

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 13801

CA CERT# 1-1068

VA CERT# 00395

AZ CERTS AZ0529

MA CERT# M-PL44 9

USACE CERT

1

Marino Fernandez
Laboratory Director
L8736-6

ND CERT# R-148

V.O.C. Analytical Laboratories, Inc.

Area

Analysis
Date
;^al:

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

INO

P a g e : Page 1 of 4
Date: 08/09/96
Log # : L 8 7 3 6 - 7

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren
Scunple Description:
6N2201
KJ5100

1

Parameter

Results

e a u i v o l a t i l e O r g a n i c Compounds
N-Nitrosodimethylamine
^miline
B^henol
^ i s (2-Chloroethyl) Ether
2-Chlorophenol
•l,3-Dichlorobenzene
Hi,4-Dichlorobenzene
Benzyl a l c o h o l
1,2-Dichlorobenzene
-Methylphenol
is(2-Chloroisopropyl) Ethe
N-Nitrosodi-n-propylamine
^-Methylphenol
•iexachloroethane
Rjitrobenzene
Isophorone
-Nitrophenol
,4-Dimethyl Phenol
i s ( 2 - C h l o r o e t h o x y ) Methane
Benzoic Acid
•I-Nitrosodiethylamine
• I,4-Dichlorophenol
1,2,4-Trichlorobenzene
aphthalene
-Chloroaniline

t

t

f

I
I
I

Label:
Date Sampled:
Time Sampled:
Date Received:
C o l l e c t e d By:

J05-9607-807

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg.
mg/kg
mg/kg
mg/kg
mg/kg

Method

Reportable
Detect
Limit

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

V.O.C. Analytical Laboratories, Inc.

0.33
0.10
0.10
0.17
0.27
0.10
0.10
0.26
2.1
0.39
0.35
0.59
0.42
0.28
0.26
0.27
0.21
0.20
0.15
0.50
0. 10
0.14
0.49
0.16
0.10

S4 Drum Spill Area
07/24/96
15 :15
07/25/96
Client

Extr.
Date

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date
Analyst

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of 4
Date: 08/09/96
Log #: L8736-7

Sample Description:
6N2201
KJ5100

Parameter

Results

s
Semivolatile. Organic Compounds
•Mexachlorobutadiene
K-Chloro-3-Methylphenol
^-Methylnaphthalene
2-Methylnaphthalene
exachlorocyclopentadiene
, 4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
Bb-Nitroaniline
R)imethylphthalate
2,6-Dinitrotoluene
MAcenaphthylene
•3-Nitroaniline
^^cenaphthene
Dibenzofuran
•E,4-Dinitrotoluene
•2,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
luorene
-Chlorophenyl-phenylether
4-Nitroaniline
^,6-Dinitro-2-Methylphenol
m-Nitrosodiphenyl amine
H^zobenzene
4-Bromophenyl-phenylether
lpha-BHC
exachlorobenzene
entachlorophenol
gamma-BHC
eta-BHC
henanthrene
Anthracene
delta-BHC
•Tarbazole
Bkeptachlor

t

t

t
f
I
I
I

Lab el:
Date Sampled:
Time Sampled:
Date Received:
Coll ected By:

J05-9607-807
7

Units

(con tinued)
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg•
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg

Method

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

Reportable
Detect
Limit

0.10
0.10
0.10
0.10
0.32
0.20
0.19
0.25
0.31
0.10
0.14
0.10
0.23
0.26
0.10
0.15
0.60
0.18
0.10
0.25
0.16
0.10
0.26
0.28
0.36
0.70
0.66
0.25
0.29
0.40
0.15
0.15
0.20
0.16
. 0.20
0.44

V.O.C. Analytical Laboratories, Inc.

S4 Drum Spill Area
07/24/96
15:15
07/25/96
Client

Extr.
Date

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date
Analyst

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of 4
Date: 08/09/96
Log #: L8736-7

Sample Description:
6N2201
KJ5100

Parameter

Results

s
i-n-butylphthalate
Idrin
rluoranthene
Heptachlor Epoxide
|fcenzidine
Kiyrene
Endosulfan I
4,4'-DDE
•3ieldrin
»,4'-DDD
Endosulfan I I
n d r i n Aldehyde
ndrin
utylbenzylphthalate
Endosulfan S u l f a t e
•4,4'-DDT
K n d r i n Ketone
^Benzo(a)anthracene
3,3'-Dichlorobenzidine
hrysene
,2-Diphenylhydrazine
Bis{2-Ethylhexyl)Phthalate
^ i - n - o c t y l phthalate
M e n z o (b) f l u o r a n t h e n e
Bfeenzo(k)fluoranthene
Benzo(a)pyrene
•jEndeno ( 1 , 2 , 3 - c , d) p y r e n e
M i b e n z o ( a , h) A n t h r a c e n e
^Benzo(g,h,i)perylene
PCB 1016
CB 1221
CB 1232
PCB 1242
PCB 1254
ftcB
1260
B:hlordane

C

(

t
f

I
I
I

Label:
Date Sampled:
Time Sampled:
Date Received:
C o l l e c t e d By:

J05-9607-807

Units

(cont:Lnued)
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL(?
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg.
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
mg/kg
4.5 «^
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg

Method

Reportable
Detect
Limit

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

V.O.C. Analytical Laboratories, Inc.

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
2
2
2
2
0

21
16
34
27
27
39
50
12
17
57
30
25
22
26
24
18
20
51
52
22
10
51
22
42
54
28
24
77
10
0
0
0
0
0
0
67

S4 Drum S p i l l Area
07/24/96
15:15
07/25/96
Client

Extr.
Date

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date
1\nsLl

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

P a g e : Page 4 of 4
Date: 08/09/96
Log # : L 8 7 3 6 - 7

C l i e n t #: CHI-96-031104
Address:
E c o l o g y and E n v i r o n m e n t
E c o l o g y and E n v i r o n m e n t
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave H e n d r e n
Sample D e s c r i p t i o n :
6N2201
KJ5100

Parameter

f

L a b e l : S4 Drum S p i l l
Date Sampled: 07/24/96
Time S a m p l e d : 1 5 : 1 5
Date Received: 07/25/96
C o l l e c t e d By: C l i e n t

J05-9607-807

oxaphene
ilution Factor

Results

Units

(continued)
mg/kg
BDL
1.0

Reportable
Detect
Limit

Method

Extr.
Date

Area

Analysis
Date
Analyst

3550/8270
3550/8270

1 5

08/06/96 08/07/96
08/06/96 08/07/96

EP
EP

JK
JK
JK
JK
JK
JK
JK
JK

Metals

t
t

rsenic
arium
Cadmium
Chromium
ead
ercury
Selenium
Silver

15
43
BDL
4000
950
BDL
BDL
BDL

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5 0
1 0
1 0
1 0
1 0
0 10
IC)
1 0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

eneral Chemistry
Cyanide

BDL

mg/kg

335.3

0.10

08/07/96 08/07/96

c

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G

HRS# E86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SC CERT# 96031

NC CERT# 444

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 13 801

CA CERT# I-1068

VA CERT# 00395

AZ CERT# AZ0529

MA CERT# M~FL4 4 9

USACE CERT

jectfully submittec

/
Marino S^rnandez__^
Laboratory Director
L8736-7

ND CERT# R-148

V.O.C. Analytical Laboratories, Inc.

,

INO

C l i e n t #: CHI-96-031104
Address:
E c o l o g y and E n v i r o n m e n t
Ecology and Environment
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave H e n d r e n

Page: Page. 1 of 4
Date: 08/09/96
Log #: L8736-8

Sample D e s c r i p t i o n :
6N2201
KJ5100

Parameter

Results

s e m i v o l a t i l e O r g a n i c Compounds
N-Nitrosodimethylamine
niline
henol
is(2^Chloroethyl) Ether
2-Chlorophenol
, 3-Dichlorobenzene
,4-Dichlorobenzene
Benzyl a l c o h o l
1,2-Dichlorobenzene
-Methylphenol
is(2-Chloroisopropyl) Ethe
N-Nitrosodi-n-propylamine
^-Methylphenol
Blexachloroethane
•Nitrobenzene
Isophorone
-Nitrophenol
,4-Dimethyl Phenol
is(2-Chloroethoxy) Methane
Benzoic Acid
-Nitrosodiethylamine
, 4-Dichlorophenol
1,2,4-Trichlorobenzene
aphthalene
-Chloroaniline

K
f
I

t
f

f
I
I
I

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

rnits

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
16
25
17
17
26
18
22
28
12
88
29
21
22
17
23
21
11
15
200
28
26
13
23
67

Dl Drum: 55 G a l BLK
07/24/96
14:45
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of 4
Date: 08/09/96
Log #: L8736-8

Sample Description:
6N2201
KJ5100

Parameter

Results

s
jHexachlorobutadiene
»-chloro-3-Methylphenol
^-Methylnaphthalene
2-Methylnaphthalene
exachlorocyclopentadiene
, 4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
-Nitroaniline
imethylphthalate
2,6-Dinitrotoluene
™Acenaphthylene
•3-Nitroaniline
^^cenaphthene
Dibenzofuran
•p,4-Dinitrotoluene
^P,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
luorene
-Chlorophenyl-phenylether
4-Nitroaniline
j4, 6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine
kzobenzene
4 -Bromophenyl-phenylether
lpha-BHC
exachlorobenzene
entachlorophenol
gamma-BHC
•seta-BHC
whenanthrene
Anthracene
delta-BHC
arbazole
eptachlor

f
t

t
I

t
t
I
I
I

LabelL: D l D r u m :
Date Sampled: 07/24/96
Time Sampled: 14:45
Date Received: 07/25/96
Coll ected By: Client

J05-9607-807
7

Units

(cont Lnued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

55 Gal B L K

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of 4
Date: 08/09/96
Log #: L873,6-8

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Reportable
Detect
Parameter

Results

s

•jDi-n-butylphthalate
•\ldrin
^"luoranthene
Heptachlor Epoxide
^benzidine
»>yrene
Endosulfan I
4,4'-DDE

t
(

ieldrin
,4'-DDD
Endosulfan II
ndrin Aldehyde
ndrin
utylbenzylphthalate
Endosulfan Sulfate
W , 4 ' -DDT
K n d r i n Ketone
^Benzo(a)anthracene
3,3'-Dichlorobenzidine
fchrysene
^ , 2-Diphenylhydrazine
Bis(2-Ethylhexyl)Phthalate
^i-n-octyl phthalate
M e n z o (b) f luoranthene
•Benzo(k)fluoranthene
Benzo(a)pyrene
•lEndeno (1, 2 , 3 - c, d) pyrene
•Dibenzo(a,h)Anthracene
^Benzo(g,h,i)perylene
PCB 1016
* C B 1221

U=CB 1232
PCB 1242
PCB 1254
CB 1260
hlordane

t
I
I
I

Units

Method '

(cont.Lnued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL P^
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
130 |0
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

Dl Drum: 5 5 G a l BLK
07/24/96
14 : 4 5
07/25/96
Client

Extr.

Analysis

Limit

Date

Date

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
48
15
11
60
25
59
20
10
52
69
52
600
600
600
600
600
600
200

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

V.O.C. Analytical Laboratories, Inc.

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

i\nal

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 4 of 4
Date: 08/09/96
Log #: L8736-8

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
C o l l e c t e d By:

J05-9607-807

Parameter

Results

Method

Units

Semivolatile Organic Compounds
(continued)
BDL
oxaphene
ug/1
ilution Factor
10

f

Reportable
Detect
Limit

•

Dl Drum: 55 Gal BLK
07/24/96
14 :45
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245.2
3010/6010A
3010/6010A

20
1.0
2.0
1.0
1.0
0.10
1.0
1.0

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

0.10

08/07/96 08/07/96

Jiiilipil::-;;;:

f

rsenic
arium
Cadmium
chromium
Kiead
B/Iercury
Selenium
j llVf
ilver

(

BDL
BDL
BDL
9000
BDL
BDL
BDL
BDL

mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/31/96
07/29/96
07/29/96

eneral Chemistry
0.00

150.1

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G

HRS# E86240,86356

SUB HRS# 86122,86109,E86048

ADEM ID# 40850

SC CERT# 96031

NC CERT# 444

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 13 8 01

CA CERT# 1-1068

VA CERT# 00395

AZ CERT# AZ0529

MA CERT# M-FL449

USACE CERT

Marino Fernandez
Laboratory Director
L8736-8

ND CERT# R-14 8

V.O.C. Analytical Laboratories, Inc.

INO

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 4
Date: 08/09/96
Log #: L8736-9

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Coll ected By:

J05-9607-807
7

D2 Drum: 55 Gal BLK
07/24/96
15:15
07/25/96
Client

Reportable

Detect
Parameter

;jiiilli^iiiiS;iiiis^iiaii:is^ii^

N-Nitrosodimethylamine
niline
henol
i s (2-Chloroethyl) E t h e r
2 -Chlorophenol
•L,3-Dichlorobenzene
HL ,4-Dichlorobenzene
Benzyl a l c o h o l
1,2-Dichlorobenzene
-Methylphenol
i s (2-Chloroisopropyl) Ethe
N-Nitrosodi-n-propylamine
^-Methylphenol
Mexachloroethane
Writrobenzene
Isophorone
-Nitrophenol
,4-Dimethyl Phenol
i s ( 2 - C h l o r o e t h o x y ) Methane
Benzoic Acid
-Nitrosodiethylamine
,4-Dichlorophenol
1,2,4-Trichlorobenzene
aphthalene
-Chloroaniline

K
K

t

r

f
I
I
I

Results

Units

Method

Limit

Extr.
Date

Analysis
Date
Analyst

Is
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
16
25
17
17
26
18
22
28
12
88
29
21
22
17
23
21
11
15
200
28
26
13
23
67

07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96-08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96
07/31/96 08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

C l i e n t # : CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave H e n d r e n

P a g e : Page 2 of 4
Date: 08/09/96
Log # : L8736-9

Sample D e s c r i p t i o n :
6N2201
KJ5100

J05-9607-807

Parameter

Results

SBmiv<:>latile O r g a n i c Compounds
^lexachlorobutadiene
1 -chloro-3-Methylphenol
^-Methylnaphthalene
2-Methylnaphthalene
exachlorocyclopentadiene
, 4,6-Trichlorophenol
2,4,5-Trichlorophenol
^-Chloronaphthalene
ft-Nitroaniline
•bimethylphthalate
2,6-Dinitrotoluene
^^c enaphthylene
•3-Nitroaniline
^^cenaphthene
Dibenzofuran
K,4-Dinitrotoluene
K,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
luorene
-chlorophenyl-phenylether
4-Nitroaniline
^,6-Dinitro-2-Methylphenol
•SI-Nitrosodiphenylamine
Btizobenzene
4-Bromophenyl-phenylether
•alpha-BHC
Mexachlorobenzene
^"entachlorophenol
gamma-BHC
•seta-BHC
^'henanthrene
Anthracene
delta-BHC
barbazole
Heptachlor

f

t

I

I
I
I

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

D2 Drum: 55 Gal BLK
07/24/96
15:15
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of 4
Date: 08/09/96
Log #: L8736-9

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Coll ected By:

•

6N2201
KJ5100

•

J05-9607- 807

1
^

Results

Parameter

Units

Method

Reportable
Detect
Limit

D2 Drum: 55 Gal BLK
07/24 /96
15:15
07/25 /96
Client

Extr.
Date

Analysis
Date
Analyst

1
i'ffiiii^i^iiiliii«:-iJiSi§^iiii

Sfeompounds

•pi-n-butylphthalate

Bvldrin
^luoranthene
Heptachlor Epoxide
^benzidine
(pyrene
Endosulfan I
^ , 4 ' -DDE
•Dieldrin

Bi ,4'-DDD
Endosulfan II
•Endrin Aldehyde
•Bndrin
"Butylbenzylphthalate
Endosulfan Sulfate
• i ,4'-DDT
• E n d r i n Ketone
Benzo(a)anthracene
3,3'-Dichlorobenzidine
•Chrysene
•l,2-Diphenylhydrazine
Bis(2-Ethylhexyl)Phthalate
JDi-n-octyl phthalate
•Benzo(b)fluoranthene
^Benzo(k)fluoranthene
Benzo(a)pyrene
•Indeno(1,2,3 -c,d)pyrene
Hoibenzo(a,h)Anthracene
^Benzo(g,h,i)perylene
PCB 1016
•PCB

1221

| P C B 1232
PCB 1242
^ C B
1254
H P C B 1260
Bchlordane

I
I
I

( c o n t .Lnued)

BDL
BDL
BDL
BDL
BDLR.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

ug/1
ug/1
ug/1
ug/1
ug/1

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
48
15
11
60
25
59
20
10
52
69
52
600
600
600
600
600
600
200

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
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07/31/96
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07/31/96
07/31/96
07/31/96
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07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
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08/02/96
08/02/96
08/02/96
08/02/96
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08/02/96
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08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

C l i e n t # : CHI-96-031104
Address:
Ecology and Environment
Ecology and Environment
111 W. J a c k s o n B l v d .
C h i c a g o , IL 60604
A t t n : Dave Hendren

P a g e : Page 4 of 4
Date: 08/09/96
Log # : L8736-9

Sample D e s c r i p t i o n :
6N2201
KJ5100

Label:
Date Sampled:
Time S a m p l e d :
Date Received:
C o l l e c t e d By:

J05-9607-807

Parameter

Results

Units

S e m i v o l a t i l e O r g ^ ^ l c Compounds
(continued)
•Toxaphene
BDL
ug/1
ftilution
Factor
10

Miiiiii

f

rsenic
arium
Cadmium
^I^hromium
Kead
Bi>1ercury
Selenium
ilver

I

BDL
0.24
BDL
19
1.2
0.0041
BDL
BDL

mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1

Reportable
Detect
Limit

Method

D2 Drum: 55 Gal BLK
07/24/96
15:15
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245.2
3010/6010A
3010/6010A

0
0
0
0
0
0
0
0

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

10
10
10
10
10
0010
10
10

08/01/96
07/29/96
07/29/96
08/01/96
08/01/96
07/31/96
07/29/96
07/29/96

eneral Chemistry

pH'••"'''"••••••

8.0

150.1

0.10

08/07/96 08/07/96

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G

HRS# £86240,86356

SUB HRS# 86122,86109,E86046

ADEM ID# 40850

SC CERT# 96031

NC CERT# 444

TN CERT# 02985

CT CERT# PH-0122

ELPAT# 13801

CA CERTft 1-1068

VA CERT# 00395

AZ CERT# AZ0529

MA CERT# M-FL44 9

USACE CERT

ted.

Marino Fernandez
Laboratory Director

ND CERT# R-148

L8736-9

V.O.C. Analytical Laboratories, Inc.

INO