Site Assessment Report for Frost Manufacturing Company Kenosha, Kenosha County, Wisconsin

Site assessment report, done by Ecology and Environment, Inc., in on the site conditions, human health, and environment threats at Frost Manufacturing Company, in Kenosha, Wisconsin.

254393

1996-09-20 00:00:00.0

WID006090286

Frost Manufacturing Company

PDF

Ecology and Environment, Inc.

Site Assessment

Administrative Record

text

Human health

Environment

Site conditions

Frost Manufacturing Company

Environmental reporting

Midwest

Ecology and Environment, Inc.

Environmental Protection Agency

City of Kenosha

1996-09-20

Ecology and Environment, Inc.

Environmental Protection Agency

City of Kenosha

Copyright undetermined

eng

Kenosha, Wisconsin

PDF

EPA Region 5 Records Ctr.

254393

SITE ASSESSMENT REPORT
FOR
FROST MANUFACTURING COMPANY
KENOSHA, KENOSHA COUNTY, WISCONSIN
TDD: SOS-9606-022
PAN: 6N2201SI

September 20, 1996

Prepared for:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Emergency and Enforcement Response Branch
77 West Jackson Boulevard
Chicago, Illinois 60604

Prepared by:

Date:
John A. Nordine, START Project Manager

Reviewed by:

Date:
M.J. Ripp, Assistant START Program Manager

Approved by:

Date:

Thomas Kouris, START Program Manager

Table of Contents

Section
1
2
f

3
4
5
6

Page
Introduction
Background
2.1 Site Description
2.2 Site History
Site Assessment
Analytical Results
Discussion of Potential Threats
Proposed Removal Actions

Appendix
A
B
C

Photodocumentation
Analytical Results
Cost Estimates

1-1
2-1
2-1
2-1
3-1
4-1
5-1
6-1
Page
A-l
B-l
C-l

List of Figures

Figure
2-1
3-1

Page
Site Location Map
Site Features/Sample Location Map

2-5
3-3

in

List of Tables

Table
4-1
4-2
4-3
4-4

Page
Cyanide, pH, and Total Metals Analytical Results
TCLP Metals Analytical Results
Volatile Organic Compounds Analytical Results
Semivolatile Organic Compounds Analytical Results

IV

4-2
4-3
4-4
4-5

1. Introduction

The United States Environmental Protection Agency (U.S. EPA) has tasked the Superfund
Technical Assessment and Response Team (START) contractor Ecology and Environment, Inc.
(E & E), under Technical Direction Document (TDD) S05-9606-022 to assess site conditions and
threats to human health and the environment at the Frost Manufacturing Company (FMC) site located
in Kenosha, Kenosha County, Wisconsin.

1-1

2. Background

2.1 Site Description

The FMC site is located at the southeast corner of the intersection of 14th Avenue and 65th
Street, 6523 14th Avenue, in Kenosha, Kenosha County, Wisconsin. The legal description of the site
is: Northwest 1/4, Section 6 Township 1 North, Range 23 East (latitude 42°34'29.1"N; longitude
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•• 87 49'36.4"W)(Figurej£rl). The site is comprised of 4.75 acres of land with an adjacent 0.41 acres,

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which is used for parking. Currently, the site is an inactive plumbing supply manufacturer. The site
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is comprised of the brass foundry building, located on the northwest portion of the site; the main
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plant building 'located south of the foundry building; and five storage sheds located east of the main

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,, t , . plant building and west of the Union Pacific Railroad (UPRR) (formerly the Chicago and
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Northwestern Railroad). The brass foundry building consistsyof seven main areas: a core department,

/v ji/1^ a grinding department, a mold department, a south blowmatic molder, a link shakeout, a melt
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'-'•y L-; department, and a boiler room. The southern part of the main plant building was a new addition and
contained the wastewater pretreatment system, the treatment area, product storage, and loading docks.
The northern part of the main building contained the production process area and offices. The
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production process area consisted of an annealing furnace, metal drawing machines, a plating area, an "-"
electropolish and stripping area, and a buffing process area.. The site is bordered by the UPRR line
to the east, 14th Avenue to the west, 65th Street to the north, and Becker Inc., property to the south.
The site topography is relatively flat. The site is located in a residential/heavy industrial area

The

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population of Kenosha is 80,352 persons according to the 1990 U.S. Census.

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-7

2.2 Site History

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The FMC site has been in use since 1903. FMC's brass foundry was used from
approximately 1969 to 1991, for the manufacture of leaded brass parts. In September 1991, the
leaded- brass foundry ceased operations. Records indicate that approximately 1,120 cubic yards of

2-1

"7

foundry sand were generated at the site between 1986 and 19£1__ The remainder of the facility
(plating) has been inactive since the company detelared bankruptcy in 1994. FMC manufactured
copper cubing, chrome-plated plumbing trim, swimming pool deck equipment, and leaded-brass
castings. In 1987, a wastewater pretreatment system was completed to meet federal pretreatment
standards for metal finishing under the Code of Federal Regulations (CFR) 443.
Products manufactured at the FMC site consisted of plumbing fittings and fixtures, brass
goods, specialized plumbing fittings, heat exchanger fittings, and swimming pool components. FMC
V- j '••' *. ". ••

manufactured 550,000 square feet per year (sq ft/yr) chrome plating; 700 sq ft/yr hard chrome

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plating; 440,000 sq ft/yr electropolishing; 50,000 sq ft/yr-bright dipping; 550,000 sq ft/yr nickel
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plating; and 550,000 sq ft/yr copper plating. The process employed in the manufacturing of these

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products included chrome plating, hard chrome plating" electropolishing, bright dipping, nickel
plating, and copper plating. Raw materials used in the manufacturing of these products are: brass
tube, sheet brass, brass ingot, copper tube, stainless steel tube, and stainless steel sheet. Chemicals
utilized in the manufacturing processes included: sulfuric acid, hydrochloric acid, nitric acid,

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phosphoric and sulfuric acid (Batelle #2067), potassium cyanide, chromic acid, nickel chloride, nickel

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sulfate, boric acid, and prepared cleaners (Oxy-prep #176, #157, #274, #293; Udylite).

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The facility was a large quantity generator of hazardous wastes regulated under the Resource
Conservation and Recovery Act (RCRA). The U.S. EPA hazardous waste generator identification

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number for FMC was WID006090286. Hazardous wastes generated on site were foundry sand and
buffing dusts; which are considered D008 lead from the leaded-brass foundry, and F006 wastewater
treatment sludges from electroplating operations. Other generated hazardous waste included spent
solvents.
The site was initially discovered through a large quantity generator inspection of the FMC
facility by the Wisconsin Department of Natural Resources (WDNR), on September 28, 1993. As a
result of the inspection, FMC received several Notices of Noncompliance.
On October 6, 1993, WDNR conducted a second inspection to collect samples of the foundry
sand. WDNR collected two samples of the foundry sand; the first sample was collected near the
south- blowmatic molder, and the second sample was collected near the eastern end of the building by

2-2

""

the shaker area. Both samples were analyzed by the Wisconsin State Laboratory of Hygiene for
Toxicity Characteristic Leaching Procedure (TCLP) for lead. Both sample results were 37
micrograms per liter (jug/L) TCLP lead. The samples were split with FMC. FMC had their samples
analyzed for TCLP lead by CBC Environmental Laboratories (CBC) of Oak Creek, Wisconsin. The
CBC analytical result for the shakeout area was 37 /j,g/L and the south blowmatjc molder sample
L

result was 28 /ig/L. The analyses confirmed that the waste foundry sand Js'a hazardous waste
(D008), due to TCLP lead results greater than 5 /^g/L. FMC estimated that approximately 20 cubic
yards of waste foundry sand remain in the foundry building. ""^ ,

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To comply with the WDNR closure performance standards, S.NR685.05 (1), May 1994,
FMC contracted the services of Sigma Environmental Services, Inc. (Sigma), to prepare a Closure
Plan for the brass foundry building. The Closure Plan for the brass foundry building was completed
during September of 1994.

„..— . _ . _ .

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The plating facility has been inactive since the company declared, bankruptcy in late 19947 As
of June 30, 1996, FMC owed the County of Kenosha $190,557 in back property taxes. The City and
County of Kenosha, in cooperation with WDNR, have listed the FMC site on the WDNR Brownfield
Environmental Assessment Pilot (BEAP) program. The BEAP program goal for FMC is toljpjojl the "~—, ,- ' .,.••.
property back into productive commercial or industrial use, or for the property to be developed into a 4'iuL ^ -^'multi-use area.

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On May 16, 1996, the Kenosha Fire Department responded to a fire at the FMC facility.
Vandals had set fire to the office area of the main plant building.
On May 20, 1996, representatives from, the Wisconsin Division of Health, Bureau of Public
Health, WDNR, Kenosha County Health Department, and the City of Kenosha visited the FMC site
to determine possible health threats posed by the abandoned <?6mpeaiy in a residential neighborhood.
The Wisconsin Division of Health observed evidence of people trespassing by climbing the fence on
the east, side by the railroad and/or by climbing through an open shed window \ Trespassers entered
the main plant by using a/pool ladder to access the plant roof, and another pool Ikdder from the roof
to access an open area in the plant.

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Chemical hazards were/bbserved by the Wisconsin Division of Health at the FMC site. In
several areas in the main plant, greenish powdered chemicals had been spilled. Barrels of what

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appeared to be plating waste had been tipped onto the floor. In another room, vandals had opened a
valve on an oil tank, which created a slippery oil-covered floor. A number of barrels with unknown
contents were observed throughout the buildings. The plating area had plastic coverings over areas
2-3

where plating operations occurred.
Physical hazards were noted by the Wisconsin Division of Health at the FMC site. The
foundry building contained several trenches with dimensions of 4 feet wide and 4 feet deep. The
main plant contains several sumps with standing water. In the plating area there were sumps
containing standing liquids.
Inhalation exposure could be an issue at the FMC site. Air quality problems may occur from
the spilled plating wastes. Some people in the investigation group noted an odor of sulfuric acid. A
recent iire in the office area left the odor of smoke. No odors were noted outside of the buildings.
^ —
Ingestion exposure could be an issue. I The threat of trespassers unknowingly ingesting
contaminatesx>f which they may have contacted is a potential concern.
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'" June 17, 1996, WDNR requested that the U.S. EPA Region 5 Emergency Response Branch
conduci: a removal assessment for a time-critical removal action at the FMC site. A joint site
reconnaissance was conducted on July 2, 1996, by U.S. EPA On-Scene Coordinator (OSC) Rey
Rivera and WDNR representative John Burnett.

2-4

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Quadrangle Location

ecology and environment, inc.
Region 5 - Superfund Technical Assessment and Response Team
33 North Dearborn, Chicago, Illinois 60602
FIGURE I

TITLE

2-1

Site Location Map
SCALE

SITE

1:24,000

Frost Manufacturing Company
Kenosha
801)11(1

TDD

STATE

CITY

Wisconsin

U.S.G.S. Topographic Map, 7.5' Series
Kenosha Wisconsin Oiiadranple

2-5

S05-9606-022
DATE 1958
REVISED

1971

y • 3. Site Assessment
c_)\ '

START member John Nordine and U.S. EPA OSC Rey Rivera mobilized to the FMC site on
July 24. 1996, to conduct a site assessment. Kietn Lesniak of the U.S. EPA, John Burnett from
WDNR, and Sharon Krewson from the City of Kenosha, participated in the site assessment. The site
assessment included the collection of 10 samples, air monitoring, and photodocumentation. The
weather was partly cloudy, 80° F, and the wind was from the northwest at 10 miles per hour. The
weather changed to rain in the afternoon.
A site safety meeting was conducted and hazards associated with the FMC site were
discussed. A site reconnaissance was conducted to observe site conditions and determine sample
locations (Figure 3-1). During this site reconnaissance, site features were photographed (Appendix
A). Air monitoring was conducted using a 10.2 eV HNU photoionization detector (PID) for
screening organic vapors. Organic vapor readings monitored throughout the site with the PID were
either below or at the background level of 1 part per million (ppm).
... During the reconnaissance, eight sample locations were marked and numerous observations
were made. Two transformer areas were located on the east side of the main plant. All utilities at the
FMC site had been turned off by the City of Kenosha.
Several areas of the FMC site showed signs of vandalism. The lock on the foundry building
i—"'
door ha.d been/pried^off. Windows were broken in all of the buildings. In the alley behind the main
building, several 55-gallon drums had been tipped over, thereby releasing their contents to a storm
drain. Most of the sheds showed signs of vandalism; anything left in the sheds had been thrown to
the ground. In the boiler room, vandals had opened several 55-gallon drums of "Benzene Oil", which
released the oil onto the floor and into a floor drain. A yellow powder had been spilled on the floor
by the entrance to the plating area. In a room near the annealing furnace, two white poly 55-gallon
drums had been tipped over; the first drum contained a bright green liquid and solid with a pH of 0
standard units (S.U.). The remaining drum contained a grey semi-solid material. Vandals had set
fire to the office area of the plant.
3-1

Equipment used for sampling activities included trowels and disposable bailers and spoons.
All equipment was decontaminated prior to use. Equipment was scrubbed with a solution of alconox
and rinsed with potable water. The equipment was thoroughly rinsed with distilled water and air
dried. Site entry equipment did not indicate any readings above background levels during the
collection of environmental samples.
•.

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Sample\Vl_was collected from a sump located in the new water treatment area. Three

samples, V2, SI, and S2, were collected from the plating area; sump Sample V2 was collected from
the liquid in the plating room sump, solid Sample SI was collected from a yellow powder spilled on
the plating room floor, and Sample S2 was collected from green solids near the floor grating system
in the plating room. Samples S3, S4, Dl, and D2 were collected from a room where thirty 55-gallon
drums were stored; Sample S3 was collected from a green solid spilled from an overturned white 55gallon poly drum; Sample S4 was collected from a grey semi-solid white material spilled from an
overturned white 55-gallon poly drum; Sample Dl was collected from a dark green liquid in an 55gallon poly drum, with a field pH test of 0; and Sample D2 was a black liquid collected from a 55gallon poly drum, with a field pH test of 10 to 11. Asbestos sample Al was collected from pieces of
tile that had fallen from the ceiling near the annealing furnace.
All on-site activities concluded after the completion of sampling activities. The samples were
picked up by a courier from VOC Analytical, who delivered the samples to the laboratory, VOC
Analytical, of Naperville, Illinois. An Office of Solid Waste and Emergency Response QA level II
data package was requested under TDD S05-9607-807.
Analytical results were received on August 9, 1996. All of the samples were analyzed for
total RCRA metal and total TCLP metals concentration. Samples SI, S2, S3, Dl, and D2 were
analyzed for pH; sample S4 was analyzed for cyanide; and samples V1,'$X.S4, D|Uan4 D2 were
'. ^,.

analyzed for semivolatile organic compounds.

3-2

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17 Drums
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Superfund Technical Assessment and Response Team

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Solid Sample
Asbestos Sample
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TITLE

' Chicago, Illinois 60602

Site Features/Sample Location Map
STTE
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Frost Manufacturing Company
STATI
cmr
,.,.
Kenosha
Wisconsin
SOUKCE
Ecology and Environment, Inc.
3-3

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Dl

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Sump
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VI

Gate

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Loading dock

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Baghouse

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SCALE

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S05-9606-022
""September 26, 1996

4. ANALYTICAL RESULTS

The sample results are presented in Tables 4-1, 4-2, 4-3, and 4-4. The TCLP chromium
concentrations detected in Samples S3 and Dl exceeded the regulatory requirements of 5 mg/L.
Samples S2, S3, and Dl exhibit the characteristic of corrosivity, with a pH below 2. The validated
QA/QC analytical package is included in Appendix B.

4-1

• \

Table 4-1
CYANIDE, pH, and TOTAL METALS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
Parameter

.p1

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Sample
Identification

Cyanide
(mg/kg)

pH
(S.U.)

Arsenic
(mg/kg)

Barium
(mg/kg)

Cadmium
(mg/kg)

Chromium
(mg/kg)

Lead
(mg/kg)

Mercury
(mg/kg)

Selenium
(mg/kg)

Silver
(mg/kg)

SI

NA

4.5

13

270

3.8

1,600

700

BDL

BDL

1.4

S2

NA

1.0

14

49

BDL

3,500

130

BDL

BDL

BDL

S3

NA

0.00

46

1.5

BDL

6,900

50

0.18

BDL

1.3

S4

BDL

NA

15

43

BDL

4,000

950

BDL

BDL

BDL

Dl

NA

BDL

BDL

BDL

9,000

BDL

BDL

BDL

BDL

D2

NA

BDL

0.24

BDL

19

1.2

0.0041

BDL

BDL

0.00
8.0

Key:
NA = Not analyzed.
BDL = Below detection limit.
mg/kg = Milligrams per kilogram.
S.U. = Standard units.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9606-022.

Table 4-2
TCLP METALS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
Parameter

Sample Identification

Lead
(mg/L)

Chromium
(mg/L)

SI

0.35

BDL

S2

0.60

NA

S3

400

NA

S4

BDL

BDL

Dl

9,000

NA

D2

NA

NA

Key:

NA = Not analyzed.
BDL = Below detection limit.
mg/kg = Milligrams per liter.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9606-022.

4-3

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Table 4-3
VOLATILE ORGANIC COMPOUNDS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
(units = Mg/kg)
Sample Identification
Parameter

VI

V2

2-Butanone

0.13

BDL

Chloroform

0.0060

BDL

4-Methyl-2-pentanone

0.080

BDL

Toluene

0.080

BDL

Styrene

0.0090

BDL

Key:
^g/kg = Micrograms per kilogram.
BDL = Below detection limit.
Source: VOC Analytical. Naperville, 1L. Analytical TDD S05-9606-022.

4-4

Table 4-4
SEMTVOLATILE ORGANIC COMPOUNDS ANALYTICAL RESULTS
FROST MANUFACTURING COMPANY
JULY 24, 1996
(units = ;*g/kg)
Sample Identification
Parameters
bis(2-Ethylhexyl)phthalate
di-n-Octyl phthalate

VI

V2

S4

Dl

D2

2,300

BDL

4.5

130

BDL

240

BDL

BDL

BDL

BDL

Key:
Hg/kg = Micrograms per kilogram.
BDL = Below detection limit.
Source: VOC Analytical, Naperville, IL. Analytical TDD S05-9696-022.

4-5

5. DISCUSSION OF POTENTIAL THREATS

Conditions present at the FMC site that warrant an appropriate removal action as set forth in
paragraph (b) (2) of Section 300.415 of the National Oil and Hazardous Substances Contingency Plan

(NCP) are:

•

Actual or potential exposure to nearby human populations,
animals, or the food chain from hazardous substances or
pollutants or contaminants. The FMC site is located in an industrial
and residential area. The industrial buildings are surrounded by a
chain-link fence; however, this is not sufficient to prevent access by
children, animals, and vandals. Elevated concentrations of TCLP
chromium were detected in Samples S3 and Dl at 400 and 9,000
mg/L, respectively. Chromium is a cumulative toxicant, and the
human exposure conditions of most concern are long-term exposure to
elevated levels in the diet. Samples S2, S3, and Dl, which had pH
levels of 1.0, 0.0, and 0.0, respectively, exhibit the characteristic of
corrosivity as defined by paragraph (a)(l) of 40 Code of Federal
Regulations (CFR) Section 261.21 of the NCP; it is aqueous and has a
pH of less than or equal to 2 or greater than or equal to 12.5; or
paragraph (2), a solid waste that exhibits the characteristic of
corrosivity has the EPA Hazardous Waste Number of D002.

•

Hazardous substances or pollutants or contaminants in drums,
barrels, tanks, or other bulk storage containers, that may pose a
threat of release. Samples collected during the site assessment
indicate that hazardous materials are present on site. Approximately
eighty-four 55-gallon drums, two 30-gallon drums, fourteen 5-gallon
buckets, three 1-gallon pails, and 11 sumps were found on site.
Sample results of some of the drum and vat contents indicate the
presence of plating wastes. Several open 55-gallon drums of
flammable liquids, acids, and unknown contents were observed in the
main plant building and in some of the sheds on site. The drums
pose a potential threat of release.

•

Weather conditions that may cause hazardous substances or
pollutants or contaminants to migrate or be released. The roof of

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5-1

the facility leaks during precipitation events; therefore, the possibility
exists that sumps, pits, and drums that were open could overflow due
to events of heavy precipitation. Freezing temperatures during winter
months may cause a rupture of containers at the site, resulting in a
release.

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The threat of fire or explosion. The office area of FMC was set on
fire by vandals on May 16, 1996. Should another fire occur, the
potential for a rupture of an on-site drum or^cpmtainer exists. The
resulting release would posevhealth risksCto near-by residents.
The unavailability of other appropriate Federal or State response
mechanisms to respond to the release. This factor supports the
propose actions at FMC because WDNR or local officials do not have
the necessary resources to respond to an emergency situation.
Based on the analytical results and site conditions, mitigative actions are necessary at the
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FMC sire
:e to abate potential and imminen
imminent threats to human health and the environment posed by
hazardous conditions present at the site.

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6. PROPOSED REMOVAL ACTIONS

The preferred removal action to mitigate threats associated with the FMC site consists of offsite treatment and disposal of liquid and solid wastes and disposal of nonhazardous solid wastes at a
landfill. The removal actions described in this report directly address actual or threatened releases of
hazardous substances, pollutants, or contaminants at the facility which may pose an imminent and
substantial endangerment to public health and safety, and to the environment..< -The removal action at
U>*> -'j> '-' .- >-• -'-

the FMC site would include consolidating and staging debris; conducting sampling and compatibility
testing on all drums, tanks, pits, sumps, and miscellaneous containers; conducting bulk testing; — bulking all large wastestreams; preparing composite samples and submitting the samples for disposal
bids; transporting waste off site to disposal facilities; conducting soil and concrete sampling; and
excavation and disposal of contaminated soil and concrete, if necessary. An estimate for conducting a
removal action at the FMC site totalling $945,068 was prepared using the Removal Cost Management
System (RCMS) Cost Projection Module, version 4.2 (Appendix C). The following assumptions were
made when preparing the estimate:

The project will be conducted in phases, the first of which will include
preparation of a site safety plan, mobilization of personnel and
equipment, container sampling, compatibility and bulk testing, waste
consolidation, disposal bidding, and a concrete and soil extent of
contamination (EOC) study. This phase is expected to take
approximately 60 working days. The second phase will include
excavation of any contaminated soil and concrete, and transportation
and disposal of all wastestreams. A total of 30 working days will be
required for this phase.
The Emergency Response Cleanup Services (ERCS) contractor rates
will be used for cleanup contractor personnel and equipment costs.
ERCS contractor personnel will consist of one response manager, one
foreman/equipment operator, one field clerk, and five laborers. The
START contractor will include one geologist. One U.S. EPA OSC

6-1

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will be on site at all times.
Wastestreams will include acidic liquids; base/neutral liquids; debris,
including concrete (contaminated and noncontaminated); combustible
liquids; and RCRA-empty containers

.-v
Volumes for liquid wastes were based upon a worst case scenario,
assuming all tanks, drums, and pits were full.
All plating waste will be shipped to disposal facilities for treatment.
The mixed acids wastestream (9,500 gallons) will be shipped in bulk
to Clean Harbors in. Cincinnati, Ohio, at a unit cost of $0.65 per
gallon and a transportation charge of $1,500 per load (2 loads).
Base/neutral liquids (2,000 gallons) will be shipped in bulk to Heritage
in Indianapolis, Indiana, at a unit cost of $0.75 per gallon, and a
transportation cost of $1,300 per load (1 load).
Concrete and soil volumes were estimated using the plating area of the
building (30,000 square feet) with an excavation depth of 6 inches.
An additional 25 % contingency was added to account for soil
contamination beneath the concrete. Based upon file information, this
cost estimate assumes that contaminated soil contains chromium and
lead, which would require treatment prior to landfilling. It is assumed
that the concrete and soil will be transported to the Chemical Waste
Management (CWM) Adams Center Landfill for treatment and
disposal at a cost of $100 per cubic yard and 51,500 per load for
transportation.
Nonhazardous debris and RCRA-empty drums is assumed to be a
special waste. A total volume of 60 cubic yards was assumed to be
transported to a permitted local landfill at a cost of $20 per cubic yard
and a transportation cost of $200 per load.

6-2

L/

Appendix A
Photodocumentation

A-l

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the west side of the main plant building.
1

~"

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the loading dock area of the main plant building

"

>*a^*Wj>

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southeast
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the southwest end of the main plant building.

•• ...^y^u.A.^.,
^^a^^^^J'-^

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The south gate was located along 14th Avenue. Note that access is possible even with the
gate locked.
mv-K^--wvwmw:^w!£-^c*;j;^^

-V

n*tP- 7-24-96 Direction: Northeast

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The north gate was located on 14th Avenue.

Site: Frost Manufacturing Company Date: 1-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the fence along 14th Avenue.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southeast
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the second gate along 14th Avenue.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Up
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Friable ceiling material located above the annealing furnace.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the south side of the plating area.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the north side of the plating area.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: View of the northeast side of the plating area.

•'-I*, W - . . . , , V I

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Northwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: White substance that was spilled on the plating room floor.

::;L.<:-;s.-i*^-*..:Jf-

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Bright green liquid spilled from piping plating room.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Down
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sump located in the plating room.

"-*1- .."•«• <

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample SI collected from a yellow powder that had been spilled near the plating room.

Site- Frost Manufacturing Company Date: 7-24-96

Direction

Site: Frost Manufacturing Company Date: 7-24-96 Direction: —
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample S4 was collected from solids that spilled from a drum.

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample Dl was collected from a liquid in this drum.

Site- Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sample D2 was collected from a liquid from this arum.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Sign on building face "Frost Co. Founded 1902."

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: North gate of Frost Manufacturing Company. Note the gate is locked, but still accessible.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: North side of the brass foundry building along 66th Street.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The west front of the brass foundry building.
(fc'xfi

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The parking area south of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: South
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The southeast gate to the alley was open at the time of the site assessment.

V.*'

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: A view of the alley to the north.

?. V!-

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Three 55-gallon drums that have been tipped over in the alley on the east side of the main
plant building. The drums spilled an oily liquid onto the concrete and into a drain in the alley. Note
the large electrical transformers in background.

••'*,

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: 3,000-gallon vertical tank labeled "acid" located on the east side of the main plant building.

«ttf4

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine

Subject: 2,500-gallon horizontal tank labeled "acid" located on the east side of the main plant
building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The pool ladder used to gain access to the roof of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Southwest
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject:: A second pool ladder used to gain access to the roof of the main plant building.

>

Site: Frost Manufacturing Company Date: 7-24-96 Direction: West
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Two large transformers located on the east side of the main plant building.

Site: Frost Manufacturing Company Date: 1-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Eighteen 55-gallon drums of unknown contents located in a shed east of the main plant
building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: East
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: The north side of the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction:
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Thirty 55-gallon drums located in the main plant. Three of the drums had been tipped over
by vandals, spilling the drums' contents.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: North
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: Seventeen 55-gallon drums and four 5-gallon pails located in the old water treatment area of
the main plant building.

Site: Frost Manufacturing Company Date: 7-24-96 Direction: Unknown
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: 55-gailon drum labeled "Protopet White No. IS, White Petroleum USP Case# 8009-03-8.

Site:: Frost Manufacturing Company Date: 7-24-96 Direction: Unknown
Camera: Olympus Infinity 35mm Photographer: J. Nordine
Subject: One of several pits filled with unknown liquids in the main plant.

Appendix B
Analytical Results

B-l

' -ina .?:ir'rr
International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602

Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DATE:

September 11, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Inorganic Data Quality Review for Toxicity
Characteristic Leaching Procedure (TCLP) Chromium and
Lead, Frost Manufacturing, Kenosha, Kenosha County,
Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four solid samples
collected from the Frost Manufacturing site is complete. The
samples were collected on July 24, 1996, by the Superfund
Technical Assessment and Response Team (START) contractor,
Ecology and Environment, Inc. (E & E) . The samples were
submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846
Methods 1311 and 6010.
Sample Identification
START
Identification No.

SI
S2
S3
S4

recycled paper

Laboratory
Identification No.
L9328-1
L9328-2
L9328-3
L9328-4

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
TCLP Chromium, Lead
Page 2
Data Qualifications:
I.

Sample Holding Time; Acceptable
The samples were collected on July 24, 1996, and analyzed
on August 16, 1996. This is within the 6-month holding
time limit.

II.

Calibration;
Initial Calibration: Acceptable

""*'

Recoveries for the initial calibration verification were
within 90 to 110%, as required.
Continuing Calibration:

Acceptable

All analytes included in the continuing calibration
verification standard were within 90 to 110%, as required.
III.

Blanks;

Acceptable

Calibration and preparation blanks were analyzed with each
analytical batch. No target analytes were detected in the
blanks.
IV.
^r

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

. Inc.
Our Qualm Control Is Your Qualm Assurance

Client #: CHI-96-031I03
Address:

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-1

Ecology and Environment, Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

GN2201; J05-9607-807
Relog of L8736

Parameter

Chromium
Lead

Reportable
Detect
Limit

Results

Units

Method

0.35
BDL

tng/1
mg/1

1311/6010
1311/6010

0.010
0.050

SI
07/24/96
00:00
07/25/96
Client

Extr,
Date

08/14/96 08/16/96
08/14/96 08/16/96

BOL = Below Detection Units
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTH, UScs, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
GAP* 900376G

SUB HRS* 86122,86109,E86048
SC CERT* 96031
TH CERT* 02985
ELPAT* 13301
VA CERT* 00395
HA CERT*-M-FL449
N> CERT* R-148

HRS* £86240,86356
AOEM ID* 40850
NC CERT* 444
CT CERT* PH-0122
CA CERT* 1-1068
AZ CERT* AZ0529
USACE CERT

Respectfully

Analysis
Date
Analys

/

MarincrFernande
nd«<
Laboratory Director
L9328-1

V.O.C. Anaiytkal Laboratories, Inc.
710 East Ogden Avenue, S'."te #104, Napcmlle, Dlinois 60563-8603 • Phone: (708) 35MVOC(8862) • Fix: (708) 3554915

SH
SH

Client #: CHI-96-031103
Address: Ecology and Environment,Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-2

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
—
Collected By:

GN2201; J05-9607-807
Relog of L8736

Parameter

Chromium

Results

Units

0.60

mg/1

Report able
Detect
Limit

Method

1311/6010

0.010

S2
07/24/96
00:00
07/25/96
i
i
Client

Extr.
Date

Analysis
Date
Analys

08/14/96 08/16/96

BOL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All

analyses were performed using EPA, ASTH, USGS, or Standard Methods.

All

analyses were performed within EPA holding times unless otherwise noted.
QAP* 900376C

HRS* £86240,86356

SUB HRS* 86122.86109,E86048

ADEN ID* 40850

SC CERT* 96031

NC CERT* 444

TN CERT* 02985

CT CERT* PH-0122

ElPAT# 13801

CA CERT* 1-1068

VA CERT* 0(1395

AZ CERT* AZ0529

HA CERT* M-FL449

USAGE CERT

Respectfully submitted,

Marino
Laboratory Dired€or
L9328-2

NO CERT* R-148

V.O.C. Analytical Laboratories, Inc.

SH

Client #: CHI-96-031103
Address: Ecology and Environment,Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-3

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

GN2201; J05-9607-807
Relog of L8736

Parameter
Metals
Chromium

Results

400

Units

mg/1

Reportable
Detect
Limit

Method

1311/6010

0.010

S3
07/24/96
00:00
07/25/96

Client

Extr.
Date

08/14/96 08/16/96

SOL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTH, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP* 900376G
SUB HRS* 8612Z.86109.E86048
SC CERT* 96031
TM CERT* 02985
EI.PAT* 13801
VA CERT* 00395
MA CERT* M--FL449
ND CERT* R-148

HRS* £86240,86356
ADEH ID* 40850
NC CERT* 444
CT CERT* PH-0122
CA CERT* 1-1068
AZ CERT* AZ0529
USAGE CERT

Respectfu

MarincfFernande
Laboratory Director
L9328-3

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analys

SH

Client #: CHI-96-031103
Address: Ecology and Environment,Inc.
Ill W. Jackson Blvd.
Chicago, IL 60604
Attn:David Hendren

Page: Page 1 of 1
Date: 08/19/96
Log #: L9328-4

Sample Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

GN2201; J05-9607-807
Relog of L8736

Parameter

Chromium
Lead

Results

Units

BDL
BDL

mg/1
mg/1

Reportable
Detect
Limit

Method

1311/6010
1311/6010

0.010
0.050

S4
07/24/96
00:00
07/25/96

Client

Extr.
Date

08/14/96 08/16/96
08/14/96 08/16/96

BDL ~ Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All

analyses were performed using EPA, ASTH, USGS, or Standard Methods.

All analyses were performed within EPA holding times unless otherwise noted.

Respectfully subm

QAP* 900376G

MRS* £86240,86356

SUB MRS* 86122,86109,E86048

AOEH ID* 40850

SC CERT* 96031

NC CERT* 444

TN CERT* 02985
ELPAT* 13801

CT CERT* PH-0122
CA CERT* 1-1068

Marifeo' Fernandjkr •

VA CERT* 00395

AZ CERT* AZ0529

Laboratory Director

HA CERT* M-FL449

USAGE CERT

-—*}

NO CERT* R-U8

L9328-4

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analys-

SH
SH

?coiogy and envir
international Specialists in the Environment

LJ
^

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/573-9243, Fax: 312/578-9315

M E M O R A N D U M
DATE:

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Organic Data Quality Review for Volatile Organic
Compounds, Frost Manufacturing, Kenosha, Kenosha
County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of two liquid waste
samples collected from the Frost Manufacturing site is complete.
The samples were collected on July 24, 1996, by the Superfund
Technical Assessment and Response Team (START) contractor,
Ecology and Environment, Inc. (E & E). The samples were
submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
8240.
Sample

Identification

START
Identification No.

Laboratory
Identification No.

VI
V2

L8736-1
L8736-2

Data Qualifications:
I.

sample Holding Time:

Acceptable

The samples were collected on July 24, 1996, and analyzed
on July 31, 1996. This is within the 14-day holding time
limit.

recycled paper

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
VOA
Page 2
II.

Gas Chromatoaraphy/Mass Spectrometry CGC/MS) Tuning;
Acceptable
GC/MS tuning to meet ion abundance criteria using
bromofluorobenzene (BFB) were acceptable and samples were
analyzed within 12 hours of BFB tuning.

III.

Calibrations:
• Initial Calibration; Acceptable
A five-point initial calibration was performed prior to
analysis. All average response factors were greater than
0.05. The percent relative standard deviations (%RSDs)
between response factors were less than 30% for all
detected target compounds.
• Continuing Calibration; Acceptable
The percent differences of the response factors were less
than 25%, as required for detected target compounds.

IV.

Blank: Acceptable
A method blank was analyzed with the samples. No target
compounds or contaminants were detected in the blank.

V.

Internal Standards; Acceptable
The areas of the internal standards in the samples were
within -50% to +100% of the associated calibration check
standard. The retention time of the internal standard was
within the 30-second control limit.

VI.

Compound Identification; Qualified
The mass spectra of detected target compounds was not
provided by the laboratory; therefore, all reported
compound have been qualified "N" .

VII.

Additional QC Checks;

Acceptable

The recoveries of the surrogates used in the samples and
blank were within laboratory-established guidelines.

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
VOA
Page 3
VIII. Overall Assessment of Data for Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April
1990), Data Validation Procedures, Section 5.0, VOAs By
GC/MS analysis. Based upon the information provided, the
data are acceptable for use, with the above-stated
qualifications.
Data Qualifiers and Definitions;
"*•""'

N - Presumptive evidence of presence of material.

International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312;578-92t3, Fax: 312/578-9345
M E M O R A N D U M

DATE:

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Organic Data Quality Review for Semivolatile
Organic Compounds, Frost Manufacturing, Kenosha,
Kenosha County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and one
solid waste samples collected from the Frost Manufacturing site
is complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor, Ecology and Environment, Inc. (E & E). The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
8270.
Sample Identification
START
Identification No.

VI
V2
S4
Dl
D2

recycled paper

Laboratory
Identification No.
L8736-1
L8736-2
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
SVGA
Page 2
Data Qualifications:
I.

Sample Holding Time: Acceptable
The samples were collected on July 24, 1996, extracted on
July 31, 1996, and analyzed on August 2, 1996. Sample S4
was analyzed on August 7, 1996. This is within the 14-day
holding time limit, from collection to extraction and 40day limit from extraction to analysis.

II.

Gas Chromatography/Mass Spectrometry (GC/MS) Tuning;
Acceptable
• GC/MS tuning to meet ion abundance criteria using
decaf luorotriphenylphosphine (DFTPP) were acceptable and
samples were analyzed within 12 hours of DFTPP tuning.

III.

Calibrations;
• Initial Calibration; Qualified
A five-point initial calibration was performed prior to
analysis. All average response factors were greater than
0.05 except benzidine; therefore, the nondetect values for
this compound have been flagged "R", as required. The
percent relative standard deviations (%RSDs) between
response factors were less than 30% for all detected target
compounds .

• Continuing Calibration;

Acceptable

The percent differences of the response factors were less
than 25%, as required for detected target compounds.
IV.

Blank:

Acceptable

A method blank was analyzed with the samples. No target
compounds or contaminants were detected in the blank.
V.

Internal Standards:

Acceptable

The areas of the internal standards in the samples were
within -50% to +100% of the associated calibration check
standard. The retention time of the internal .standard was
within the 30-second control limit.

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
SVGA
Page 3
VI.

Compound Identification;

Qualified

The mass spectra of detected target compounds were not
provided by the laboratory; therefore all reported
compounds have been qualified "N".
VII.

Additional PC Checks; Acceptable
The recoveries of the surrogates used in the samples and
blank were within laboratory-established guidelines.

<•*•/

VIII. Overall Assessment of Data for Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April
1990), Data Validation Procedures, Section 4.0 BNAs By
GC/MS analysis. Based upon the information provided, the
data are acceptable for use, with the above-stated
qualifications.
Data Qualifiers and Definitions;
N - Presumptive evidence of presence of material.
R - The sample results are rejected (analyte may or may not
be present) due to gross deficiencies in quality control
criteria. Any reported value is unusable. Resampling
and/or reanalysis is necessary for verification.

ecology and env«rt)nnie^: k
International Specialists in the Environment

.
•.

j
^

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-9345

M E M O R A N D U M
DAT!-::

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Inorganic Data Quality Review for Resource
Conservation and Recovery Act (RCRA) Metals, Frost
Manufacturing, Kenosha, Kenosha County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and four
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor, Ecology and Environment, Inc. (E & E). The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846
Methods 6010 and 7471.
Sample Identification

START
Identification No.
VI
V2
Si
S2
S3
S4
Dl
D2

recycled oaoer

Laboratory
Identification No.
L8736-1
L8736-2
L8736-4
L8736-5
L8736-6
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Prolect TDD S05-9506-022
Analytical TDD S05-9607-807
RCRA Metals
Pago 2
Data Qualifications:
I.

Sample Holding Time;

Acceptable

The samples were collected on July 24, 1996, and analyzed
on July 27 to 29, 1996. Analysis for mercury was performed
on July 16, 1996. This is within the 6-month (28 days for
mercury) holding time limit.
II.

Calibration;
'

Initial Calibration; Acceptable

Recoveries for the initial calibration verification were
within 90 to 110% (80 to 120% for mercury), as required.
The correlation coefficient for mercury exceeded 0.995.
Continuing Calibration; Acceptable
All analytes included in the continuing calibration
verification standard were within 90 to 110% (80 to 120%
for mercury), as required.
III.

Blanks:

Acceptable

Calibration and preparation blanks were analyzed with each
analytical batch. No target analytes were detected in the
blanks.
IV.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

ecology and environjne-IT, (n
international Specialists m the Environment

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-93':5

M E M O R A N D U M
DATE:

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Miscellaneous Data Quality Review for pH and
Asbestos, Frost Manufacturing, Kenosha, Kenosha
County, Wisconsin

REFERENCE:

Project TDD S05-9606-022
Project PAN 6N2201SIXX

Analytical TDD S05-9607-807
Analytical PAN 6UAG01TA

The data quality assurance (QA) review of four liquid and four
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor, Ecology and Environment, Inc. (E & E). The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United States
Environmental Protection Agency (U.S. EPA) Solid Waste 846 Method
9045 and EPA method 150.1.
Sample Identification
START
Identification No.
VI
V2
SI
S2
S3
S4
Dl
D2

Laboratory
Identification No.
L8736-1
L8736-2
L8736-4
L8736-5
L8736-6
L8736-7
L8736-8
L8736-9

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
pH, Asbestos
Page 2
Data Qualifications:
I.

Sample Holding Time; Acceptable
The samples were collected on July 24, 1996, and analyzed
on August 7, 1996. The Office of Solid Waste and Emergency
Response (OSWER) Directive 9360.4-01 (April 1990) does not
provide holding times for these parameters.

II.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Data Validation Procedures,
Section 9.0, Generic Data Validation Procedures. Based
upon the information provided, the data are acceptable for
use.

««*'

ecology and env^
International Specialists in the Environment

33 North Dearborn Street
Chicago, Illinois 60602
Tel. 312/578-9243, Fax: 312/578-9345
M E M O R A N D U M

DATE:

September 2, 1996

TO:

John Nordine, START Project Manager, E & E, Chicago,
Illinois

FROM:

David Hendren, START Analytical Services Manager,
E & E, Chicago, Illinois

THROUGH:

Mary Jane Ripp, Assistant START Program Manager,
E & E, Chicago, Illinois

SUBJECT:

Inorganic Data Quality Review for Cyanide, Frost
Manufacturing, Kenosha, Kenosha County, Wisconsin

REFERENCE:

Project TDD S05-9606-022 Analytical TDD S05-9607-807
Project PAN 6N2201SIXX Analytical PAN 6UAG01TA

The data quality assurance (QA) review of two liquid and one
solid samples collected from the Frost Manufacturing site is
complete. The samples were collected on July 24, 1996, by the
Superfund Technical Assessment and Response Team (START)
contractor, Ecology and Environment, Inc. (E & E) . The samples
were submitted to V.O.C. Analytical, Naperville, Illinois. The
laboratory analyses were performed according to the United states
Environmental Protection Agency (U.S. EPA) Method 335.3.
Sample Identification
START
Identification No.

VI
V2
S4

Laboratory
Identification No.
L8736-1
L8736-2
L8736-7

Data Qualifications:
I.

Sample Holding Time; Acceptable
The samples were collected on July 24, 1996, and analyzed
on August 7, 1996. This is within the 14-day holding time.

recycled paper

Frost Manufacturing
Project TDD S05-9506-022
Analytical TDD S05-9607-807
Cyanide
Page 2
II.

Calibration: Acceptable
The correlation coefficient of the initial calibration
curve exceeded 0.995. Recoveries of continuing
calibrations were within 85-110%.

III.

Overall Assessment of Data For Use;

Acceptable

The overall usefulness of the data is based on criteria for
QA Level II as outlined in the Office of Solid Waste and
Emergency Response (OSWER) Directive 9360.4-01 (April 1990)
Data Validation Procedures, Section 3.0, Metallic Inorganic
Parameters. Based upon the information provided, the data
are acceptable for use.

Our Qualm Control Is Ynur Qualllv Assurance

Client #: CHI-96-031104
Address:
Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 6
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Compounds
N-Nitrosodim«thylamine
BDL
Aniline
BDL
Phenol
BDL
Bis(2-Chloroethyl) Ether
BDL
2-Chlorophenol
BDL
l,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Benzyl alcohol
BDL
1,2-Dichlorobenzene
BDL
2-Methylphenol
BDL
Bis(2-Chloroisopropyl) Ethe
BDL
* N-Nitrosodi-n-propylamine
BDL
4-Methylphenol
BDL
Hexachloroethane
BDL
Nitrobenzene
BDL
Isophorone
BDL
2-NitrophenoL
BDL
2,4-Dimethyl Phenol
BDL
Bis(2-Chloroethoxy) Methane
BDL
Benzoic Acid
BDL
N-Nitrosodiethylamine
BDL
2.4-Dichlorophenol
BDL
1,2,4-Trichlorobenzene
BDL
Naphthalene
BDL
4-Chloroaniline
BDL

rnits

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

ug/1
ug/1
ug/1

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

Reportable
Detect
Limit

190
160
250
170
170
260
180
220
280
120

880
290
210
220
170
230
210
110
150
2000
280
260
130
230
670

VI Sump-H2O Treat
07/24/96

13 :30
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
J».nar

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
OB/02/96
OB/02/96
OB/02/96
OB/02/96
OB/02/96
OB/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
OB/02/96
08/02/96
08/02/96

V.O.C. Analytical Laboratories, Inc.

710 East Ogdcn Avenue, Z jite #104, Napemlle, Illinois 60563-8603 • Phone: (708) 3554VOC(8862) • Fu: (708) 35S4915

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

EP
EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client ft: CHI - 96-031104
Address: Ecology and Environmenc
Ecology and Environmenc
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of
Date: 0 8 / 0 9 / 9 6
Log #: L 8 7 3 6 - 1

Sajnple Description:
6N2201
KJ5100

Parameter

Results

:3em±volatile Organic Compounds
Hexachlorobutadiene
'-Chloro-3-Me~hylphenol
,,^-Methylnapht/ialene
2-Methylnaphtaalene
Hexachlorocyclopentadiene
2,4,6-T'richlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
DimethylphthaLate
2,6-Dinitroto Luene
Acenaphthylene
3-Nitroaniline
Acenaphthene
Oibenzofuran
2,4-DinitrotoLuene
2,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
Fluorene
^
-Chlorophenyl-phenylether
4-Nitroaniline
4,6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine

Azobensiene
4-Bromophenyl-phenylether
alpha-BHC

Hexachlorobenzene
Pentachlorophenol

gamma-BHC
beta-BHC
PhenanUhrene
Anthracene
delta-BHC
Carbazole

Heptachlor

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

Reportable
Detect
Limit

190
120
120
260
340
210
500
100
220
150
220
170
1000
120
130
2000
2000
2000
910
100
100
2000
2000
190
120
210

150
160
1000
140
210
120
160
140
1000
210

V.O.C. Analytical Laboratories, Inc.

VI Sump-H20 Treat
07/24/96
13:30
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client tt: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
A t t n : Dave Hendren

Page: Page 3 of
Date: 0 8 / 0 9 / 9 6
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Units

(continued)
Organic Compounds
BDL
Di-n- butyl phthalate
ug/1
BDL
"' Idrin
ug/1
BDL
ug/1
BDL
Heptachlor Epoxide
ug/1
BDL ,
Benzidine
ug/1
BDL
Pyrene
ug/1
BDL
Endosulfan I
ug/1
BDL
ug/1
4 , 4 ' -DDE
BDL
Dieldrin
ug/1
BDL
ug/1
4 , 4 ' -ODD
BDL
Endosulfan II
ug/1
BDL
Endrin Aldehyde
ug/1
BDL
Endrin
ug/1
BDL
Butylbenzylphl;halate
ug/1
BDL
Endosulfan Sulfate
ug/1
BDL
ug/1
4 , 4 ' -DDT
BDL
Sndrin Ketone
ug/1
BDL
ug/1
Benzo (a) anthracene
BDL
3 , 3 ' -Dichlorobenzidine
ug/1
BDL
Chrysene
ug/1
BDL
ug/1
, 2-Diphenylhydrazine
2300
ug/1
3is (2-Ethylhexyl) Phthalate
240
ug/1
3i-n-octyl ph~halate
BDL
ug/1
Benzo (b) f luoranthene
BDL
ug/1
Benzo (k.) f luoranthene
BDL
ug/1
Benzo (a) pyrene
BDL
ug/1
Indeno ( 1 , 2 , 3 - c , d) pyrene
BDL
ug/1
Dibenzo (a, h) Anthracene
BDL
ug/1
Benzo ( g , h , i) perylene
BDL
ug/1
PCB 1016
BDL
ug/1
PCB 1221
BDL
ug/1
PCB 1232
BDL
ug/1
PCB 1242
BDL
ug/1
PCB 1254
BDL
ug/1
PCB 1260
BDL
ug/1
Chlordane

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

160
220
150
240
2000
120
340
370
230
220
1100
1600
200
120
130
210
1000
120
480
150
110
600
240
590
200
100
520
690
520
6000
6000
6000
6000
6000
6000
2000

V.O.C. Analytical Laboratories, Inc.

VI Sump-H20 Treat
07/24/96
13 :30
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
TO

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 4 of
Date: 08/09/96
Log #: L8736-1

Sample Description:
Label:

6N2201
KJ5100

J05-9607-807

Parameter

Date Sampled:
Time Sampled:
Date Received:
Collected By:

Results

Units

Method

Reportable
Detect
Limit

VI Sump-H20 Treat
07/24/96

13 :30
07/25/96

Client

Extr.
Date

Analysis
Date
Analyst

Samivolatile .Organic Compounds
( continued)
Toxaphene
BDL
ug/1
' lution Factor
•
100

3510/8270
3510/8270

4000

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

Metals
Arsenic
Barium
Cadmium
Chromium.
Lead
Mercury
Selenium
Silver

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245.2
3010/6010A
3010/6010A

10
1.0
1.0
1.0
1.0
0.10
1.0
1. 0

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0. 0050
0.0050
0.0050

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

Organic Compounds
Dichlorodif luoromethane
Ethanol
Chlorome thane
Vinyl Chloride
Bromomethane
^Moroethane
^ichlorof luoromethane
Acrolein.
1, 1-Dichloroethene
Acetone
lodomethane
Carbon Disulfide
Methylene Chloride
Acrylonitrile
Trans -1,2- dichloroethene
1, 1-Dichloroechane
Vinyl Acetate
2-Butanone
Chloroform
1, 1, 1-Trichloroethane
Carbon Tetrachloride
Benzene

BDL
5. 4
BDL
540
57
0.11
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.13 •
0.0060

BDL
BDL
BDL

mg/l

mg/1
mg/l
mg/1
mg/l
mg/l
mg/l
mg/l

mg/kg
5030/8240
mg/kg ' 5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
5030/8240
mg/kg
mg/kg
5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
5030/8240
mg/kg
mg/kg
5030/8240
5030/8240
mg/kg
mg/kg
5030/8240
mg/kg
5030/8240
5030/8240
mg/kg
5030/8240
mg/kg
mg/kg
5030/8240
mg/kg
5030/8240
mg/kg
5030/8240
5030/8240
mg/kg

V.O.C. Analytical Laboratories, Inc.

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 5 of
Date: 08/09/96
Log #: L8736-1

Sajnple Description:
6N2201
KJ5100

Parameter
Volatile Organic Compounds
1 , 2 -Dichloroei:hane
'"richloroetheiie
m.,. , 2 -Dichloropropane
Dibromome thane
Bromodichlorornethane
2-Chloroethylvinyl Ether
Cis-1, 3-Dichloropropene
4 -Methyl - 2 -pentanone
Toluene
Trans-1, 3-Dichloropropene
Sthyl Methacrylate
1,1, 2 -Trichloroethane
2-Hexanone
Dibromochlorome thane
Chlorobenz ene
Ethylbenzene
Total Xylenes
Styrene
Bromoform
"7is-l, 4-dichloro-2-butene
^,1,2, 2 -Tetrachloroethane
1,2,3 -Trichloropropane
Trans-1 , 4-dichloro-2-butene
MTBE
1,1,1,2 -Tetrachloroethane
Cis-1, 2-Dichloroethene
Tetrachloroethene
1 , 2 -Dibromoethane
1, 2-Dibromo-3-Chloropropane
Dilution Factor

Cyanide
pH

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results

Units

Method

(continued)
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.080
0.080
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.0090
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1.0

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

BDL
3.0

mg/l

Reportable
Detect
Limit

335.3
150.1

V.O.C. Analytical Laboratories, Inc.

VI Sump-H20 Treat
07/24/96
13 :30
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

0.010
0.10

08/07/96 08/07/96
08/07/96 08/07/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

INO
INO

Client ft: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment:
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Paqe 6 of 6
Date: 08/09/96
Log #: L8736-1

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results

Parameter
General Chemistry

Units

Method

Reportable
Detect
Limit

VI Sump-H20 Treat
07/24/96
13 :30

07/25/96
Client

Extr.
Date

(continued)

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses; were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses; were performed within EPA holding times unless otherwise noted.
QAP# 9 0 0 3 7 6 3

HRS# £ 8 6 2 4 0 , 8 6 3 5 6

SUB HRStt 86122,86109,E86048

ADEM IDtt 4 0 8 5 0

SC CERTtt 96031

NC CERTS

TN CERT* 02985

CT CERTtt P H - 0 1 2 2

Respectfully submrtt

f

444

ELPATtt 13801

CA CERTtt 1-1068

VA CERTtt 00395

AZ CERTtt AZ0529

MA CERTtt M-FL449

USACE CERT

Marine
Laboratory Dire"c"Eor
L8736-1

ND CERTtt R-148

V.O.C. Analytical Laboratories, Inc.

Analys i s
Date
Analyst

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 6
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

V2 Sump-Platinq
07/24/96
14 :00
07/25/96
Client

Reportable
Parameter

Results

Units

Method

Detect
Limit

Extr.
Date

Analysis
Date
lHial;

Compounds
N-Nitrosodimethylamine
Aniline

BDL
BDL

Phenol

BDL

Bis(2-Chloroethyl) Ether
2-Chlorophenol

BDL
BDL

1,3-Dichlorobenzene

BDL

1,4-Dichlorobenzene
Benzyl alcohol

BDL
BDL

1,2-Dichlorobenzene

BDL

^-Methylphenol
(2-Chloroisopropyl) Ethe

BDL
BDL

N-Nitrosodi-n-propylamine
4-Methylphencl
Hexachloroeth.ane

BDL
BDL
BDL

Nitrobenzene

BDL

Isophorone
2-Nitrophenol
2,4-Dimethyl Phenol
Bis(2-Chloroethoxy) Methane
Benzoic Acid

BDL
BDL
BDL
BDL
BDL

N-Nitrosodiet:hylamine

BDL

2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline

BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19

16
25
17
17
26
18
22
28
12
88
29
21
22
17
23
21
11
15
200
28
26
13
23
67

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31 /c>6
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of
Date: 03/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Parameter

Results

ttamivolatile
Organic Compounds
Hexachlorobutadiene
4 -Chloro- 3 -Met:hylphenol
•Methylnaphthalene
.; -Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthy1ene
3-Nitroaniline
Acenaphthene
Dibenzofuran
2,4-Dinitrotoluene
2,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
Fluorene
-Chlorophenyl-phenylether
'""-f-Nitroanilims
4,6-Dinitro-2-Methylphenol
N-Nitrosodiph«nylamine
Azobenzene
4-Bromophenyl--phenylether
alpha-BHC

Hexachlorobenzene
:?entachlorophenol
gamma-BHC

beta-BHC
Phenanthrene
Anthracene
delta-BHC
Carbazole
Heptachlor

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

V2 Sump-Plating
07/24/96
14 :00
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI- 96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren
Sample
6N2201
KJ5100

Page: Page 3 of
Date: 08/09/96
Log #: L8736-2

Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

JC5-96U 7-807

Parameter

Results

Units

(continued)
Semi volatile Organic:: Compounds
BDL
Di-n-butylphthalate
ug/1
BDL
Aldrin
ug/1
BDL
ug/1
"luorarithene
BDL
ug/1
'"""keptachlor Epoxide
BDL
ug/1
Benzidine
BDL
ug/1
Pyrene
BDL
ug/1
Endosulfan I
BDL
ug/1
4,4'-DDE
BDL
ug/1
Dieldrin
BDL
ug/1
4,4'-DDD
BDL
ug/1
Endosulfan II
BDL
ug/1
Endrin Aldehyde
BDL
ug/1
Endrin
BDL
Butylbenzylphthalate
ug/1
BDL
ug/1
Endosulfan Sulfate
BDL
ug/1
4,4'-DDT
BDL
ug/1
Endrin Ketone
BDL
ug/1
Benzo(a)anthracene
BDL
ug/1
3,3'-Dichlorobenzidine
BDL
ug/1
Chryserie
BDL
ug/1
',2-Diphenylhydrazine
BDL
ug/1
%*6is(2-Ethylhexyl)Phthalate
BDL
ug/1
Di-n-octyl phthalate
BDL
ug/1
Benzo(b)fluoranthene
BDL
ug/1
Benzo(k)fluoranthene
BDL
ug/1
Benzo(a)pyrene
BDL
ug/1
Indeno(1,2,3-c,d)pyrene
BDL
ug/1
Dibenzo(a,h)Anthracene
BDL
ug/1
Benzo(g,h,i)perylene
BDL
ug/1
PCB 1016
BDL
ug/1
PCB 1221
BDL
ug/1
PCB 1232
BDL
ug/1
PCB 1242
BDL
ug/1
PCB 1254
BDL
ug/1
PCB 1260
BDL
ug/1
Chlordane

Method

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/3270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

Reportable
Detect
Limit

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
43
15
11
60
25
59
20
10
52
69
52
600
600
600
600
600
600
200

V.O.C. Analytical Laboratories, Inc.

V2 Sump-Plating
07/24/96
14:00
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment:
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 4 of
Date: 08/09/96
Log #: L8736-2

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

B Suits

Units

:3amivolatile Organic-Compounds
(continued)
Toxaphene
BDL
ug/1
Dilution Factor
10
Volatile Organic Compounds
Dichlorodifluoromethane
Ethanol

Chloromethane
Vinyl Chloride
Bromomethane

Chloroethane
Trichlorofluoromethane
Acrolein
1,1-Dichloroethene
Acetone
lodomethane
Carbon Disulfide
Methylene Chloride
Acrylonitrile
Trans-1,2-dichloroethene
l,1-Dichloroethane

inyl Acetate
- Butanone
Chloroform

1,1,1-Trichloroethane
Carbon Tetrachloride
Benzenes
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Dibromomethane
Bromodichloromethane
2-Chloroethylvinyl Ether
Cis-1,3-Dichloropropene
4 -Methyl - 2 -pe;ntanone
Toluene
Trans-l,3-Dichloropropene

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
3DL

BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

V2 Sump-Plating
07/24/96
14 :00
07/25/96
Client

Extr . Analysis
Date
Date
Anal

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
4.0
10
1.0
1.0
1.0
1.0

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

V.O.C. Analytical Laboratories, Inc.

1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Client #: CHI- 96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
A t t n : Dave Hendren

Page: Page 5 of
Date: 0 8 / 0 9 / 9 6
Log #: L 8 7 3 6 - 2

Sample Description:
6N2201
K.J5100

Parameter
Volatile Organic Compounds
Ethyl Methacrylate
1,1,2-Trichloroethane
^2-Hexanone
Dibromochloromethane
Chlorobenzeru;
Ethylbenzene
Total Xylenes
Styrene
Bromoform
Cis-l,4-dichloro-2-butene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Trans-1,4-dichloro-2-butene
MTBE
1,1,1,2-Tetrachloroethane
Cis-l,2-Dichloroethene
Tetrachloroethene
1, 2-Dibromoei:hane
1, 2-Dibromo-3-Chloropropane
Dilution Factor
Cyanide

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results
(continued)
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1.0

BDL

Units

Method

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240
5030/8240

mg/1

335.3

Reportable
Detect
Limit

V.O.C. Analytical Laboratories, Inc.

1. 0
1.0
1.0
1. 0
1.0
1.0
1. 0
1.0

1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

0.010

V2 Sump -Plating
07/24/96
14:00
07/25/96
Client

Extr . Analysis
Analyst
Date
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

08/07/96 08/07/96

KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS
KS

INO

Client #: CHI-9S-031104
Address: Ecology and Environment
Ecology and Environment
111 w7"Jackson Blvd.
Chicago, IL 6 0 6 0 4
Attn: Dave Hendren
Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results

Parameter
Ganeral Chemistry

Page: Page 6 of 6
Date: 0 ^ / 0 9 / 9 6
Log #: L8736-2

Units

Method

Reportable
Detect
Limit

V2 Sump-Plating
07/24/96
14:00
07/25/96

Client

Extr.
Date

(continued)

1DL = 3elow Detection Limits
Compounds are Screened Only, w i t h an estimated detection l i m i t .
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAPtt 900376G

MRS* £86240,86356

SUB KRStt 86122.86109,E86048

ADEM ID» 40850

SC CERTtt 96031

NC CERTS 444

TN CERTtt 02985

CT CERT* PH-0122

ELPATtt 13801

CA CERTtt 1-1068

VA CERTtt 00395

AZ CERTtt AZOS29

MA CERTtt M-Ft*49

USAGE CERT

Marino Fernandei
Laboratory Director
L8736-2

ND CERTtt R-148

V.O.C. Analytical Laboratories, Inc.

Analysis
Date
Analyst

Our Qualm/ Control Is Your Quality Assurance

Client #: Cffl-96-031104
Address: Ecology & Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: David Hendren

Page: Page 1 of 1
Date: 08/08/96
Log#: L8736-3

Sample Description:

Label: Al
Date Sampled: 07/24/96
Time Sampled: 14:10
Date Received: 07/25/96
Collected By:
Client

Bulk: Asbestos ID

Extraction Date: 07/30/96
Analysis Date: 07/30/96

Description

Present

Method

Homogeneous
sample

% Cellulose

Ceiling tile

no

EPA-600/PLM

No

20-25%

% Nonfibrous % Fibrous Glass
Material

70-75%

2-5%

Color

cream

Respectfully submitted,

Marino Fernandez
Laboratory Director

V.O.C. Analytical Laboratories, Inc.

710 East Ogden Avenue, Suite #104, NaperviUe, Illinois 60563-8603 • Phone: (708) 35S*VOC(8862) • Fix: (708) 3554915

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 1
Date: 08/09/96
Log #: L8736-4

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver

Results

Units

13
270
3.8

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

1600
700
BDL
BDL
1.4

Reportable
Detect
Limit

Method

SI Yellow Powder
07/24/96

14:00
07/25/96

Client

Extr.
Date

Analysis
Date
Analyst

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5.0
1.0
1.0
1.0
1.0
0.10
1.0
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

9045

0 .10

08/07/96 08/07/96

JK
JK
JK
JK
JK
JK
JK
JK

.;:-OieiBiBtr3fx:;
4.5

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAPtt 900376G
SUB HRStt 86,122.86109,E86048
SC CERTtt 9J.031
TN CERTtt 0::985
ELPATtt 138CI1
VA CERTtt 0(1395
MA CERT* M--FM49

HRStt £ 8 6 2 4 0 , 8 6 3 5 6
ADEM ID* 40850
NC CERTtt 444
CT CERTtt PH-0122
CA CERTtt 1-1068
AZ CERTtt AZ0529
USAGE CERT

Marino Fernand
Laboratory Director
L8736-4

NE> CERTtt R--H8

V.O.C. Analytical Laboratories, Inc.

INO

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 1
Date: 08/09/96
Log #: L8736-5

Sample Description:
6N2201
KJ5100

Parameter

Mfetals-.. "

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Results

Units

Reportable
Detect
Limit

Method

32 Plating Room FL
07/24/96
14:15
07/25/96
Client

Extr.
Date

Analysis
Date
Analyst

'::;:;•;' " ;

Arsenic
Barium

Cadmium
Chromium
Lead
Mercury
Selenium
Silver

14

49
BDL
3500
130
BDL
BDL
BDL

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5.0
1.0
1.0
1. 0
1.0
0.10
10
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

9045

0.10

08/07/96 08/07/96

JK
JK
JK
JK
JK
JK
JK
JK

General Chenu stry
1.0

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP» 90Q37.5G
SUB HRStt 8'5122. 86109, E86048

HRSft E86240,B6356
ADEM ID* 40850

SC CERTtt 9S031
TO CERTtt 02985

NC CERTtt 444

ELPATtt 13801
VA CERTS 00395
MA CERTtt M-FL449
ND CERTtt R-148

CT CERT* PH-0122
CA CERTS 1-1068
AZ CERTIt AZ0529
USAGE CZRT

Respectfully

Marino Fernandez
Laboratory Director
L8736-5

V.O.C. Analytical Laboratories, Inc.

INO

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 6 0 6 0 4
Attn: Dave Hendren

Page: Page 1 of 1
Date: 0 8 / 0 9 / 9 6
Log #: L 8 7 3 6 - 6

S.ample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter
M^|ii:ix:?;:'''-:l:::-r:-:;^.. \ : :"Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver

Results

Units

46
1.5
BDL

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

6900
50
0.18
BDL
1.3

S3 Drum Spill Area
07/24/96
15:00
07/25/96
Client

Reportable
Detect
Limit

Extr.
Date

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5.0
1.0
5.0
1.0
1.0
0.10
10
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

9045

0.10

08/07/96 08/07/96

Method

Analysis
Date
Analys07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

General: -ChoniBtry
0.00

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
CAPS 9003T6G
SUB HRSS E6122,86109.E86048
SC CERTS S6031
TN CERTtt 02985
ELPATS 13801
VA CERT* (10395
MA CERTtt H-FL449
ND CERTtt It-14 8

HRStt E86240, 86356
ADEM IDS 40850
NC CERTS 444
CT CERTtt PH-0122
CA CERTS 1-1068
AZ CERTS AZ0529

Marino Fernandez
Laboratory Director

USACE CERT
L8736-6

V.O.C. Analytical Laboratories, Inc.

INO

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 4
Date: 08/09/96
Log #: L8736-7

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:

J05-9607-807

S4 Drum Spill Area
07/24/96

15:15

07/25/96
Collected By: Client

Parameter

Results

Organic Compounds
N-Nitrosodimethylamine
BDL
Aniline
BDL
Phenol
BDL
Bis(2-Chloroethyl) Ether
BDL
2-Chlorophenol
.
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Benzyl alcohol
BDL
l,2-Dichlorobenzene
BDL
2-Methylphenol
BDL
Bis(2-Chloroisopropyl) Ethe
BDL
"•H^N-Nitrosodi-n-propylamine
BDL
4-Methylphenol
BDL
Hexachloroethane
BDL
Nitrobenzene
BDL
Isophorone
BDL
2-Nit3rophenol
BDL
2,4-Dimethyl Phenol
BDL
3is(2-Chloroethoxy) Methane
BDL
Benzoic Acid
BDL
N-Nitrosodiethylamine
BDL
2,4-Dichlorophenol
BDL
1,2,4-Trichlorobenzene
BDL
Naphthalene
BDL
4-Chloroaniline
BDL

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

Method

Reportable
Detect
Limit

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

V.O.C. Analytical Laboratories, Inc.

0.33
0.10
0.10
0.17
0.27
0.10
0.10
0.26

2.1
0.39
0.35
0.59
0.42
0.28
0.26
0.27
0.21
0.20
0.15
0.50
0.10
0 .14
0.49
0.16
0.10

Extr.
Date

03/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date
JSinai-

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of
Date: 0 8 / 0 9 / 9 6
Log #: L 8 7 3 6 - 7

Sample Description:
6N2201
KJ5100

Label: S4 Drum Spill
Date Sampled: 0 7 / 2 4 / 9 6
Time Sampled: 15:15
Date Received: 0 7 / 2 5 / 9 6

J05-9607-807-

Collected By: Client

Parameter

Results

Samivolatile Organic Compounds
HexachlorobuUadiene
4-Chloro-3-M«thylphenol
l-Methylnapht:halene
-Msthylnaphuhalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2 , 4 , 5 -Trichlcjrophenol
2-Chloronapht;halene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotcjluene
Acenaphthyleiie
3-Nitroaniline
Acenaphthene
Dibenzofuran
2,4-Di:aitrotoluene
2 , 4 - D init ropheno1
4-Ni tropheno1
Diethylphthalate
Fluorene
4-Chlorophenyl-phenylether
_i-Nitroaniline
4,6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine
Azobenzene
4-Bromopheny L-phenylether
alpha-BHC
Hexachlorobenzene
Pentachlorophenol
gamma-BHC
beta-BHC
Phenanthrene
Anthracene
delta-BHC
Carbazole
Heptachlor

Units

(continued)
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg

Method

Reportable
Detect
Limit

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

0.10
0 . 10
0.10
0 . 10
0.32
0.20
0 . 19
0.25
0.31
0.10
0.14
0.10
0.23
0.26
0.10
0.15
0.60
0.18
0.10
0.25
0.16
0.10
0.26
0.28
0.36
0.70
0.66
0.25
0.29
0.40
0.1S
0.15
0.20
0.16
0.20
0.44

V.O.C. Analytical Laboratories, Inc.

Extr.
Date

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
06/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

EP
EP

EP
EP
EP
EP
EP
EP
EP
EP

EP

Client #: CHI- 96 - 031104

Address:

Page: Page 3 of
Date: 08/09/96
Log #: L8736-7

Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Sample Description:
Label: S4 Drum Spill Area
6N2201
KJ5100

J05-9607-o07

Date Sampled: 07/24/96
Time Sampled: 15 :15
Date Received: 07/25/96
Collected By: Client

Parameter

Semivolatile -Organic; Compounds
Di-n-butylphthalate
Aldrin
P
luoranthene
,ptachlor Epoxide
tfenzidine
Pyrene
Endosulfan I
4,4'-DDE
Dieldrin
4,4'-ODD
Endosulfan II
Endrin Aldehyde
Endrin
Butylbenzylphthalate
Endosulfan SuJ.fate
4,4'-DDT
Endrin Ketone
Benzo(a)anthracene
3,3' -Dichlorobenzidine
Chrysene
1,2-Diphenylhydraz ine
.s(2-Ethylhexyl)Phthalate
n-octyl phthalate
3enzo(b)fluoranthene
3enzo(k)fluoranthene
Benzo (alpyrenca
IndenoCl,2,3-c,d)pyrene
Dibenzo (a, h) Anthracene
Benzo(g,h,i)perylene
PCS 1016
PCB 1221
PCS 1232
PCB 1242
PCB 1254
PCB 1260
Chlordane

ssults

Units

(continued)
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
4.5 '
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg
BDL
mg/kg

Method

Reportable
Detect
Limit

3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270
3550/8270

V.O.C. Analytical Laboratories, Inc.

0.21
0.16
0.34
0.27
0.27
0.39
0.50
0.12
0.17
0.57
0.30
0.25
0.22
0.26
0 .24
0.18
0.20
0.51
0.52
0.22
0.10
0.51
0.22
0.42
0.54
0.28
0.24
0.77
0.10

2.0
2.0
2.0
2.0
2.0
2.0
0.67

Extr.
Date

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06,'2G

08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96

Analysis
Date
Anal

08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96
08/07/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-95-031104
Address:: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Paae 4 of
Date: ,'8/09/96
Log #: L8736-7

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Units

Samivolatile Organic Compounds
(continued)
Toxaphene
BDL
mg/kg
Dilution Factor
1.0

.petals
Arsenic

15

Barium

Cadmium
Chromium

Lead
Mercury
Selenium
Silver

mg/kg
mg/kg

43
BDL
4000
950
BDL
BDL
BDL

mg/kg
mg/kg
mg/kg

BDL

mg/kg

mg/kg
mg/kg

mg/kg

Reportable
Detect
Limit

Method

S4 Drum Spill Area
07/24/96
15:15
07/25/96
Client

Extr.
Date

Analysis
Date
Analys'

3550/8270
3550/8270

1.5

08/06/96 08/07/96
08/06/96 08/07/96

EP
EP

3050/6010
3050/6010A
3050/6010A
3050/6010
3050/6010A
7471
3050/6010A
3050/6010A

5.0
1.0
1.0
1.0
1.0
0.10
10
1.0

07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96
07/27/96

07/31/96
07/29/96
07/29/96
07/31/96
07/29/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

0 .10

08/07/96 08/07/96

Chemi. stry

Cyanide

335.3

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAPtt 900375G
SJB HRS» 86122.86109,E86048
SC CERT* 96031

MRS* £86240,86356
ADEM ID* 40850
NC CERTtt 444

TN CERT* 02985

CT CERTtt PH-0122
CA CERTtt 1-1068

ELPATtt 13801
VA CERT* 003*9 5
MA CERT* P-FL449
NT! CERTtt R-148

AZ CERTtt AZ0529
USAGE CERT

Marino P^rnandez_
Laboratory Director
L8736-7

V.O.C. Analytical Laboratories, Inc.

INO

Client #: CHI- 96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 1 of 4
Date: 08/09/96
Log #: L8736-8

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Semivolatile•:Organic Compounds
N-Nitrosodime:thylamine
BDL
Aniline
BDL

Phenol
Bis(2-Chloroethyl) Ether

BDL
BDL

2-Chlorophenol

BDL

1, 3-Dichlorobenzene
1,4-Dichlorobenzene

BDL
BDL

Benzyl alcohol

BDL

1,2-Dichlorobenzene

BDL

2-Methylphenol
Bis(2-Chloroisopropyl) Ethe

BDL
BDL

;-Nitrosodi-ri-propylamine
4-Methylphenol
Hexachloroethane
Nitrobenzene

BDL
BDL
BDL
BDL

r

Isophorone

BDL

2-Nitrophenol

BDL

2,4-Diraethyl Pheno1
Bis(2-Chloroethoxy) Methane

BDL
BDL

Benzoic Acid
N-Nitrosodie-hylamine
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene

BDL
BDL
BDL
BDL
BDL

4-Chloroaniline

BDL

Fnits

ug/1
ug/1
ug/1
ug/1
ug/1

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19

16
25
17
17
26
18
22
28
12
88
29
21
22
17
23
21
11
IS
200
28
26
13
23
67

Dl Drum: 55 Gal BLJ
07/24/96
14 :45
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
J\jial;

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address?: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of
Date: 08/09/96
Log #: L8736-8

Sample Description:
6N2201
KJ5100

Label: Dl Drum:
Date Sampled: 0 7 / 2 4 / 9 6
Time Sampled: 14 :45
Date Received: 0 7 / 2 5 / 9 6

J05-9607-807

55 Gal PLF

Collected By: Client

Parameter

Results

Send.volatile:: Organic Compounds
Hexachlorobuf.adiene
4-Chloro-3-Methylphenol
n
.-Methylnapht:halene
-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronapht:halene
2-Nitroaniline
Dimethylphthalate
2,6-Di:nitrotoluene
Acenaphthy1ene
3-Nitroaniline
Acenaphthene
Dibenzofuran
2, 4-Di.nitrotoluene
2,4-Dinitrophenol
4-Nitropheno!.
Diethylphthalate
Fluorene
4 -Chiorophenyl-phenylether
ti - Ni t roani 1 ine
4,6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine
Azobenzene
4 -Bromopheny L-phenylether
alpha-BHC
Hexachlorobenzene
Pentachlorophenol
gamma-BHC
beta-BHC
Phenanthrene
Anthracene
delta-BHC
Carbazole
Heptachlor

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

EP
EP

EP
EP
EP
EP
EP
EP
EP
EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104

Address:

Page: Pacre 3 of
Date: 08/09/96
Log #: L8736-8

Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Kendren

Sample Description:
6N2201
KJ5100

Label: Dl Drum: 55 Gal 51.

Date Sampled: 07/24/96
Time Sampled: 14 :45

J05-9607-807

Date Received: 07/25/96
Collected By: Client

Parameter

Results

3ftmivolatile Organic Compounds
Di-n-butylphthalate
Aldrin
Fluoranthene
^^Heptachlor Epoxide
Benzidine
Pyrene
Endosulfan I
4,4'-DDE
Dieldrin
4,4'-ODD
Endosulfan II
Endrin Aldehyde
Endrin
Butylbenzylphthalate
Endosulfan Sulfate
4,4'-DDT
Endrin Ketone
Benzo(a)anthracene
3,3'-Dichlorobenzidine
Chrysene
1,2-Diphenylhydrazine
^Bis(2-Ethylhexyl)Phthalate
Di-n-octyl phthalate
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(l,2, 3 -c,d)pyrene
Dibenzo(a,h)Anthracene
Benzo(g, h,i)perylene
PCS 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1254
PCB 1260
Chlordane

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL .,
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
130
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
48
15
11
60

25
59
20
10
52
69
52
600
600
600
600
600
600
200

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/35
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
03/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104

Address:

Page: Page 4 of
Date: 08/09/96
Log #: L8736-8

Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Units

Samivclatile Organic Compounds
(continued)
Toxaphene
BDL
ug/1
Dilution Factor
10
petals
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
©itoeral:-"them! stry
pH

BDL
BDL
BDL
9000
BDL
BDL
BDL
BDL

mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1

0.00

Reportable
Detect
Limit

Method

Dl Drum: 55 Gal BLF
07/24/96
14 :45
07/25/96

Client

Extr.
Date

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245.2
3010/6010A
3010/6010A

20
1.0
2. 0
1.0
1. 0
0.10
1.0
1.0

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

0.10

08/07/96 08/07/96

150.1

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAP# 900376G
SUB HRStt 86122,86109,E86048
SC CERTS 96031
TN CERTtt 02985
ELPATtt 13801
VA CERTtt 0033S
PA CERTtt N - F L 4 4 9

HRStt E 8 6 2 4 0 , 86356
ADEM IDtt 40850
NC CERTtt 444
CT CERTIt PH-0122
CA CERTtt 1-1068
A2 CERTIt AZ0529

Analysis
Date
JAnal

Marino Fernandez
Laboratory Director

USAGE CERT
L8736-8

NU CERTtt R - 1 4 8

V.O.C. Analytical Laboratories, Inc.

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/31/96
07/29/96
07/29/96

INO

Client #: C H I - 9 6 - 0 3 1 1 0 4
Address:
Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 6 0 6 0 4
A t t n : Dave Hendren
Sajnple
6N2201
KJ5100

Page: Page 1 of
Date: 0 8 / 0 9 / 9 6
Log #: L 8 7 3 6 - 9

Description:
Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Semivoliitile Organic Compounds
N-Nitrosodime-ihylamine
BDL
Aniline
BDL
Phenol
BDL
Bis (2-Chloroe'ihyl) Ether
BDL
2-Chlorophenol
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Benzyl alcohol
BDL
1,2-Dichlorobenzene
BDL
2-Methylphenol
BDL
Ms (2-Chloroisopropyl) Ethe
BDL
^^-Nitrosodi-n-propylamine
BDL
4-Methylphenol
BDL
Hexachloroethane
BDL
Nitrobeinzene
BDL
Isophorone
BDL
2 -Ni tropheno1
BDL
2,4-Dimethyl Phenol
BDL
Bis(2-Chloroethoxy) Methane
BDL
Benzoic Acid
BDL
N-Nitrosodiethylamine
BDL
2,4-Dichlorophenol
BDL
l,2,4-Trichlcrobenzene
BDL
Naphthalene
BDL
4-Chloroaniline
BDL

Units

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
16
25
17
17
26
18
22
28
12

88
29
21
22
17
23
21
11
15
200
28
26
13
23
67

D2 Drum: 55 Gal BLK
07/24/96

15 :15
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
JUnal;

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 2 of 4
Date: 08/09/96
Log #: L8736-9

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

iiBmivolatile: Organic Compounds

Hexachlorobutadiene
4-Chloro-3-Methylphenol
-Methylnaphtinalene
Methylnaphthalene
'^fexachlorocycLopentadiene
2,4, 6-Trichlorophenol
2, 4 , 5-Trichlorophenol
2-Chloronaphtnalene
2-Nitrcaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthylens
3-Nitroaniline
Acenaphthene
Dibenzofuran
2,4-Dinitrotoluene
2,4-Dinitrophenol
4-Nitrophenol
Diethylphthalate
:?luorene
4-Chlorophenyl-phenylether
Ni t raani1ine
, 6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine
Azobenzene
4-Bromophenyl-phenylether
alpha-BHC
Hexachloroben.zene
Pentachlorophenol
gamma-BHC
beta-BHC
Phenanthrene
Anthracene
delta-BHC
Carbazole
Heptachlor

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1

BDL
BDL

BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL

ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1
ug/1

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

19
12
12
26
34
21
50
10
22
15
22
17
100
12
13
200
200
200
91
10
10
200
200
19
12
21
15
16
100
14
21
12
16
14
100
21

D2 Drum: 55 Gal BLJ
07/24/96
15 :15
07/25/96
Client

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
. 07/31/96
07/31/96
07/31/96
07/21/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Page 3 of 4
Date: 08/09/96
Log #: L8736-9

Scimple Description:
6N2201
KJ5100

Label: D2 Drum: 55 Gal BLr"
Date Sampled: 0 7 / 2 4 / 9 6
Time Sampled: 15:15
Date Received: 0 7 / 2 5 / 9 6
Collected By: Client

J05-9607-607

Parameter

Results

Semivolatile Organic Compounds
Di-n-butylphthalate
Aldrin
^luoranthene
*2ptachlor Epoxide
Benzidine
Pyrene
Endosulfan I
4,4'-DDE
Dieldrin
4,4'-DDD
Endosulfan II
Endrin Aldehyde
Endrin
Butylbenzylphthalate
Endosulfan Sulfate
4,4'-DDT
Endrin Ketone
Benzo(a)anthracene
3,3'-Dichlorcbenzidine
Chrysene
1,2-Diphenylhydrazine
is(2-Ethylhexyl)Phthalate
Di-n-octyl phthalate
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indenod, 2, 3-c,d)pyrene
Dibenzo(a,h)Anthracene
Benzo (g,h, Dperylene
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 1254
PCB 1260
Chlordane

Units

(continued)
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/1
BDL
ug/l
BDL
ug/l
BDL
ug/1
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l
BDL
ug/l

Method

Reportable
Detect
Limit

3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270
3510/8270

V.O.C. Analytical Laboratories, Inc.

16
22
15
24
200
12
34
37
23
22
110
160
20
12
13
21
100
12
48

15
11
60

25
59
20
10
52
69
52
600
600
600
600
600
600
200

Extr.
Date

07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/95
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96
07/31/96

Analysis
Date
Analyst

08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96
08/02/96

EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP
EP

Client #: CHI-96-031104
Address: Ecology and Environment
Ecology and Environment
111 W. Jackson Blvd.
Chicago, IL 60604
Attn: Dave Hendren

Page: Paae 4 of 4
Date: "8/09/96
Log #: L8736-9

Sample Description:
6N2201
KJ5100

Label:
Date Sampled:
Time Sampled:
Date Received:
Collected By:

J05-9607-807

Parameter

Results

Units

Samivolatile Organic: Compounds
(continued)
Toxaphene
BDL
ug/1
Dilution Factor
10

Arsenic

BDL
0.24
BDL
19
1.2
0.0041
BDL
BDL

Barium
Cadmium

Chromium
Lead
Mercury
Selenium

Silver
Siineral Chem-tstry
PH

mg/1

mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1

8.0

Reportable
Detect
Limit

Method

D2 Drum: 55 Gal ELY
07/24/96
15:15
07/25/96
Client

Extr. Analysis
Date

Date

3510/8270
3510/8270

400

07/31/96 08/02/96
07/31/96 08/02/96

EP
EP

3010/6010A
3010/6010A
3010/6010A
3010/6010A
3010/6010A
245 .2
3010/6010A
3010/6010A

0.10
0.10
0.10
0.10
0.10
0.0010
0.10

07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96
07/29/96

08/01/96
07/29/96
07/29/96
08/01/96
08/01/96
07/31/96
07/29/96
07/29/96

JK
JK
JK
JK
JK
JK
JK
JK

0.10

08/07/96 08/07/96

150.1

0.10

BDL = Below Detection Limits
* Compounds are Screened Only, with an estimated detection limit.
All analyses were performed using EPA, ASTM, USGS, or Standard Methods.
All analyses were performed within EPA holding times unless otherwise noted.
QAPtt 900375G
SUB HRStt

85122.86109,E86048

SC CERTtt 96031
TN CERTtt 02985
ELPATtt 13801
VA CERTS 00335
MA CERTtt M-FL449
ND CERTtt R - 1 4 8

tted,

HRSIt £ 8 6 2 4 0 , 8 6 3 5 6
ADEM ID* 4 0 8 5 0
NC CERTtt 444
CT CERTtt P H - 0 1 2 2
CA CERTS 1-1068
AZ CERTtt AZ0529

Analyst

Marino Fernandez
Laboratory Director

USACE CERT
L8736-9

V.O.C. Analytical Laboratories, Inc.

INO

V

Cost Summary
Page:

Projection Name: Frost Manufacturing

Date: 09/18/96

Projection Type: Initial

Prime Contractor: RES5

Projection

Archive

Total

CONTRACTOR
Personnel Cost

335824

0

Equipment Cost

46881

0

46881

Other Direct Cost

204531

0

204531

Toi:al for Contractor

587236

Contractor Contingency:15.00%

335824

587236

88085

Including Contractor Contingency

675321

Sii:e Contingency: 20 . 00%

117447

Including Site Contingency

792769

GOVERNMENT
Personnel Cost

110650

Equipment Cost

0

0

16266

16266

126916

126916

Otier Direct Cost

Toral for Goverment

Site Contingency:

20.00%

Including Site Contingency

PROJECT TOTAL

110650

25383

152299

945068

COSTS BY TASK CODE PORTION OF THE COST ESTIMATES
5 PAGES

HAS BEEN REDACTED

NOT RELEVANT TO THE SELECTION OF THE REMOVAL ACTION