Ecology and Environment, Inc., Site Assessment Report

Ecology and Environment, Inc., conducts a site assessment at the Kenosha Iron and Metal site, evaluating human health and environment threats.

254310

1994-08-09 00:00:00.0

WID988574257

Kenosha Iron and Metal

PDF

Ecology and Environment, Inc.,

Administrative Record

Site Assessment

text

Human health

Environment

Kenosha Iron and Metal site

Environmental reporting

Midwest

Ecology and Environment, Inc.,

City of Kenosha

1994-08-09

Ecology and Environment, Inc.,

City of Kenosha

Copyright undetermined

eng

Kenosha, Wisconsin

PDF

EPA Region 5 Records Ctr.

254310

SITE ASSESSMENT REPORT
FOR
KENOSHA IRON AND METAL
U.S. EPA ID: WID988574257
88 ID: NA
TDD: T05-9403-013B
PAN: EWI0423SAA

ecology and environment, inc.
International Specialists in the Environment

SITE ASSESSMENT REPORT
FOR
KENOSHA IRON AND METAL
,S. EPA ID: WID988574257
SS ID: NA
TDD: T05-9403-013B
PAN: EWI0423SAA

August 9, 1994

Prepared by:

Date:.

Reviewed by:

Date:.

Approved by

Date:

ecology and environment, inc.
111 WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
recycled paper

TABLE OF CONTENTS
Section

Page

1.0

INTRODUCTION

1

2.0

SITE DESCRIPTION

1

3.0

SITE BACKGROUND

1

4.0

SITE ASSESSMENT

5

5.0

ANALYTICAL RESULTS

8

6. 0

DISCUSSION OF POTENTIAL THREATS

15

6.1 Potential Exposure to Hazardous Substances...
6.2 Migration of Contaminants
6. 3 Weather Conditions

15
15
15

7.0

REMOVAL ACTION

16

8.0

ESTIMATED COST

16

Appendix
A

PHOTO LOG

A-l

B

DATA QUALITY ASSURANCE REVIEW

B-l

C

XRF 920 FIELD DATA

C-l

D

FASP LABORATORY PCB DATA

D-l

E

RCMS 4.0 COST ESTIMATE

E-l

LIST OF TABLES

Table

Page

1

ANALYTICAL DATA FOR TOTAL METALS

12

2

ANALYTICAL DATA FOR TCLP METALS

13

ANALYTICAL DATA FOR PCBs

14

3 & 4

LIST OF FIGURES

Figure

Page

1

SITE LOCATION MAP

2

2

SITE FEATURES MAP

3

3

SAMPLE LOCATION MAP

6

4

XRF 920 LEAD DATA FOR SITE SOILS

9

5

XRF 920 CHROMIUM DATA FOR SITE SOILS

10

6

FASP PCB DATA FOR SITE SOILS

11

1. 0

INTRODUCTION

Ecology & Environment, Inc. (E & E) , Technical Assist ?nce
Team (TAT) was tasked by the United States Environmental
Protection Agency (U.S. EPA) to conduct an site assessment under
Technical Directive Document (TDD) T05-9403-013 at the Kenosha
Iron and Metal (KIM) site and evaluate threats to human health
and the environment.
The site assessment was conducted in two phases: the first phase
on March 30, 1994, was to collect soil samples for chemical
analysis; and the second phase on May 9 through 12, 1994, was to
conduct a extent of contamination survey. The following report
provides a summary of these activities.
2.0

SITE DESCRIPTION

The KIM Site is located at 5512-5514 19th Avenue, Kenosha,
Kenosha County, Wisconsin (87° 37' 55" north, 41° 52' 50" west;
see Figure 1, Site Location Map) . The KIM site is located in an
industrial and low-income residential area. The facility is a
1.3 -acre abandoned scrap yard that was used for the reclamation
of batteries and metals and consists of an empty lot covered with
sparse vegetation with metal and other debris mixed with the
soil. A school is located on 55th Street approximately 100 feet
to the north and a second school is located two blocks south of
the site.
The site is unsecured, and the southeast corner of the property
is used as a shortcut for area residents and students of the two
nearby schools. The shortcut runs from 19th Avenue near the
Chicago and North Western railroad tracks to an empty lot at 1919
55th Street.
The scrap yard is
and by industrial
and North Western
scrap yard. East

bordered on the north and west by residences
property to the east and south. The Chicago
Railroad tracks border the south side of the
of the scrap yard is 19th Avenue.

Activities at the KIM site included the purchase and acceptance
of scrap metal, followed by sorting, sizing, and resale. Both
ferrous and non-ferrous metals were handled, with ferrous metals
being handled in the yard and non-ferrous metals handled in a
former warehouse. This warehouse and other on-site buildings
have been removed. Operation ceased at the site approximately in
the mid-1980' s.
3.0 SITE BACKGROUND
The property had been reportedly used for industrial purposes for
40 years. Prior to its use as a scrap yard, the property was

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SITE LOCATION MAP
KENOSHA IRON & METAL
STATl

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T05-9403-013

QUADRANGLE LOCATION
USGS TOPO QUADRANGLE KENOSHA

REVISED

971

FIGURE 2
SITE FEATURES MAP
KENOSHA IRON & METAL KENOSHA, WISCONSIN
MARCH AND MAY 1994
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used as a coal storage yard by the Chicago Northwest Railway
Company (CNRCO). In 1948, CNRCO conveyed the property by quit
claim deed to the M & R Land Company. In 1955, the M & R Land
Company conveyed the property by warranty deed to Maurice sabin
as trustee. Sabin is a trustee of a land trust that now holds
title to the property. Sabin identified the current owners of
the land as Max Wolkomir, Shirley Halper, and Dorothy Berenson.
Reportedly the site was used as a scrap yard by a Mr. Ruppa from
an unknown date until 1983. In 1983, Sabin conveyed the property
by land contract to Harold R. and Roy M. Federman. In a letter
dated November 8, 1991, Harold Federman informed the Wisconsin
Department of Natural Resources (WDNR) that he had not fully
executed the land contract with trustee Sabin and that as a
result the ownership of the property reverted back to Sabin.
The Kenosha County Register of Deeds lists the Federmans as the
current owners. The tax key number of the property is 12-223-31334-021. According to county records the property is abandoned
and tax delinquent.
During its operation as a scrap yard, the KIM site reportedly
accepted batteries, electrical transformers, and ferrous and nonferrous metals for purchase and resale.
In 1988, an environmental consultant, Canow, Conibear &
Associates, LTD. (CCA), was retained by the City of Kenosha,
Wisconsin, to conduct an asbestos survey at the KIM Site. The
survey was performed on July 27, 1988. The survey included a
building with a connecting garage, a second building, and the
yard area. A total of 53 bulk asbestos samples were collected.
No asbestos-containing material was found in either of the
buildings. However, asbestos material was found on pipes in the
yard, in tile insulation, and in one soil sample.
In August, 1988, an environmental consultant, Foth & Van Dyke,
was retained by the City of Kenosha to perform an Environmental
Site Assessment (ESA) of the KIM site. The ESA included a legal
description of the property and the collection and analysis of 43
soil samples from 9 soil borings. The analytical results of the
soil samples indicated elevated concentrations of lead up to
2,900 parts per million (ppm) and polychlorinated biphenyls
(PCBs) up to 102 ppm. The Foth & Van Dyke report found that
there was evidence of significant environmental impairment at the
KIM site.
In 1990, the City of Kenosha razed and removed two buildings onsite. The city also removed deteriorating fencing, a concrete
scale, and metal debris. The asbestos-containing material was
removed with the debris.

On September 28, 1993, WDNR performed a Screening Site Inspection
(SSI) at the KIM site. The SSI included the collection of 18
soil samples fr-->m t^>e site and from private residences. The
results of the soil sampling at private residences indicated
elevated concentrations of cadmium (52.0 ppm and 61.6 ppm), and
lead (1,070 ppm). Soil samples collected on-site contained
concentrations of chromium (35,500 ppm), lead (3,380 ppm), and
total PCBs (1,140,000 parts per billion (ppb)).
WDNR representatives interviewed residents of properties
bordering the site, who indicated that following episodes of
heavy precipitation, there is significant runoff from the site to
the north and into the storm sewer on 55th Street that discharges
into Kenosha Harbor. According to census data gathered by WDNR,
the KIM Site is on the border between the Columbus Park census
tract (39% of the population below the federal poverty level),
and the Washington Park census tract (27.5% of the population
below the federal poverty level).
4.0

SITE ASSESSMENT

On March 30, 1994, TAT members John Nordine and Nabil Fayoumi met
with U.S. EPA On-Scene-Coordinator (OSC) Charles Gebien and Bill
Ramsey of WDNR at the KIM site. A site safety meeting was held
and the potential hazards of the site were discussed. A site
reconnaissance of the KIM site was completed, which included a
tour of the facility (see Appendix A for Site Photo Log).
To characterize the possible hazardous substances on-site the TAT
collected 15 soil samples, including a duplicate sample (see
Figure 3 Sample Location Map). Several sampling locations that
were chosen were close to previous WDNR sampling locations, from
WDNR's September 1993 site inspection, to provide confirmation of
previous sampling results. All soil samples were collected from
1 to 6 inches in depth with a shovel and/or a trowel. Prior to
sample collection the sampling equipment was washed with a brush
and a solution of alconox and distilled water and triple rinsed
with distilled water.
Soil sample SI was collected from the backyard of a residential
property at 2007 55th Street near a shed, 12 feet from the
southeast corner of the foundation. The sample location was near
the location of WDNR soil sample S01/S02. Soil sample S2 was
collected 40 feet east of the alley, in the southwest corner of
the site. Soil sample S3 was collected 27 feet south of the
southwest corner of the shed of the 2007 55th Street property.
Sample S3 was also collected WDNR samples S17 and S18. Soil
sample S4 was collected from the backyard of 1933 55th Street,
along the west fence 5 feet north of the southwestern corner of
the property boundary. The location of soil sample S4 was also
near the location WDNR soil sample S04. Soil sample S5 was

FIGURE 3 SAMPLE LOCATION MAP
KENOSHA IRON & METAL. KENOSHA, WISCONSIN
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WCNH SAMPLE LOCATION 9/28/93

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collected 48 feet south of the southeast corner of house at 1933
55th Street. Soil sample S6 was collected 6 feet south of the
southeast corner of the house at 1929 55th Street. Soil sample
S7 was collected 79.8 feet south of the fence in line with the
air conditioner of the house at 1929 55th Street. The location
of soil sample S7 was also near the location WDNR soil sample
S13.
Soil sample S8 was collected 108 feet south of the fence line in
line with the southwest corner of the house at 1929 55th Street.
Soil sample S9 was collected 21.5 feet from the private fence
line in line with the air conditioner of the house at 1933 55th
Street. Soil sample S9 was also collected near the location of
WDNR sample WS15. Soil sample S10 was collected 14 feet south of
the midpoint of the south side of the house at 1923 55th Street
foundation. The location of soil sample S10 was also near the
location of WDNR soil sample S20. Soil sample Sll was collected
53 feet south of the midpoint of the foundation of the house at
1913 55th Street, also near WDNR soil sample S12. Soil sample
S12 was collected 27 feet south of the southwest corner of the
house at 1913 55th Street in the path. Soil sample S13 was
collected 26 feet southeast of the corner of the foundation of
the house at 1913 55th Street. Soil sample S13 was also
collected near WDNR soil sample WS11. Soil samples S14 and S15
were collected 31 feet west of the light pole in the southeast
corner of the site, in the on-site path. Soil sample S14 and S15
was also collected near WDNR soil sample WS9. Soil sample S14
was a duplicate of soil sample S15.
The March 1994, soil samples were analyzed by Quality Analytical
Labs, Inc., 1938 C University Lane, Lisle, Illinois. The soil
samples were analyzed for total metals (samples SI through S15),
Toxicity Characteristic Leaching Procedure (TCLP) for metals (SI
through S15), and PCBs (S2 through S10 and S13). Samples SI
through S15 were screened with a X-ray fluorescence (XRF) metal
analyzer.
A site-specific model was developed for the KIM Site.
The analytical data from soil samples SI through S15 for total
metals and the XRF screening data was used to developed a site
specific model. The following metals present at the site were
used in the model: barium, chromium, lead, and mercury.
XRF spectroscopy is a non-destructive qualitative and analytical
technique used to determine the elemental composition of samples.
As the XRF analyzes a sample, a spectrum of x-rays is generated
by all of the elements in the sample. Because a distinct x-ray
is emitted for each type of electron orbital transition, each
element will have many characteristic peaks in the spectrum. The
XRF instrument uses a multichannel microprocessor to collect the
x-ray spectrum given off by the sample, statistically processes
the data, and makes a qualitative identification and nondefinitive measurement of the elements present.

On May 2, 1994, the KIM site TDD was amended to require an
extent-of-contamination survey to be conducted so that a removal
action plan may be prepared. The survey would determine what
t=oils should be removed. The XRF Ottokompu Model 920 detector
(XRF 920) would be used to screen soil samples for site-specific
metals. The Field Analytical Support Program (FASP) mobile
laboratory, using a Varian 3400 gas chromatography with electron
capture detector would be used to screen the soil samples for
PCBs.
On May 9 through 12, 1994, TAT members John Nordine and Nabil
Fayoumi met with U.S. EPA On-Scene-Coordinator (OSC) Charles
Gebien and WDNR representative Bill Ramsey at the KIM site to
conduct phase II of the site assessment. A site safety meeting
was held and the potential hazards of the site were discussed.
An extent-of-contamination survey was conducted. The site was
divided into a grid with a spacing of 25 feet between grid
points.
Soil samples were collected at the nodes to a maximum depth of 2
feet. The soil samples were collected using either a pesthole
digger, a hand auger, a pick, and/or trowel. Prior to sample
collection the sampling equipment was washed with a brush and a
solution of alconox and distilled water and triple rinsed with
distilled water. Two samples were collected at each node point
of the grid, from 0 to 1 foot and 1 to 2 feet in depth. Samples
were not collected at depths greater than 2 feet due to buried
metal debris.
Each sample was screened using the XRF 920 to determine the
content of barium, chromium, lead, and mercury (see Figures 4 and
5, also see Appendix C for XRF data). The soil samples were also
screened for PCBs at the FASP mobile lab (see Figure 6 and
Appendix D for FASP PCB Data). Selected soil samples were sent
to Heritage Laboratories, Inc., 1319 Marquette Drive, Romeoville,
Illinois, for PCB, pesticides, and herbicides analysis.
5.0

ANALYTICAL

RESULTS

Results of the TAT collected samples revealed the presence of
Total Resource Conservation and Recovery Act (RCRA) metals;
Toxicity Characteristic Leaching Procedure (TCLP); and PCBs (see
Appendix B for data quality assurance review). See Tables 1, 2,
3, and 4 for summaries of analytical data results.
For soil samples collected in March 1994, sampling results for
total metals indicated cadmium (120 ppm) in sample S2; chromium
(12,000 ppm) in sample S10; lead (12,000 ppm) in sample S13; and
mercury (5.4) in sample S3. TCLP metals results indicated
cadmium at 1.0 milligrams per liter (mg/1) in sample S13 and lead
at 43 mg/1 in sample S13. Total concentrations of PCBs in soils
results ranged from 6.2 to 55 ppm in samples S9 and S10.

8

FIGURE 4
XRF 920. LEAD DATA FROM SOIL SAMPLES, MAY 1994
KENOSHA IRON & METAL. KENOSHA. WISCONSIN

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XRF 920, CHROMIUM DATA FROM SOIL SAMPLES, MAY 1994
KENOSHA IRON & METAL KENOSHA, WISCONSIN
LEGEND

FIGURES
FASP PCS DATA FOR SOIL SAMPLES, MAY 1994
KENOSHA IRON & METAL KENOSHA, WISCONSIN
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TABLE 1
ANALYTICAL DATA FOR TOTAL METALS
AT THE KBNOSHA IRON i METAL SITE
KBN08HA, WISCONSIN
MARCH 30, 1994

SAMPLE
AMBER
PARAMETER

SI

S2

ARSENIC

U

U

IAR1UM

510

CADMIUM

60

CHROMIUM
LEAD
4ERCURY

500
2,300

1.6

m
;**'

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37

58

S9

S10

S11

S12

S13

S14

S15*

U

U

U

U

U

U

U

5.2

U

500

760

650 2,400

400

540

700

1,000

730

880

21

91

51

55

38

45

98

19

25

56 1,100

880

350 12,000

450

210

7,500

130

160

2,200 2.200 2,500 12,000 1,300

1,700

SS

S6

U

U

870 1.000 200

850

86

11

84

430 1,400

50

280

120

U

U
6.3

t,200 4.000 S80
0.62

5.4 0.27

78

5,400 1,100 4,900 2,300 5.000
0.73

0.13

0.91

1.2

0.7

0.4

0.93

0.73

0.47

SELENIUM

U

U

U

U

U

U

U

U

U

U

U

U

U

SILVER

U

U

U

U

U

U

U

U

U

U

U

U

U

Units - parts per m i l l i o n (ppra)
U = Non Detect
* Duplicate soil sample of S14

12

2.7

24
U

2.9

U
U

TABLE 2
ANALYTICAL DATA FOR TCLP METALS
AT THE KENOSHA IRON & METAL SITE
KENO8HA, WISCONSIN

March 30, 1994
SAMPtf
HUMER
'AMMETER

61

52

iB
-: •?$>

lit-

w

55

86

S7

$8

S9

$10

S11

S12

S13

$14

S15*

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LEVEL

CADMIUM

0.008

0.65

0.41

0.051

0.63

U

0.54

0.19

0.27

0.37

0.23

0.47

1.0

0.11

0.19

1.0

CHROMIUM

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

5.0

LEAD

U

3.6

1.6

0.11

1.5

0.16

1.5

0.43

0.8

3.3

1.6

2.0

43

0.27

0.81

5.0

4ERCURY

U

0.1

0.013

0.02 A

0.011

0.094

0.084

0.025

0.19

0.018

0.097

0.019

0.049

0.018

0.04

0.2

Units = parts per million (pp»)
U = Not Detected

* Duplicate soil sample of S14

13

TABLE 3
ANALYTICAL DATA FOR PCBs
AT THE KENOSHA IRON t METAL SITE
KBN08HA, WISCONSIN
MARCH 30, 1994
SAMPLE
NUMBER

*i
32

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S5

S6

S7

S8

S9

S12

S10

PARAMETER
PCB 1248

U

U

11

39

53

U

23

U

55

U

PCB 1254

23

16

U

U

U

31

U

6.2

U

32

TOTAL
PCBs

23

39

53

31

23

6.2

55

32

.
^ -11

Units = parts per million (ppm)
U = Not Detected
TABLE 4
ANALYTICAL DATA FOR PCBs
AT THE KENOSHA IRON i METAL SITE
KENOSHA, WISCONSIN
MAY 1994
SAHPIE NUMBER
PARAMETER

S4

S22

540

S44

S51

S68

871

S90

S112

S122

PC8 1248

35

21

52

35

53

10

280

36

110

27

PCB 1254

U

U

U

U

U

U

U

U

U

32

PCS 1260

1.6

13

5.3

7.8

5.4

15

19

46

82

14

36.6

34

57.3

42.8

58.4

25

299

82

192

41

TOTAL PCBs

Units = parts per m i l l i o n (ppm)
U = Not Detected

14

Total PCB results for soil samples collected in May 1994, soil
sampling results for indicated total PCBs at 299 ppm in soil
sample SV.
Pesticide results for soil samples collected in May
1994, chlordane was indicated in soil sample S48 at 35,000 ppm.
6.0

DISCUSSION OF POTENTIAL THREATS

Conditions at the KIM site that may warrant a removal action, as
set forth in paragraph (b)(2) of Section 300.415 of 40 Code of
Federal Regulations (CFR), the National Contingency Plan (NCP),
include:

6.1

1.

Actual or potential exposure to nearby human
populations, animals, or the food chain from
hazardous substances or pollutants or
contaminants;

2.

High levels of hazardous substances or pollutants
or contaminants in soils largely at or near the
surface, that may migrate; and

3.

Weather conditions that may cause hazardous
substances or pollutants or contaminants to
migrate or be released.

Potential Exposure To Hazardous Substances

Site investigations and analytical data obtained by WDNR and the
TAT have identified surface and subsurface soils containing
materials that possess characteristics of hazardous wastes, as
defined by RCRA, at the KIM site. Total concentrations of PCBs
in soil sample S71 indicated 299 mg/kg. PCBs are known
carcinogens and are toxic substances; children are particularly
at risk. TCLP metals were detected above the RCRA regulatory
limit for cadmium (1 mg/1) and lead (5 mg/1). In soil sample
S13, cadmium (1.0 mg/1) and lead (43 mg/1) were detected in onsite soils above the RCRA TCLP regulatory limits. Cadmium may
cause irritation to the nose and throat. Lead is a suspected
carcinogen. Parts of the site are used by children and local
residents as a shortcut; these persons could be at risk. The
site is sparsely vegetated, increasing the chance of off-site
migration of contaminated particulates via strong winds.
6.2

Migration of Contaminants

Site investigations have documented the presence at the KIM site
of chemicals associated with scrap metal recycling (lead
batteries and transformers) and heavy metals that were above the
RCRA regulatory limits for cadmium and lead (1 and 5 mg/L,
respectively) in surface soil samples. The site is sparsely
vegetated. PCBs were detected in surface soil samples at
concentrations above Toxic Substance Control Act (TSCA)
15

regulatory limit of 50 ppm with the highest concentration in
sample S71 at 299 mg/kg. Contaminants may migrate off site
during dry windy conditions hv airborne dusts or by storm run-off
during rain events. Resident's homes are adjacent to the site to
the north and a school is located across 55th Street.
6.3

Weather Conditions

PCBs and heavy metals have been found at the KIM site in surface
soil at concentrations above RCRA regulatory levels. The site is
sparsely vegetated. Migration of contaminated soils by airborne
particulates is possible during periods of dry, dusty conditions.
Migration of contaminated soils during storm events is possible
due to erosion of the surface soils. Storm runoff from the site
is to the north and into the storm sewer on 55th Street that
discharges into Kenosha Harbor.
7.0

REMOVAL ACTION

The site assessment has documented the presence of hazardous
substances at the KIM site. These substances were detected in
samples of soil, which were found to contain materials that
possess characteristics of hazardous wastes, as defined by RCRA.
The site is unsecured and accessible, and children and the public
are known to use the property as a shortcut. Based on the
findings of the site assessment, a time-critical removal action
at the KIM site would reduce or eliminate immediate threats to
human health and the environment.
8.0

ROMS 4.0 COST PROJECTION

Removal cost estimates for off-site disposal were projected using
the U.S. EPA Removal Cost Management System (RCMS) program. Cost
estimates to mitigate threats due to on-site contaminated
materials contained in the soil are based on the following
assumptions:
1.

There is a total of approximately 6,078 cubic
yards of heavy metal contaminated soils onsite. This estimated amount was generated
assuming that the 1.3-acre site may show
contamination to a depth of at least 3 feet.

2.

There is a total of approximately 417 cubic
yards of soils contaminated with PCBs at
concentrations greater than 50 ppm which will
require disposal at a TSCA approved landfill
at an approximate cost of $300.00 per cubic
yard ;

16

3.

Soil exhibiting TCLP cadmium and lead
concentrations greater than 1 and 5 mg/1,
respectively, will require stabilization
either on-site or off-site and transportation
to an appropriate RCRA-permitted off-site
landfill. If the soil also exhibits a PCB
concentration of greater than 50 mg/kg prior
stabilization, the soil will be stabilized
and disposed of at a TSCA-approved landfill
at an approximate cost of $20.00 per cubic
yard ;

4.

The excavated area of the site will be
backfilled with clean soils and graded to
prevent ponding of water; and

5.

Site security will be improved by
constructing a 6-foot chain-link security
fence topped with barbed wire and two 10-foot
gates. A total of 1,120 feet of fence
material will be needed at a cost of
$16,800.00, including installation.

The cost estimates for the cleanup are based on 60 12-hour days
by the Emergency Response Cleanup Support (ERCS) contractor
Riedel Environmental Services, and is projected to cost
$767,144.28. See Appendix E for the RCMS cost estimate.

17

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1112
DIRECTION:
SOUTHEAST
PHOTOGRAPHER: JOHN NOROINE
OESCR: SE VIEW OF SITE, NOTE LACK OF
VEGETATION & SURVEY POINTS

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1112
DIRECTION:
SOUTHEAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: SE VIEW OF SITE, NOTE LACK OF
VEGETATION & SURVEY POINTS

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1112
DIRECTION:
NORTHEAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: NE VIEW OF SITE. NOTE LACK OF
VEGETATION & SURVEY POINTS

SITE: KENOSHA IRON I METAL
DATE: 5-11-94
TIME: 1113
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NOROINE
DESCR: THE BACKYARD OF 2007 55th
STREET.

SITE: KENOSHA IRON t METAL
DATE: 5-11-94
TIME- 1114
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: THE BACKYARD OF 1933 55th
STREET.

SITE: KENOSHA IRON I METAL
DATE: 5-11-94
TIME: 1114
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: DRIVE BETWEEN 1933 AND 1929
55th STREET.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME- 1113
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NOROINE
DESCR: THE BACKYARD OF 2001 55th
STREET.

SITE: KENOSHA IRON t METAL
DATE: 5-11-94
TIME: 1116
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: DRIVE BETWEEN 2001 AND 1933
55th STREET.

SITE: KENOSHA IROM t METAL
DATE: 5-11-94
UI5
D I SECTION:
NORTHEAST
PHOTOGRAPHER: JOHN NORDINE
OESCR: BACKYARD OF 1933 55th STREET

SITE: KENOSHA IRON & HETAL
DATE: 5/11/94
TIME: 1709
DIRECTION: NORTH
PHOTOGRAPHER: JOHN NORDINE
D<:SCR: DRIVEWAY BETWEEN 1929 AND 1923
55th STREET.

SITE:

KENOSHA IRON & METAL

DATE: 5-11-94
TIME: 1116
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NOROINE
DESCR: BACKYARD OF 1923 55th STREET.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1117
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NOROINE

DESCR: BACKYARD OF 1913 55th STREET.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1117
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: SOUTH SIDE OF 5506 19th
AVENUE.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1117
DIRECTION:
NORTHEAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: BACKYARD OF 5506 19th AVENUE..

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1119
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: SCHOOL LOCATED AT THE CORNER
OF 19th AVENUE & 55th STREET.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1117
DIRECTION:
SOUTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: NOTE SCHOOL IN BACKGROUND
2-STORY BROWN BRICK BUILDING

I

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1117
DIRECTION:
SOUTH
PHOTOGRAPHER: JOHN NORDINE
DESCR: EMPTY LOT AND PATH THROUGH
SITE AT 1919 55th STREET.

SITE: KENOSHA IRON & METAL

SITE: KENOSHA IRON I METAL
DATE: 5-11-94
TIME: 1709
DIRECTION: EAST
PHOTOGRAPHER:JOHN NOROINE
OESCR: VIEU OF SITE LOOKING NORTHEAST

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1709
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: VIEW OF THE WESTERN PART OF
THE SITE.

SITE: KENOSHA IRON & METAL
DATE: 5-11-94
TIME: 1110
DIRECTION: EAST
PHOTOGRAPHER:JOHN NOROINE
DESCR: VIEU OF SITE LOOKING EAST

SITE: KENOSHA IRON I METAL
DATE: 5-11-94
TIME: 1110
DIRECTION: NORTHEAST
PHOTOGRAPHER:JOHN NORDINE
DESCR: NE VIEU OF SITE. NOTE LACK OF
VEGETATION & SURVEY POINTS

SITE: KENOSHA IRON ft METAL
DATE: 3-30-94
TIME- 1300
DIRECTION:
NORTH
PHOTOGRAPHER: JOHN NOROINE
DESCR: SCHOOL ACROSS 55th STREET
NORTH OF THE SITE.

SITE: KENOSHA IRON ft METAL
DATE: 3-30-94
TIME: 1305
DIRECTION:
SOUTHEAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: BUSINESS LOCATED SOUTH AND
EAST OF THE SOUTH.

SITE: KEMOSHA IRON t METAL
DATE: 5-11-94
TIME: 1700
DIRECTION: EAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: VIEW OF SITE LOOKING EAST.
NOTE WARNING SIGN.

SITE: KENOSHA IRON t METAL
DATE: 5-11-94
TIME: 1709
DIRECTION: EAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: VIEW OF SITE LOOKING NORTHEAST

SITE: KENOSHA IRON I METAL
DATE: 3-30-94
TIME: 1050
DIRECTION: NORTH
PHOTOGRAPHER:JOHN WORDIWE
DESCR: LOCATION OF SOIL SAMPLE 51

SITE: KENOSHA IRON & METAL
DATE: 3-30-94
TIME: 1055
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S2

SITE: KENOSHA IRON I METAL
DATE: 3-30-94
TIME: 1105
DIRECTION: NORTH
PHOTOGRAPHER .-JOHN NOROINE
DESCR: LOCATION OF SOIL SAMPLE S3

SITE: KENOSHA IRON t METAL
DATE: 3-30-94
TIME: 1115
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S4 IN
1933 55th STREET BACKYARD

SITE: KENOSHA IRON t METAL
DATE: 3-30-94
TIME: 1125
DIRECTION: NORTH
PHOTOGRAPHER:JOHN MORDINE
DESCR: LOCATION OF SOIL SAMPLE S5

SITE: KENOSHA IRON i METAL
DATE: 3-30-94
TIME: 1130
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S6

SITE: KENOSHA I ROM & HETAL
DATE: 3-30-94
TIME: 1KO
DIRECTION: NORTH
PHOTOGRAPHER-.JOHN NORDIME
DESCR: LOCATION OF SOIL SAMPLE S7

SITE: KENOSHA IRON S METAL
DATE: 3-30-94
TIME- 1145
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORD1NE
DESCR: LOCATION OF SOIL SAMPLE S8

SITE: KENOSHA IRON & METAL
TIME: 1150
DATE: 3-30-94
DIRECTION: NORTH
PHOTOGRAPHER:JOHM NORDINE
OESCR: LOCATION OF SOIL SAMPLE S9

SITE: KENOSHA IRON t METAL
DATE: 3-30-94
TIME: 1159
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S10

SITE: KENOSHA IRON t METAL
DATE: 3-30-94
TIME: 1205
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S11

SITE: KENOSHA IRON C METAL
DATE: 3-30-94
TIME: 1210
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE 512

SITE: KENOSHA IRON t METAL
DATE: 3-30-94
TIME: 1220
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S13

SITE: KENOSHA IRON & METAL
DATE: 3-30-94
TIME: 1240
DIRECTION: EAST
PHOTOGRAPHER:JOHN NORDINE
DESCR: LOCATION OF SOIL SAMPLE S14
AND SIS

SITE: KENOSHA IRON & METAL
DATE: 3-30-94
TIME: 1245
DIRECTION: NORTHUEST
PHOTOGRAPHER:JOHN NORDINE
DESCR: PERSON USUC THE PATH THROUGH
THE SITE.

SITE: KENOSHA IRON i METAL
DATE: 3-30-94
TIME: 1215
DIRECTION: NORTH
PHOTOGRAPHER:JOHN NOROIHE
DESCR: LIFETIME BATTERY CASING AND
SKELETON OF SMALL ANIMAL

SITE: KENOSHA IRON & METAL
DATE: J-50-94
T1HE:
1000
DIRECTION:
SOUTHEAST
PHOTOGRAPHER:JOHN NORDINE
DESCR: V I E W Of S I T E LOOKING SOUTEAST,
NOTE LACK OF V E G E T A T I O N

SITE: KENOSHA IRON & M E T A L
DATE: 3-30-94
TIME:
1000
DIRECTION:
NORHTEAST
PHOTOCRAPHER:JOHN NORDINt
DFSCR: HOMES ALONG THE NORTH SlOf OF
THE SITE.

SlU:
ICtNOSHA IRON & METAL
DATE: i-30-9^.
TIME:
1000
DIRECIION:
NORTH
PHOTOGRAPHER: JOHN NORD1NE
OESCR: AREA WHERE MAIN B U I L D I N G AND
SCALES WERE LOCATED.

SITE:
KENOSHA IRON & M E T A L
DATE:
3-30-94
TIME:
1000
DIRECMON:
SOUTUWLSI
P H O T O G R A P H E R : JOHN NPRD1NE
PEr>rR: LAND USE I O C A T I P TO T i l F SOUTH
MD

UEST OF THf SI II .

S I T E : KENOSIIA IRON £ M E T A L
TIME:
1000
DATL: 3-30-94
DIRECIiuN:
EAST
f-HGIUu&AHlER: JOHN NORDINE
DESCR: VIEW OF SITE LOOKING EAST,
NOTE LACK OF V E G E T A T I O N

S I T F : KFNOSHA IRON & MUAL
D A 1 E : 3 30-9i
1IMF:
DIRECTION:
NORHTEAS1
PHOlOCSAPHtR: JO»S NORD1NE
PrSfR: HOMCS AIONC THF N O R T H SU'f

sni.. NOIF LACK of vrr.i IAI \

SITE: KENOSHA IRON I METAL
DATE: 3-30-94
TIHE:
1000
DIRECTION:
NORHTEAST
PHOTOGRAPHER: JOHN NORDINE
DESCR: HOMES ALONG THE NORTH SIDE OF
THE SITE.

APPENDIX B
DATA QUALITY ASSURANCE REVIEW

ecology and environment, inc,
111 WEST JACKSON BLVD.. CHICAGO. ILLINOIS 60604. TEL. 312 663-9415
international Specialists in the Environment

M E M O R A N D U M

DATE:

June 6, 1994

TO:

John Nordine, TAT-Project Manager, E & E, Chicago, IL

FROM:

Karen Smith, TAT-Chemist, E & E, Detroit, OH

THRU:

Sandra L. Basham, ATATL, E & E, Detroit, MI

SUBJ:

Total Metals Analyses Data Quality Assurance Review,
Kenosha Iron & Metal Site, Kenosha, Kenosha County,
Wisconsin

REF:

Analytical TDD:T05-9403-810
Analytical PAN:EWI0423AAA

Project TDD:T05-9403-013
Project PAN:EWI0423FAA

The data quality assurance review of fifteen soil samples
collected from the Kenosha Iron & Metal site is complete. The
samples were collected March 30, 1994, by the Technical
Assistance Team Contractor, Ecology and Environment (E & E). The
samples were submitted to Quality Analytical Labs, Inc., Lisle,
Illinois. Laboratory analysis was performed according to SW-846
methods 6010 and 7471.
SAMPLE IDENTIFICATION
Lab #
940680-01
940680-02
940680-03
940680-04
940680-05
940680-06
940680-07
940680-08
940680-09
940680-10
940680-11
940680-12
940680-13
.940680-14
940680-15

-ecvcied paper

E & E f
SI
S2
S3
S4
55
S6
S7
S8
S9
S10
Sll
S12
S13
S14
S15

Data Qualifications
I

Sample Holding Time; Acceptable
Samples were collected on March 30, 1994, and the laboratory
received the samples on March 31, 1994. Digestion was
performed on April 7, 1994. The analyses for total and TCLP
metals were completed on April 11, 1994, well within the
recommended holding time (6 months for metals, 28 days for
mercury).

II

Initial and Continuing Calibrations;

Acceptable

Initial and Continuing calibrations were within the
recommended limits of 90%-110% of the true values for
metals, 80%-120% of the true values for mercury.
III

Blanks;

Acceptable

Calibration blanks and preparation blanks were analyzed with
the samples.. All analyte concentrations were below
instrument detection limits (BDL).
IV

ICP Interference Check Samples: Acceptable
All interference check sample results were within the
recommended control limits of plus-or-minus 20%.

V

Performance Evaluation Samples;

VI

Additional PC Checks;

Not Applicable

Acceptable

All matrix spike/matrix spike duplicate (MS/MSD) results had
percent recoveries (R%) between 81-91% of the true values.
VII

Overall Assessment of Data for Use : Acceptable
The overall usefulness of the data is based on the criteria
outlined in OSWER Directive 9360.4-01 (April 1990), Data
Validation Procedures, Section 3.0, Metallic Inorganic
Parameters and Section 2.7, Quality Assurance Requirements
for QA Level II work.
Based upon the information provided, the data are acceptable
for use as reported.

ecology and environment, inc.
12251 UNIVERSAL. T A Y L O R . MICHIGAN 48180. TEL. 3131 946-0900

M E M O R A N D U M

DATE:
TO:

June 6, 1994
John Nordine, TAT-Project Manager, E & E Chicago, IL

FROM:

Karen Smith, TAT-Chemist, E & E, Detroit, MI #".

THRU:

Sandra L. Basham, ATATL, E & E, Detroit, Ml

SUBJ:

PCB Analysis Data Quality Assurance Review, Kenosha
Iron & Metal Site, Kenosha, Kenosha County, Wisconsin.

REF:

Project TDD:T05-9403-013
Project PAN:EWI0423FAA

Analytical TDD:T05-9403-810
Analytical PAN:EWI0423AAA

The data quality assurance review of ten soil samples
collected from the Kenosha Iron & Metal Site is complete. The
samples were collected March 30, 1994, by the Technical
Assistance Team Contractor, Ecology and Environment (E & E). The
samples were submitted to Quality Analytical Labs, Inc, Lisle,
Illinois. Laboratory analysis was performed according to SW-846
method 8080 for the determination of PCB compounds and their
corresponding concentrations.
SAMPLE IDENTIFICATION

Lab
940680-02
940680-03
940680-04
940680-05
940680-06
940680-07
940680-08
940680-09
940680-10
940680-12

recycled pacer

tt

E & E »
S2
S3
S4
S5
S6
S7
S8
S9
S10
S12

Data Qualifications
I

Sample Holding Time; Acceptable
Samples were collected on March 30, 1994, and received by
the laboratory on March 31, 1994. Extraction was completed
on April 10, 1994, and the analysis was performed on April
21, 1994, meeting the specified holding time (14 days to
extract and 40 days to analyze).

II

Instrument Performance;

Acceptable

All standards and resulting chromatograms had both adequate
peak separation and shifts in the retention time windows
were less than 0.3% for capillary columns.
III

Initial and Continuing Calibration;

Qualified

All Aroclors were calibrated using a 5-point calibration on
April 13, 1994. Relative standard deviations were all >
10%, except for Aroclor 1221. All positive sample results
for Aroclors other than 1221 have been flagged as estimates
(J).
Continuing calibrations were performed using all Aroclors.
The percent differences (%D) for all Aroclors were < 15%.
IV

Blanks; Acceptable
A method blank was analyzed with the samples. All compound
concentrations were below the practical quantitation limits
(BPQL).

V

Compound Identification; Acceptable
All peaks are compared against the appropriate standard
chromatograms as identified by the laboratory. All sample
chromatograms were verified for agreement with the standard
chromatograms and all retention time windows agree.
According to the laboratory narrative, all of the PCB
samples showed weathered mixtures of PCBs. Since
differention was difficult the lab calculated the total area
as the dominant aroclor for each sample.

VI

Compound Ouantitation and Reported Detection
Limits;Acceptable
All reported data has accounted for dilutions,
concentrations, splits, cleanup procedures, dry weight
factors, and any other factors not accounted for by the
method.

VII

Performance Evaluation Samples; Not Applicable

'eCVCled paper

,., ni<ig> and envmmmrni

VIII Optional PC Checks; Acceptable
Surroqates were added to the sample and all recoveries were
within the laboratory established limits of 60-150%.
IX

Overall Assessment of Data for Use: Acceptable
The overall usefulness of the data is based on the criteria
outlined in OSWER Directive 9360.4-01 (April 1990), Data
Validation Procedures, Section 7.0, PCBs and Section 2.7,
Quality Assurance Requirements for QA Level II work.
Based upon the information provided, the data are acceptable
for use as reported.

Data Qualifiers and Definitions
J -

The associated numerical value is an estimated quantity
because the reported concentrations were less than the
contract required detection limits or quality control
criteria were not met.

'SCVCIefl Oaper

t-nl<ie\ aim rruimnmem

QUALITY
1 ANALYTICAL
LABS, INC.
Final Report
April 21, 1994

Ecology & Environment, Inc.
Ill W. Jackson Blvd., 12th floor
Chicago, IL 60604
ATTN:

Mary Jane Ripp

Chain of Custody #: 5-23185
Project Name & #:
T05-9403-013 ; Proj . #EWI0723SAA
Sampling Date:
03/30/94
Please find enclosed
samples :
OAL Lab ID
940680-01
940680-02
940680-03
940680-04
940680-05
940680-06
940680-07
940680-08

the Analytical

Report

for the

following

Sample Description
51, 12' S 2007th 55th WDNRS02
52, 40' E of alley SW corner site
S3, 27' SE of 2007th 55th shed
S4, Backyard fence 1933 55th SO4
S5, 48' S 1933 SE corner of house
S6, 6' S of SE Corner of 1929 55th
S7, 79.8' S 1929 fence ac
S8, 108' S of 1929 SW
house corner fence
S9, 21.5' S fence i.e. 1925 55th ac
14' S of mid pt 1923 55th
Sll 53' S of mid pt 1913
S12 27' S of 1913 mid pt in path
S13 26' S of SW corner 1913 55th
S14 S14 SE corner of site
S15 31' W of light pole

940680-09
940680-10
940680-11
940680-12
940680-13
940680-14
940680-15
FINAL REPORT.
Note: All PCS samples showed weathered mixtures of two to three
arochlors.
Differention was difficult
so total area was
quantitated as dominant arochlor in each sample.
If you have any questions please contact Mike Kimmel at our
laboratories.
Respectfully submitted,
Quality Analytical Laboratories, Inc.

John Boudreau
Laboratory Director
sy:EC940680
"Precision, Accuracy and Service"

1938C UNIVERSITY LANE

LISLE, IL 60532

•

708 / 512-0061

FAX 708 / 512-0089

Quality Analytical Laboratories, Inc.
Page 2 of 16
Sample ID:

SI.

940680-01

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

50.
10.
15.
50.
200.
50.
10.
0.10

Hg- Digestion Date:
Analysis
mg/Kg
U
60.
500.
2300.
U
U
510.
1.6

04/11/94

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/13/94

Quality Analytical Laboratories, Inc.
Page 3 of 16
Sample ID:

52.

940680-02

Digestion Date:
04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg

50.
10.
15.
50.
200.
50.
10.
0.070

Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

Hg-Digestion Date:
Analysis
mg/Kg

U
120.
430.
4200.
U
U
870.
0.62

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

PCBs Analysis
% Moisture: 3
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

04/11/94

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0 .083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
U
23.
U

U
U

J-

Quality Analytical Laboratories, Inc.
Page 4 of 16
Sample ID:

S3,

940680-03

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
PQL
Parameter
mg/Kg
Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

50.
10.
15.
50.
200.
50.
10.
0.10

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/13/94

U
86.
1400.
4000.
U
U
1000.
5.4

PCBs Analysis
% Moisture: 5
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

SH846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
U
16.
U
U
U

Quality Analytical Laboratories, Inc.
Page 5 of 16

Sample ID:

S4.

Digestion Date:

Project #940680

940680-04
04/07/94

TOTAL RCRA METALS (soil)
PQL
Parameter
mg/Kg
5.0
Arsenic
1.0
Cadmium
Chromium
1.5
Lead
5.0
20.
Selenium
Silver
5.0
Barium
1.0
Mercury
0.060

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Analysis
Date
04/08/94
04/08/94
04/08/94
04/08/94
04/08/94
04/08/94
04/08/94
04/11/94

6.3
11.
50.
680.
U
U
200.
0.27

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

PCBs Analysis
% Moisture: 21
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

SW846 8080

Analysis Date.- 04/21/94

0.083
0 .083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
11.
U
U
U
U

T

Quality Analytical Laboratories, Inc.
Page 6 of 16
Sample ID:

35.

940680-05

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

50.
10.
15.
50.
200.
50.
10.
0.06

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

U
84.
280.
3400.
U
U
850.
0.73

PCBs Analysis
% Moisture: 5
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
39.
U
U
U
U

Quality Analytical Laboratories, Inc.
Page 7 of 16

Sample ID:

S6.

Digestion Date:

Project #940680

940680-06
04/07/94

TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
5.0
Arsenic
1.0
Cadmium
Chromium
1.5
5.0
Lead
100.
Selenium
5.0
Silver
1.0
Barium
0.070
Mercury

Hg-Digestion Date:
Analysis
mg/Kg
U
21.
56.
1100.
U
U
500.
0.13

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

PCBs Analysis
% Moisture: 24
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

04/11/94
Analysis
Date
04/08/94
04/08/94
04/08/94
04/08/94
04/11/94
04/08/94
04/08/94
04/11/94

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
53 .
U
U
U
U

Quality Analytical Laboratories, Inc.
Page 8 of 16
Sample ID:

S7.

940680-07

Digestion Date:
04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg

50.
10.
15.
50.
200.
50.
1.0

Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

0. 060

Hg-Digestion Date:
Analysis
mg/Kg

U
91.
1100.
4900.
U
U
760.
0.91

04/11/94

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

PCBs Analysis
% Moisture: 4
Extraction Date: 04/10/94

Analysis Date: 04/21/94

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

Method:

0.083
0. 083

0.083
0.083
0.083
0.083
0.083
0.083
0.083

SW846 8080
Dry Weight
Analysis (mg/Kg)
U
U
U
U
U
31
U
U
U

Quality Analytical Laboratories, Inc.
Page 9 of 16
Sample ID:

S8.

940680-08

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

50.
10.
15.
50.
200.
50.
10.
0.11

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/13/94

U
51.
880.
2300.
U
U
650.
1.2

PCBs Analysis
% Moisture: 5
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
23.
U
U
U
U

Quality Analytical Laboratories, Inc.
Page 10 of 16
Sample ID:

SB.

940680-09

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg

50.
10.
15.

Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

50.
200.
50.
10.
0.060

Hg-Digestion Date:
Analysis
mg/Kg

Method
SW846-

Analysis
Date

U

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

78.
350.

5000.
U
U

2400.
0.70

FCBs Analysis
% Moisture: 19
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

04/11/94

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
U

6.2
€
U
U
U

J

Quality Analytical Laboratories, Inc.
Page 11 of 16
Sample ID:

S10.

940680-10

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg

PCBs Analysis
% Moisture: 10
Extraction Date
Parameter
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/08/94
04/11/94
04/11/94

50.
U
10.
55.
12000.
15.
50.
2200.
U
200.
U
5.0
400.
1.0
0.060
0.40

Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Project #940680

Method:
04/10/94

SW846 8080

Analysis Date: 04/21/94
PQL (mg/Kg)

1016
1221
1232
1242
1248
1254
1260
1262
1268

0.083
0.083
0.083
0.083
0.083
0 .083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
55
U
U
U
U

Quality Analytical Laboratories, Inc.
Page 12 of 16

Sample ID:

511.

Digestion Date:

Project #940680

940680-11
04/07/94

TOTAL RCRA METALS (soil)
PQL
Parameter
mg/Kg
25.0
Arsenic
Cadmium
1.0
1.5
Chromium
5.0
Lead
100.
Selenium
5.0
Silver
1.0
Barium
0.060
Mercury

Hg-Digestion Date:
Analysis
mg/Kg
U
38.
450.
2200.
U
U
540.
0.93

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

04/11/94
Analysis
Date
04/11/94
04/08/94
04/08/94
04/11/94
04/11/94
04/08/94
04/08/94
04/11/94

Quality Analytical Laboratories,
Page 13 of 16
Sample ID:

Inc. Project #940680

512. 940680-12

Digestion Date: 04/07/94
TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg

50.
10.
15.
50.
200.
50.
10.
0.060

Arsenic
Cadmium
Chromium
Lead
Selenium
Silver
Barium
Mercury

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg

Method
SW846-

Analysis
Date

6010
6010
6010
6010
6010
6010
6010
7471

04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

U
45.
210.
2500.
U
U
700.
0.73

PCBs Analysis
% Moisture: 18
Extraction Date: 04/10/94

Method:

Parameter

PQL (mg/Kg)

Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor
Aroclor

1016
1221
1232
1242
1248
1254
1260
1262
1268

SW846 8080

Analysis Date: 04/21/94

0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083
0.083

Dry Weight
Analysis (mg/Kg)
U
U
U
U
U
32.
U
U
U

Quality Analytical Laboratories, Inc.
Page 14 of 16

Sample ID:

S13,

Digestion Date:

Project #940680

940680-13
04/07/94

TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
100.
Arsenic
10.
Cadmium
Chromium
15.
50.
Lead
Selenium
200.
Silver
50.
Barium
10.
Mercury
0.060

Hg-Digestion Date:
Analysis
mg/Kg
U
98 .
7500.
12000.
U
U
1000.
0.47

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

04/11/94
Analysis
Date
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94
04/11/94

Quality Analytical Laboratories, Inc.
Page 15 of 16

Sample ID:

S14.

Digestion Date:

Project #940680

940680-14
04/07/94

TOTAL RCRA METALS (soil)
PQL
Parameter
mg/Kg
5.0
Arsenic
Cadmium
1.0
Chromium
1.5
5.0
Lead
Selenium
20.
5.0
Silver
1.0
Barium
Mercury
0.11

Hg-Digestion Date:
Analysis
mg/Kg
5.2
19.
130.
1300.
24.
U
730.
2.7

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

04/11/94
Analysis
Date
04/08/94
04/08/94
04/08/94
04/08/94
04/08/94
04/11/94
04/11/94
04/13/94

Quality Analytical Laboratories, Inc.
Page 16 of 16

Sample ID:

S15.

Digestion Date:

Project #940680

940680-15
04/07/94

TOTAL RCRA METALS (soil)
Parameter
PQL
mg/Kg
Arsenic
50.
1.0
Cadmium
Chromium
1.5
Lead
5.0
Selenium
20.
5.0
Silver
1.0
Barium
Mercury
0.10

Hg-Digestion Date:

04/11/94

Analysis
mg/Kg
U

Analysis
Date
04/11/94
04/08/94
04/08/94
04/08/94
04/08/94
04/11/94
04/11/94
04/13/94

25.
160.
1700.
U
U
880.
2.9

Method
SW8466010
6010
6010
6010
6010
6010
6010
7471

- Defined Data Qualifiers
B

Compound detected in blank (Normalized concentration)

C

Used when blank value exceeds half of the CRDL (PQL).
Pesticide result confirmed by GC/MSD

D

Compound identified in analysis at a secondary dilution factor

E

Used when two or more dilutions of a sample are needed to acquire valid data.
Compounds concentration exceeds calibration range
Used when upper level of calibration curve is exceeded by 10%. Analyses greater than 50% of upper calibration level are
reanalyzed at a higher dilution.

J
P
U
X

Estimated value. Compound detected below the CRDL (PQL).
Pesticide or Aroclor analysis where results between analytical and confirmation columns is > 25%.
Compound analyzed for but not detected at or above the CRDL (PQL).
NON-Specific flag • See definition at the end of the report

Data Validation
NJ

Presumptive evidence of presence of material at an estimated quantity.
Used when QA/QC failures are present AND data is true. Must be accompanied by NCR

PND

R

RND

Precision Not Determined

Used when non-approved methods are used to obtain data.
Reported value is unusable due to gross QA/QC deficiencies.

Recovery Not Determined
Used when non-approved methods are used to obtain data.

UJ

Compound analyzed for but not detected, reported detection limit estimated because QA/QC criteria
were not met.

Detection LJmit Definitions
CRDL
IDL

Contract Required Detection Limits = Detection limits specified by client or agency
Based on wet weight analysis
Instrument Detection Limit
Statistically derived detection limit from 7 + analyses of a low level standard near but above the estimated Method Detection

MDL

Limit.
Method Detection Limit
Instrument Detection Limit

PQL

X End Volume (specified by the method) / Mass, Volume or Area of the Sample [specified by the

method) (Based on wet weight analysis)
Practical Quantitation Limit
Method Detection Limit
analysis)

X End Volume (analytical)

/ Mass, Volume or Area of the Sample [analytical) (Based on wet weight

ecology and environment, inc.
Ill WEST JACKSON BLVD , CHICAGO, ILLINOIS 60604. TEL. 312 663-9415
international Specialists in the Environment

M E M O R A N D U M

DATE:

June 23, 1994

TO:

John Nordine, TAT-Project Manager, E & E, Chicago, IL

FROM:

David Hendren, TAT, E & E, Chicago, IL

THRU:

Mary Jane Ripp, Analytical Services Coordinator, E & E,
Chicago,IL

SUBJ:

selected TCLP Metals Data Quality Assurance
Review, Kenosha Iron & Metal site, Kenosha, Kenosha
County, Wisconsin

REF:

Analytical TDD:T05-9403-810
Analytical PAN:EWI0423AAA

Project TDD:T05-9403-013
Project PAN:EWI0423FAA

The data quality assurance review of fifteen soil samples
collected from the Kenosha Iron & Metal site is complete. The
samples were collected March 30, 1994, by the Technical
Assistance Team Contractor, Ecology and Environment (E & E). The
samples were submitted to Quality Analytical Labs, Inc., Lisle,
Illinois. Laboratory analysis was performed according to SW-846
methods 6010 and 7470 for the selected metals, Cadmium, Chromium,
Lead, and Mercury.
SAMPLE IDENTIFICATION

Lab *
940680-01
940680-02
940680-03
940680-04
940680-05
940680-06
940680-07
940680-08
940680-09
940680-10
940680-11
940680-12
940680-13

; ecycled paper

E & E #
SI
S2
S3
S4
S5
S6
S7
S8
S9
S10
Sll
S12
S13

940680-14
940680-15

S14
S15

Data Qualifications;

I.

Holding Tine: Acceptable

The samples were collected on 3/30/94, subjected to TCLP
extraction on 4/22/94, digested on 4/27/94 and analyzed on
4/28/94. Samples were extracted for mercury on 4/20/94 and
analyzed on 5/3/94. The holding time criteria of 6 months (28
days for mercury) from collection to analysis for metals was
satisfied.
II.

calibration:
A.

Initial Calibration:

Acceptable

Recoveries for the initial calibration verification were
within 90-110% (80-120 % for mercury), as required.
B.

Continuing Calibration:

Acceptable

All analytes of interest in the continuing calibration
verification standard were within 90-110% recoveries (80-120 %
for mercury), as required.
III. Method Blank:

Acceptable

A method blank was analyzed with each batch of samples. No
contaminants or target analytes were detected.

IV.

Interference Check Sample (ICS) Analysis:

Acceptable

All analytes included in the ICS were recovered within 80120%, as required.

v.

Matrix Spike/Matrix Spike Duplicate (MS/MSD):Not Applicable

A Matrix Spike/Matrix Spike Duplicate (MS/MSD) was not
performed on a sample from this group. The laboratory did perform
a MS/MSD on a sample from another batch and recoveries were
acceptable.
vi.

overall Assessment of Data For Use:

The overall usefulness of the data is based on the criteria
outlined in "Quality Assurance/Quality Control Guidance for
Removal Activities" (OSWER 9360.4-01 April, 1990). Based upon the
information provided, the data are acceptable for use.

Quality Analytical Laboratories, Inc.
Page 2 of 16

Sample ID:

SI.

Project #940807

940807-01

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
PQL
Parameter
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0 .10
0.005

0.008
U
U
U

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page j of 16

Sample ID:

S2.

Project #940807

940807-02

TCLP Extraction Date: 04/22/94,ICP
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
Analysis
PQL
mg/L
mg/L

Method
SW846

Analysis
Date

Cadmium
Chromium
Lead
Mercury

6010
6010
6010
7470

04/28/94
04/28/94
04/28/94
05/03/94

0.005
0.015
0.10
0.005

0.65
U
3.6
0.10

04/20/94, Hg

Quality Analytical Laboratories, Inc.
Page 4 of 16

Sample ID:

S3.

Project #940807

940807-03

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846

Analysis
Date

Cadmium
Chromium
Lead
Mercury

04/28/94
04/28/94
04/28/94
05/03/94

0.005
0.015
0.10
0.005

0 .41
U
1.6
0.013

6010
6010
6010
7470

Quality Analytical Laboratories, Inc.
Page 5 of 16

Sample ID:

S4.

Project #940807

940807-04

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Analysis Method
Parameter
PQL
SW846
mg/L
mg/L
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0.051
U
0.11
0.024

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 6 of 16

Sample ID:

S5.

Project #940807

940807-05

TCLP Extraction Date: 04/22/94, ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0 .10
0.005

0.63
U
1.5
0.011

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 7 of 16

Sample ID:

S6.

Project #940807

940807-06

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846

Analysis
Date

Cadmium
Chromium
Lead
Mercury

04/28/94
04/28/94
04/28/94
05/03/94

0.005
0.015
0.10
0.005

U
U
0.16
0.094

6010
6010
6010
7470

Quality Analytical Laboratories, Inc.
Page 8 of 16

Sample ID:

S7.

Project #940807

940807-07

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0 .54
U
1.5
0.084

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 9 of 16

Sample ID:

S8,

Project #940807

940807-08

TCLP Extraction Date:
04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
PQL
Analysis Method
Parameter
SW846
mg/L
mg/L
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0.19
U
0.43
0.025

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 10 of 16

Sample ID:

59.

Project #940807

940807-09

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date:
04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0.27
U
0.80
0.019

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 11 of 16

Sample ID:

S10.

Project #940807

940807-10

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846

Analysis
Date

Cadmium
Chromium
Lead
Mercury

04/28/94
04/28/94
04/28/94
05/03/94

0.005
0.015
0.10
0.005

0.37
U
3.3
0.018

6010
6010
6010
7470

Quality Analytical Laboratories, Inc.
Page 12 of 16

Sample ID:

Sll.

Project #940807

940807-11

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Analysis Method
PQL
Parameter
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0. 015
0.10
0.005

0.23
U
1.6
0.097

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 13 of 16

Sample ID:

S12.

Project #940807

940807-12

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date: 04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846

Analysis
Date

Cadmium
Chromium
Lead
Mercury

04/28/94
04/28/94
04/28/94
05/03/94

0.005
0.015
0.10
0.005

0.47
U
2.0
0.019

6010
6010
6010
7470

Quality Analytical Laboratories, Inc.
Page 14 of 16

Sample ID:

Project #940807

S13. 940807-13

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date:
04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0 .005

1.0
U
43.
0.049

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 15 of 16

Sample ID:

S14.

Project #940807

940807-14

04/20/94, Hg
TCLP Extraction Date: 04/22/94,ICP
Digestion Date: 04/27/94
TCLP Metals (selected)
Analysis Method
PQL
Parameter
SW846
mg/L
mg/L
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0.11
U
0.27
0.018

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

Quality Analytical Laboratories, Inc.
Page 16 of 16

Sample ID:

S15.

Project #940807

940807-15

TCLP Extraction Date: 04/22/94,ICP
04/20/94, Hg
Digestion Date:
04/27/94
TCLP Metals (selected)
Parameter
PQL
Analysis Method
mg/L
mg/L
SW846
Cadmium
Chromium
Lead
Mercury

0.005
0.015
0.10
0.005

0.19
U
0.81
0.040

6010
6010
6010
7470

Analysis
Date
04/28/94
04/28/94
04/28/94
05/03/94

- Defined Data
B

Compound detected in blank (Normalized concentration)

C

Used when blank value exceeds half of the CRDL (PQL).
Pesticide result confirmed by GC/MSD

D

Compound identified in analysis at a secondary dilution factor

E

Used when two or more dilutions of a sample are needed to acquire valid data.
Compounds concentration exceeds calibration range
Used when upper level of calibration curve is exceeded by 10%. Analyses greater than 50% of upper calibration level are
reanalyzed at a higher dilution.

J
P
U
X

Estimated value. Compound detected below the CROL (PQL).
Pesticide or Aroclor analysis where results between analytical and confirmation columns is > 25%.
Compound analyzed for but not detected at or above the CRDL (PQL).
NON- Spec/ fie flag - See definition at the end of the report

Data Validation
NJ
PND
R

RND

Presumptive evidence of presence of material at an estimated quantity.
Used when QA/QC failures are present AND data is true. Must be accompanied by NCR
Precision Not Determined
Used when non-approved methods are used to obtain data.
Reported value is unusable due to gross QA/QC deficiencies.

Recovery Not Determined
Used when non-approved methods are used to obtain data.

UJ

Compound analyzed for but not detected, reported detection limit estimated because QA/QC criteria
were not met.

Detection JLimit De-pinitions
CRDL
IDL

Contract Required Detection Limits = Detection limits specified by client or agency
Based on wet weight analysis
Instrument Detection Limit
Statistically derived detection limit from 7 +• analyses of a low level standard near but above the estimated Method Detection
Limit.

MDL

Method Detection Limit
Instrument Detection Limit X End Volume (specified by the method) / Mass. Volume or Area of the Sample [specified by the
method) (Based on wet weight analysis)

PQL

Practical Quantitation Limit
Method Detection Limit
analysis}

X End Volume [analytical] / Mass, Volume or Area of the Sample [analytical) (Based on wet weight

ecology and environment* inc.
6777 ENGLE ROAD, CLEVELAND. OHIO 44130, TEL. (216) 243-3330
International Specialists in the Environment

M

E

M

O

R

A

N

D

U

M

DATE:

July 19, 1994

TO:

J. Nordine, TAT Project Manager, E & E, Inc., Chicago, IL

FROM:

E.S. Landis, TAT Geochemist, E & E, Inc., Cleveland, OH

VIA:

Nabil Fayoumi, TAT Chemist, E & E, Inc., Chicago, iL

SUBJ:

PCBs Data Quality Assurance Review, Kenosha Iron & Metal
Site, Kenosha, Kenosha County, WI

RE:

Analytical TDD: T059405802
Analytical PAN: EWI0423ABA

Project TDD: T059403013
Project PAN: EWI0423SAA

The data quality assurance review of 10 discrete soil samples
analyzed for polychlorinated biphenyls (PCB Aroclors 1248 and 1260)
is now complete.
The samples were submitted to Heritage
Laboratories, Inc. of Romeoville, Illinois (HLI) on May 19, 1994.
The laboratory analyzed 10 of the samples for PCBs by dual-column
gas chromatography with flame ionization and electron capture
detectors (GC/FID/ECD), following SW-846 Method 8080. The samples
were labeled as follows:
TAT Station Location/Heritage Lab ID
S40/C156818
S112/C156820
S44/C156821
S51/C156822
S68/C156824
S71/C156825
S4/C156826
S90/C156827
S122/C156828
S22/C156830

•ecycicd oaper

Data Qualifications;
I.

Sample Holding Times: Acceptable.

The samples were collected at the Kenosha Iron & Metal site in
Kenosha, Wisconsin, on May 10, 1994. The samples were extracted
May 20, and analyzed May 25 and 26, 1994. The samples were
handled in compliance with the respective 14-day and 40-day
holding time limits.
II.

Instrument Performance:

Acceptable.

The PCB standard chromatogram peaks appear to be adequately
separated. Surrogate compound peaks were not identified on the
chromatogram; however, peak retention time shifts in general were
minimal.
III. Initial & Continuing Calibrations:

Qualified.

Initial calibration standards were run for Aroclors 1248 and
1260.
The percent relative standard deviations (%RSD) of the
initial calibration factors for Aroclors 1248 and 1260 both
exceeded the 10% RSD limit (RSD = 1 1 % and 18%, respectively).
Because this criterion for linearity was not met, the results are
flagged "J", as required. Daily continuing calibration check
standards were analyzed for both Aroclors. Daily continuing
calibrations check standards were analyzed for both Aroclors,
each having a percent difference (%D) from the initial
calibration of less than 15%, as required.
IV.

Analytical Error:

Precision Not Determined.

PCB matrix spike and matrix spike duplicate (MS/MSD) recoveries
were within the stated quality control limits. The MS and MSD
were prepared using sample C156830.
V.

Blanks: Acceptable.

A PCB method blank was prepared and analyzed with the samples, as
required. PCB values in both the method and calibration blanks
were below the respective detection limits.

VI.

Compound Identification:

Acceptable.

Positive identifications for PCB were verified by dual-column
analysis.
VII. Quantitation & Detection Limits:

Acceptable.

The reported values were correctly adjusted to reflect dilutions
and initial sample mass. The results are reported on dry weigh
basis.

Overall Assessment of Data:
This data evaluation is based upon guideline established in OSWER
Directive 9360-4-01 (April 1990). With the qualification
described above, the results are acceptable.

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

i
;

Receivea

HERITAGE LABORATORIES.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441

INC.

Project

\

19-MAY-94
'
complete
i 26-MAY-94

(708)378-1600

Report To

Lao 10

C156818

PO Number

VERBAL

Printed

Ol-JUN-94

i
:

Sampled
10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S40
NO.: 25 & 275

PCB SON I CAT I ON EXTRACTION SW846-3550
Analyst: S. BUSSEY

Analyst* Date: 20-MAY-94

Test: P231.1.0

Parameter

Result

Del. Limit

2.55
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

Units

Grams
mL

POLY CHLORINATED BIPHENYLS (PCBS) SH846-8080
Analyst: M. JAEGER

Analysis Date: 25 -KAY -94

Instrument: GC/ECO

Test: 0301.2.0

Prep: PCB SON 1 CAT ION EXTRACTION SU846-3550 P231.1.0
Result

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

BDL
BDL
BDL
BDL
52
BDL
5.3
BDL

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

Det. Limit

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

t

T

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

HERITAGE LABORATORIES,
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(708)378-1600

,

Project

Lab ID

19-MAY-94 i

INC.

C156820

Complete

PO Number

26 -MAY -94 i
Printed

Report To

VERBAL

i

Sampled

Ol-OUN-94 !

10-MAY-94

BUI To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: SI12
NO.: 75 & 325

PCB SONICATION EXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20 -MAY -94

Test: P231.1.0
Result

Parameter

Det.

Units

Limit

Grams

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

ml

POLYCHLORIKATED BIPHENYLS (PCBS) SW846-8080
Analyst: H. JAEGER
Analysis Date: 25 -MAY -94
Prep: PCB SONICATION EXTRACTION SW84A-3550 P231.1.0

Instrunent: GC/ECO
Result

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

BDL
BDL
BDL
BDL
110
BDL
82
BDL

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

Test: 0301.2.0
Det.

Limit

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

m

ft
tf

vV
'

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ma/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

C E R T I F I C A T E

O F

A N A L Y S I S
Received

Service Location

!
!

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(703)378-1600

i

Lab ID

19-MAY-94

Project

'

C156821

Complete

PO Number

26-MAY-94

VERBAL

Printed

!
Report To

Ol-JUN-94

Sampled

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S44
NO.: 50 & 400

PCB SON I CAT I ON EXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20 -MAY -94

Test: P231.1.0

Parameter

Result

Det. Limit

Units

Grams
mi

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME
POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080
Analyst: M. JAEGER

Analysis Date: 25 -MAY -94

Instrument: GC/ECO

Test: 0301.2.0

Prep: PCB SON I CAT I ON EXTRACTION SW846-3550 P231.1.0

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Result

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

BDL
BDL
BDL
BDL
35
BDL
7.8
BDL

Det. Limit

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

i
<>(

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

:
i

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

.

Deceived

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(708)378-1600

,

19-MAY-94

'

Complete

Project

: ci 56822
PO Number

26-MAY-94
;

Printed

Ol-JUN-94
Report To

lab 10

VERBAL
'

Sampled

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY 4 ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S51
NO.: 25 4 275

PCB SON I CAT I ONEXTRACTION SW846-3550
Analyst: 5. BUSSEY

Analysis Date: 20-MAY-94

Test: P231.T.O

Parameter

Result

Det.

Units

Limit

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

Grams
mL

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080
Analyst: M. JAEGER
Analysis Date: 25 -MAT -94
Prep: PCB SON 1 CAT I ON EXTRACTION SW846-3550 P231.1.0

!
Instrument: GC/ECO

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Result

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

BDL
BDL
BDL
BDL
53
BDL
5.4
BDL

1

Test: 0301.2.0

Det. Limit

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page 1 (last page)

,

!
i

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(708)376-1600

i

Project

tab 10

19 -MAY -94 i

C156824
PO Number

Complete

26-MAY-94

VERBAL

Printed

Sampled

Ol-JUN-94
Report To

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S68
NO.: 50 i 425

PCB SON I CAT I ONEXTRACTION SH846-3550
Analyst: S. BUSSEY

Analysis Date: 20-MAY-94

Test: P231.1.0

Parameter

Result

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME
POLYCHLORINATED BIPHENYLS (PCBS)

Units

Grams

mi

SW846-8080

Analyst: N. JAEGER
Analysis Date: 25 -MAY -94
Prep: PCB SON I CAT I ON EXTRACTION SU&W.-3550 P 231. 1.0

Instrument: GC/ECO
Result

Parame ter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Det. Limit

BDL
BDL
BDL
BDL

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

10

BDL
15
BDL

^

(T
rv
<Y
*

Test: 0301.2.0
Oet. Limit

1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page 1 (last page)

C E R T I F I C A T E
!

O F

A N A L Y S I S

Service Location

Received

'
1

HERITAGE LABORATORIES,
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441

1

(/OB)3/8-lfaUU

INC.

Project

19-MAY-94
complete
27-MAY-94

VERBAL
Sampled

Ol-JUN-94
Report To

56825

PO Number

Pr,nted

i

tab ID
Cl

!

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY 4 ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S71
NO.: 25 & 325

PCB SON I CAT I ONEXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20-MAY-94

Test: P231.1.0
Result

Parameter

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

Det.

Limit

Units

Grams

2.50
50

mL

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080
Analyst: M. JAEGER
Analysis Date: 25-MAY-94
Prep: PCB SON I CAT ION EXTRACTION SW84A-3550 P231.1.0

Instrument: GC/ECO

Result

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR

1016
1221
1232
1242
1248
1254
1260
1262

Test: 0301.2.0
Det. Limit

Units

mg/kg
mg/kg
mg/kg

*
*
*
*
*

mg/k
1.0
1.0
1.0

BDL
19 <V
BDL 1

mg/kgmg/kg
mg/kg
mq/kq

* This value is outside of the linear calibration range. The sample will
be diluted and reanalyzed.
POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080
Analyst: M. JAEGER
Analyst* Date: 25-MAY-94
Prep: PCB SON I CAT I ON EXTRACTION SU846-3S50 P231.1.0

Instrument: GC/ECD

Parameter

PCB
PCB
PCB
PCB
PCB

AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR
AROCHLOR

1016
1221
1232
1242
1248

Test: 0301.2.1
Result

BDL
BDL
BDL
BDL
280

Det. Limit

4.0
4.0
4.0
4.0
4.0

T

Units

mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

1:4 DILUTION.
or a mixture of 1242/1248
Sample shows characteristics of degraded arochlor 1248 ^
Page

1 (continued on next page)

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441

•

Received

i
|
|

19-MAY-94
complete
26-MAY-94

(/08)3/8-1600

Project

:

Report To

C156826

PO Number

VERBAL

Printed

Ol-JUN-94

Lab ID

Sampled

09-MAY-94

S i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC,
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604
Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S4
NO.: 0 & 75

PCB SON I CAT I ONEXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20-MAY-94

Test: P231.1.0
Result

Parameter

Det. Limit

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

Units

Grams
mL

POLYCHLORINATED BIPHENYLS (PCBS) SH846-8080
Analyst: H. JAEGER

Analysis Date: 25 -MAY -94

Instrument: GC/ECO

Test: 0301.2.0

Prep: PCB SONICAT10N EXTRACTION SU846-3550 P231.1.0
Result

Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Det. Limit

BDL
BDL
BDL

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

1.0

1.0
1.0
1.0
1.0
1.0
1.0
1.0

BDL ~,
35
HI
BDL 9

1.6 V
BDL ft

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

r

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

Project

Lab ID

19-MAY-94

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(708)378-1600

C156827

Complete

PO Nunber

26-MAY-94 !

VERBAL

Printed

Sampled

i Ol-JUN-94
Report To

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT,
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604

INC.

Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S90
NO.: 25 & 300

PCB SON I CAT I ON EXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20-MAT-94

Test; P231.1.0

Parameter

Del.

Result

INITIAL WEIGHT OR VOLUME
FINAL VOLUME

Limit

Units

Grams

2.50
50

mL

POLYCHLORINATEO BIPHENYLS (PCBS) SW846-8080
Analyst: M. JAEGER

Analysis Date: 25 -MAT -W

Instrument: GC/ECO

Test: 0301.2.0

Prep: PCB SON I CAT ION EXTRACTION SUMo-3550 P231.1.0
Parameter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

BDL
BDL
BDL
BDL
36
BDL

1. 0
1. 0
1. 0
1. 0

^
Qj

1. 0

U

1. 0

46 (v
BDL

1. 0
1. 0

U

Sample Comnents

BDL

Oet. Limit

Result

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262
Below Detection Limit

L

M

P*^ -J\'

' "

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg mg/kg
mg/kg
mq/kq

^''

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(705)375- 1600

Lab ID

Project

19-MAY-94

C 156828

Complete

PO Number

26-MAY-94

VERBAL

Printed

i

Sampled

Ol-JUN-94

Report To

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT,
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

INC.

Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S122
NO.: 75 & 250

PCB SON I CAT I ONEXTRACTION SW846-3550
Analyst: S. BUSSEY

Analysis Date: 20 -MAY -94

Test: P231.1.0

Parameter

Result

Units

Grams
mL

SW846-8080

Analyst: H. JAEGER
Analysis Date: 25 -MAY -94
Prep: PCB SON I CAT ION EXTRACTION SU846-3550 P231.1.0

Instrument: GC/ECD
Result

Parana ter

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Limit

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME
POLYCHLORINATED BIPHENYLS (PCBS)

Det.

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

Test: 0301.2.0
Det.

Limit

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0

BDL
BDL
BDL
BDL.
27 U
BDL
14 Of
BDL *

Units

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mq/kq

Sample Comments

BDL

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Page

1 (last page)

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

HERITAGE LABORATORIES, INC.
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441
(708)378-1600
--

--

Project

Complete

PO Number

Ol-JUN-94

Report To

10

C156830

VERBAL

Printed
_

Lab

i

26-MAY-94
- --

•,

19-MAY-94

Sampled

10-MAY-94

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT, INC,
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604

Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EW104235AA
LOCATION: S22
NO.: 25 & 400

PCB SON I CAT I ON EXTRACTION SH846-3550
Analyst: S. BUSSEY

Analysis Date: 20-MAY-94

Test: P231.1.0
Result

Parameter

2.50
50

INITIAL WEIGHT OR VOLUME
FINAL VOLUME
POLYCHLORINATED BIPHENYLS

Instrument: GC/ECO

Parameter

Test: 0301.2.0
Result

AROCHLOR 1016
AROCHLOR 1221
AROCHLOR 1232
AROCHLOR 1242
AROCHLOR 1248
AROCHLOR 1254
AROCHLOR 1260
AROCHLOR 1262

Oet. Limit
1.0
1.0
1.0
1.0

Units

mg/kg
mg/kg
mg/kg
mg/kc
1.0 mg/kg 1.0 mg/kg
1.0 mg/kg
1.0 mq/kq

BDL
BDL
BDL
BDL
21
fr
BDL *
13 O/
BDL \

'

Sample Comments

BDL

Units

Grams
ml

(PCBS) SW846-8080

Analyst: M. JAEGER
Analysis Date: 25-MAY-94
Prep: PCB SOMICATIOM EXTRACTION SU846-3550 P231.1.0

PCB
PCB
PCB
PCB
PCB
PCB
PCB
PCB

Det. Limit

Below Detection Limit

Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.

Quality Assurance Officer:

Q

Page 1 (last page)

vicin i «L rni_M CO I IWIM MUCIMOT

Office of Enforcement

77 West Jackson Boulevard
Chicago, Blinois 60604
Activity Code:

CHAIN OF CUSTODY RECORD
PROJ NO.

PROJECT NAME
NO.

SAMPLERS: (Print Name and Sign)

OF
CONTAINERS

m
DATE

STA. NO.

TIME

STATION LOCATION

O

TAG NUMBERS

ItW

5<T/

1MJS

?i WO

t10

J/22

XIC

0-1-300

Relinquished by: (Signature)

Date / Time

Received by: (Signature)

Relinquished by: (Signature)

Date / Time

Received by: (Signature)

Relinquished by: (Signature)

Date / Time

Received lor Laboratory by:
(Signature)

<>
Date / Time

ATTN.
Airbill Number
Chain of Custody Seal Numbers

Distribution White Accompanies Shipment; Pink - Coordinator Field Fites: i/YeKow - Laboratory File

prf pn Rmr vrlocl P.irifr Printprl with Sof

ecology and environment, inc.
6777 ENGLE ROAD, CLEVELAND, OHIO 44130. TEL. (216) 243-3330
International Specialists in the Environment

M

M

O

R

A

N

D

U

M

DATE:

August 3, 1994

TO:

J. Nordine, TAT Project Manager, E & E, Inc., Chicago, IL

FROM:

E.S. Landis, TAT Geochemist, E & E, Inc., Cleveland, OH

VIA:

Nabil Fayoumi, TAT Chemist, E & E, Inc., Chicago, iL

SUBJ:

Pesticides Data Quality Assurance Review, Kenosha Iron &
Metal Site, Kenosha, Kenosha County, WI

RE:

Analytical TDD: T059405802
Analytical PAN: EWI0423ABA

Project TDD: T059403013
Project PAN: EWI0423SAA

The data quality assurance review of one discrete soil sample
analyzed for organochlorine
pesticides
(chlordane),
is now
complete. The sample was submitted to Heritage Laboratories, Inc.
of Romeoville, Illinois (HLI) on May 19, 1994, to be analyzed for
organochlorine pesticides by the SW-846 8080 Method. IN turn, HLI
subcontracted the work to Environmental Monitoring Technologies,
Inc. of Morton Grove, Illinois (EMT). EMT followed EPA Method 608,
employing a gas chromatograph with electron capture and flame
ionization detectors (GC/ECD/FID). The sample was labeled S48,
corresponding to HLI's number, C156831.
Data Qualifications:

I.

Sample Holding Times: Acceptable.

The sample was collected at the Kenosha Iron & Metal site in
Kenosha, Wisconsin, on May 10, 1994. The HLI report noted that the
sample was received in an improper container.
The sample was
extracted May 20, and analyzed May 23, 1994. The sample was
handled in compliance with the respective 14-day and 40-day holding
time limits for extraction and analysis.
II.

Instrument Performance:

Acceptable.

The DDT peak retention time was greater than 12 minutes, as
recommended.
Pesticide standard peaks appear to have been
adequately resolved and were within the stated retention time

recycled o*D*f

windows. Internal standard reference peaks varied by less than the
1.5% limit between the standard and sample . [Evaluation Standard
Mixes A or B were not identified; therefore, the reviewer is unable
to calculate the DDT and Endrin percent breakdown.]
III. Initial & Continuing Calibrations:

Acceptable.

Percent relative standard deviation (%RSD) values of calibration
factors for aldrin, endrin, DEC, and DDT were not reported in EMT's
pesticide data packet. The correlation coefficients of eight peaks
for five standard concentrations of chlordane were greater than or
equal to 0.995 for the initial calibration, indicating that the
calibration for chlordane was linear.
A daily (continuing)
calibration standard run with the sample. Chlordane peak retention
time shifts between the standards and the sample were less than
15%, as required for the quantitation column.
IV.

Analytical Error:

Precision Not Determined.

Surrogate compounds were diluted beyond the lower detection limit.
V.

Blank: Acceptable.

No pesticide compounds were detected in the blank.
VI.

Compound Identification:

Acceptable.

Identification of chlordane was based on a multi-peak pattern
matching the initial calibration. A dual-column GC was used to
verify the compound identification.
VII. Quantitation & Detection Limits:

Acceptable.

Sample values were adjusted to reflect the extraction volume,
sample mass, and dilutions required to conduct the analysis. The
results are reported on a dry-weight basis.
Overall Assessment of Data:
This data evaluation is based upon guidelines established in OSWER
Directive 9360.4-01 (April 1990) and SW-846 "Test Methods for the
Evaluation of Solid Waste", (1986, 3rd ed.). Given the information
provided, the results may be considered acceptable for use as
reported.

C E R T I F I C A T E

O F

A N A L Y S I S

Service Location

Received

HERITAGE LABORATORIES,
1319 MARQUETTE DRIVE
ROMEOVILLE, IL 60441

INC.

19-MAY-94
complete
| 06-JUN-94

(708)3/8-1600

Printed

Project

Lab ID

C 156831
PO Nuifcer

VERBAL
Sampled

07-JUN-94
Report To

B i l l To

MARY JANE RIPP
ECOLOGY AND ENVIRONMENT,
111 WEST JACKSON BLVD.
CHICAGO, IL 60604

ACCOUNTS PAYABLE
ECOLOGY AND ENVIRONMENT, INC.
Ill WEST JACKSON BLVD.
CHICAGO, IL 60604

INC.

Sample Description

PROJECT
PROJECT
STATION
STATION

NAME: ECOLOGY & ENVIRONMENT - T05-9405-802
NO.: EWI04235AA
LOCATION: S48
NO.: 0 4 300

ORGANOCHLORINE PESTICIDES BY GC:ECD (7 PESTICIDES) SH846-8080
Analysis Date: 25 -MAY -94

Vendor: ENVIRONMENTAL MONITORING t TECHNOLOGIES
Parameter

Result

< 600
< 1200
< 400

GAMMA-BHC (LINDANE)
HEPTACHLOR
HEPTACHLOR EPOXIDE
ENDRIN
METHOXYCHLOR
CHLORDANE
TOXAPHENE

< 2000
< 2000
35000
< 10000

Test: 0164.3.0
Det. Limit

600
1200
400
2000
2000
5200
10000

Units

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uq/kq

Sample Comments

Less Than Lower Detection Limit
Sample was received in improper container.
Sample chain of custody number 5-34715.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.
As indicated, some testing was performed at the following locations:
ENVIRONMENTAL MONITORING & TECHNOLOGIES
8100 NORTH AUSTIN AVENUE, MORTON GROVE, IL 60053-3203

Quality Assurance Officer:

( &*>.<>)

Page 1 (last page)

;

APPENDIX C
TAT XRF 920 FIELD DATA

20

TAT XRF 920 SOIL SAMPLE DATA
KENOSHA IRON & METAL, KENOSHA, WISCONSIN
HAY 1994
SAMPLE
COORDINATES

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

0+0
ASSAY
STANDARD

0-1

0.0
0.007

0.0
0.002

1,296
31.64

20225
0.039

0+0

1-1.5

0.0
0.007

0.0
0.002

1,709
40.81

2.430
0.018

0+25

0-1

0.0
0.008

0.0
0.002

1,597
38.20

2.391
0.022

0+25

1-1.5

0.0
0.007

0.0
0.002

1,231
29.87

2.159
0.048

0+50

0-1

0.0
0.008

0.0
0.003

1,376
33.36

2.281
0.018

0+50

0-1.5

0.0
0.007

0.0
0.002

1,054
24.83

1.835
0.085

0+75

0-1

0.0
0.007

0.0
0.002

1,190
28.63

2.096
0.055

0+75

1-1.5

0.0
0.008

0.011
0.003

1,282
29.93

2.049
0.046

0+100

0-1

0.0
0.008

0.0
0.003

1,205
28.35

2.107
0.0352

0+100

1-2

0.0
0.008

0.0
0.002

1,340
31.02

2.207
0.046

0+125

0-1

0.0
0.007

0.0
0.003

1,209
29.07

2.118
0.049

0+125

1-2

0.0
0.007

0.0
0.002

1,024
23.28

1.530
0.115

0+150

0-1

0.0
0.008

0.105
0.003

882.2
20.86

1.818
0.017

0+150

1-2

0.0
0.008

0.0
0.003

839.5
19.10

1.719
0.076

0+175

0-1

0.0
0.007

0.0
0.003

862.8
19.88

1.607
0.098

0+175

1-2

0.0
0.008

0.001
0.003

1,130
27.02

2.034
0.032

0+200

0-1

0.0
0.007

0.0
0.003

727.5
15.74

1.299
0.120

SAMPLE
COORDINATES

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

0-1-200

1-2

0.0
0.007

0.014
0.003

857.6
19.34

1.590
0.088

0+225

0-1

0.0
0.005

0.140
0.002

542.5
5.899

0.0
0.205

0+225

1-2

0.0
0.007

0.0
0.002

406.3
0.979

0.0
0.254

0+250

0-1

0.0
0.008

0.087
0.003

450.3
1.180

0.0
0.325

0+250

1-2

0.0
0.007

0.0
0.003

753.0
17.52

1.615
0.090

0+275

0-1

0.0
0.008

0.031
0.003

586.0
9.223

0.537
0.165

0+275

1-2

0.0
0.007

0.0
0.003

626.5
10.15

0.579
0.140

25+0

0-1

0.0
0.007

0.0
0.002

485.5
7.264

0.150
0.166

25+0

1-2

0.0
0.007

0.0
0.002

454.7
5.302

0.0
0.193

0+200

0-1

0.009
0.008

0.162
0.001

626.5
7.968

0.579
0.140

0+200

1-2

0.0
0.008

0.0
0.002

500.3
6.802

0.182
0.197

TAT XRF 920 SOIL SAMPLE DATA
KENOSHA IRON fc METAL, KENOSHA, WISCONSIN
MAY 1994 (Cont.)

SAMPLE
COORDINATE
-25+100

DEPTH
IN
FEET
1-.5

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

0.0
0.007

0.0
0.003

2,252
50.27

2.601
0.017

Black

-22+0

0-.5

0.0
0.007

0.0
0.003

1,723
41.41

2.302
0.016

BROWN

-25+175

0-.5

0.0
0.007

0.0
0.002

1,545
39.28

2.361
0.032

TAN

-25+150

0-.5

0.0
0.007

0.0
0.003

2,479
59.82

2.559
0.035

BROWN

0-.5

0.0
0.007

0.0
0.003

1.949
46.33

2,497 .
0.016

BROWN

+25+150

0-1

0.014
0.009

0.609
0.008

2,538
72.79

0.889
0.164

BLACK

+25+150

0-2

0.0
0.008

0.0
0.003

3,035
69.06

2.422
0.078

BLACK

25+25

1-2

0.0
0.008

0.0
0.003

xxxxx

0.0
0.369

BROWN
& TAN

0.0
0.008

0.0
0.003

XXXXX

0.0
0.312

BROWN

208.4

-25+200

25+25

0-1

262.5

25+50

0-1

0.0
0.008

0.0
0.003

7,720
156.2

0.890
0.249

BROWN

25+50

1-2

0.0
0.007

0.0
0.003

6,244
128.3

1.559
0.202

TAN

25+75

0-1

0.0
0.008

0.08
0.004

5,561
119.9

1.792
0.158

BROWN

25+75

1-2

0.0
0.008

0.0
0.003

4,846
103.3

1.761
0.180

BROWN

25+100

0-1

0.0
0.008

0.289
0.003

5,664
124.7

0.905
0.209

BLACK

25+100

1-2

0.0
0.007

0.0
0.003

4,387
95.05

2.258
0.128

BLACK

25+125

0-1

0.0
0.008

0.280
0.005

3.435
88.80

1.268
0.162

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

25+125

1-2

0.0
0.008

0.0
0.003

3.537
82.12

1.773
0.160

BLACK

25+175

0-1

0.039
0.009

0.571
0.007

2,375
65.93

1.044
0.143

BLACK

25+125

1-2

0.0
0.008

0.136
0.003

3.877
86.02

1,638
0.159

BLACK

25+200

0-1

0.051
0.009

0.592
0.009

2,157
65.36

0.766
0.173

BLACK

25+200

1-2

0.0
0.008

0.207
0.003

2,736
65.32

1.765
0.107

BLACK

25+225

0-1

0.126
0.010

0.718
0.017

0.0
0.332

BLACK

385.9

25+225

1-2

0.025
0.009

0.420
0.011

8,756
258.2

0.0
0.273

BLACK

25+325

0-1

0.084
0.010

0.941
0.014

2,562
81.02

0.0
0.290

BLACK

25+325

1-2

0.0
0.007

0.0
0.004

2,754
70.94

2.170
0.087

BLACK

25+250

0-1

0.044
0.009

0.335
0.007

1,734
53.11

1.426
0.117

BLACK

25+250

1-2

0.0
0.008

0.0
0.003

5,448
115.8

1.631
0.187

BLACK

25+275

0-1

0.0
0.009

0.551
0.010

2,481
80.81

0.0
0.250

BLACK

25+275

1-2

0.0
0.009

0.683
0.011

4,248
131.0

0.096
0.237

BLACK

25+300

0-1

0.053
0.009

0.334
0.008

1,753
55.98

1.364
0.124

BLACK

25+300

11.5

0.146
0.010

0.432
0.010

1,460
48.11

0.234
0.214

BLACK

25+325

0-1

0.084
0.010

0.941
0.014

2,562
81.02

0.0
0.290

BLACK

25+325

1-2

0.0
0.007

0.0
0.004

2,754
70.94

2.170
0.087

BLACK

25+350

0-1

0.033
0.009

0.586
0.013

7,596
232.7

0.0
0.290

BLACK

25+350

1-2

0.027
0.009

0.626
0.014

9,000
276.1

0.0
0.248

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

25+375

0-1

0.149
0.010

0.669
0.012

1,713
54.57

0.191
0.212

BLACK

25+375

1-2

0.107
0.009

0.523
0.009

2,085
64.66

1.241
0.124

BLACK

25+400

0-1

0.0
0.009

0.570
0.010

5,323
157.0

0.152
0.239

BLACK

25+400

1-2

0.0
0.008

0.485
0.011

0.0
0.290

BLACK

395.7

25+425

0-1

0.013
0.008

0.199
0.005

1,089
29.95

1.738
0.066

BLACK

25+425

1-2

0.063
0.009

0.663
0.013

2,448
84.61

0.124
0.226

BLACK

25+450

0-1

0.086
0.010

0.061
0.009

1,881
76.86

0.0
0.263

BLACK

25+450

1-2

0.008
0.008

0.0
0.003

2,460
61.82

2.335
0.069

BLACK

50+0

1-2

0.0
0.007

0.0
0.002

1,858
44.31

2,486
0.023

TAN

50+0

0-1

0.0
0.007

0.0
0.003

1,973
47.22

2.479
0.034

TAN

50+25

0-1

0.0
0.007

0.0
0.003

2,496
57.74

2.491
0.058

BROWN

50+25

1-2

0.0
0.007

0.0
0.003

2,122
49.65

2.544
0.019

BLACK

50+50

0-1

0.0
0.008

0.0
0.003

2,283
53.22

2,453
0.062

BROWN

50+50

1-2

0.0
0.007

0.0
0.002

2,182
50.92

2.573
0.027

TAN

50+75

0-1

0.02
0.009

0.503
0.007

1,125
25.53

1.081
0.127

BLACK

50+75

1-2

0.0
0.007

0.0
0.002

1,956
46.98

2.510
0.022

TAN

50+100

0-1

0.0
0.007

0.0
0.003

2,193
53.79

2.493
0.026

BLACK

50+100

1-2

0.0
0.007

0.0
0.003

2,027
48.37

2.464
0.041

BLACK

50=125

0-1

0.0
0.008

0.074
0.004

2,051
52.29

2.153
0.054

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

50+125

1-2

0.0
0.007

0.0
0.003

2,348
56.25

2.494
0.033

BLACK

50+150

0-1

0.0
0.008

0.0
0.003

2,723
63.33

2.264
0.086

BLACK

50+150

1-2

0.0
0.008

0.0
0.003

2,717
66.95

2.330
0.073

BLACK

50+175

0-1

0.0
0.008

0.231
0.003

2,980
72.29

1.649
0.125

BLACK

50+175

1-2

0.0
0.008

0.082
0.004

3,082
72.95

2.157
0.088

BLACK

50+200

0-1

0.010
0.008

0.365
0.006

3,307
90.18

1.434
0.134

BLACK

50+200

1-2

0.0
0.008

0.063
0.003

2,916
54.81

2.640
0.056

BLACK

50+225

0-1

0.036
0.009

0.328
0.007

2,264
67.44

1.213
0.148

BLACK

50+225

1-2

0.016
0.008

0.214
0.006

978.9
26.19

1.647
0.077

BLACK

50+250

0-1

0.067
0.009

0.548
0.010

2,353
76.05

0.745
0.178

BLACK

-50+250

-1-2

0.044
0.009

0.335
0.007

1,734
53.11

1.426
0.117

BLACK

50+275

0-1

0.0
0.008

0.422
0.008

2,659
82.50

0.796
0.188

BLACK

50+275

1-2

0.004
0.008

0.085
0.003

786.2
17.03

1.696
0.031

BLACK

50+300

0-1

0.0
0.008

0.466
0.009

3,001
95.34

0.974
0.171

BLACK

50+300

1-2

0.0
0.008

0.175
0.005

2,524
70.08

1.671
0.119

BLACK

50+325

0-1

0.0
0.009

0.660
0.010

2,929
90.19

0.0
0.315

TAN

50+325

1-2

0.052
0.009

0.244
0.003

845.7
16.68

1.548
0.016

BLACK

50+350

0-1

0.057
0.010

0.596
0.009

1,576
45.49

0.493
0.193

BLACK

50+350

1-2

0.040
0.009

0.566
0.009

2,040
61.12

0.694
0.181

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

50+375

0-1

0.026
0.009

0.582
0.010

2,103
66.14

0.151
0.229

BLACK

-50+375

-1-2

0.107
0.009

0.523
0.009

2,085
64.66

1.241
0.124

BLACK

50+400

0-1

0.050
0.009

0.534
0.009

2,127
66.01

0.537
0.198

BLACK

50+400

1-2

0.036
0.009

0.586
0.010

2,628
82.63

0.017
0.192

BROWN

50+425

0-1

0.024
0.009

0.505
0.009

3,301
100.1

0.854
0.179

BLACK

50+425

1-2

0.062
0.009

0.446
0.007

3,000
84.92

0.969
0.167

BLACK

50+450

0-1

0.050
0.009

0.469
0.010

2,555
85.72

0.482
0.206

BLACK

75+0

0-1

0.0
0.008

0.055
0.003

2,215
53.50

2.146
0.075

BLACK

75+25

0-1

0.021
0.008

0.486
0.006

1,973
54.32

1.545
0.083

BROWN

75+25

1-2

0.024
0.008

0.479
0.006

1,990
52.34

1.424
0.090

BLACK

75+50

0-1

0.004
0.008

0.360
0.004

1,862
47.16

1.449
0.094

BLACK

75+50

1-2

0.0
0.007

0.0
0.002

1,573
37.53

2.376
0.024

TAN

75+75

0-1

0.023
0.009

0.426
0.005

1,105
23.76

0.839
0.151

BROWN

75+75

1-2

0.0
0.007

0.0
0.002

997.2
24.13

1.852
0.079

TAN

75+100

0-1

0.0
0.008

0.194
0.004

1,883
49.39

1.627
0.112

BLACK

75+100

1-2

0.0
0.007

0.0
0.003

4,260
90.99

2.435
0.114

TAN

75+125

0-1

0.034
0.008

0.386
0.005

2,035
55.69

1.528
0.096

BLACK

75+125

1-2

0.0
0.008

0.156
0.004

2,346
61.42

1.856
0.096

BLACK

75+150

0-1

0.015
0.009

0.632
0.013

0.0
0.355

BLACK

501.0

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

75+150

1-2

0.0
0.009

0.386
0.009

0.0
0.364

BLACK

460.8

75+175

0-1

0.086
0.009

0.694
0.010

3,163
92.95

0.638
0.182

BLACK

75+175

1-2

0.055
0.009

0.418
0.005

1,789
47.87

1.423
0.095

BLACK

75+200

0-1

0.081
0.010

0.458
0.006

957.4
16.42

0.626
0.164

BROWN

75+200

1-2

0.0
0.009

0.496
0.009

0.0
0.352

BLACK

294.8

75+225

0-1

0.178
0.011

0.460
0.008

1,441
41.47

0.564
0.181

BLACK

75+225

1-2

0.122
0.010

0.574
0.008

1,856
51.17

0.273
0.207

BLACK

75+250

0-1

0.319
0.013

0.503
0.009

1,005
22.43

0.0
0.284

BLACK

75+250

1-2

0.156
0.011

0.635
0.011

3,333
104.6

0.0
0.299

BLACK

75+275

0-1

0.100
0.011

0.383
0.007

789.5
11.26

0.0
0.285

BLACK

75+275

1-2

0.061
0.009

0.617
0.011

4,008
124.6

0.175
0.228

BLACK

75+300

0-1

0.0
0.009

0.728
0.015

0.0
0.435

BLACK

311.7

0.0
0.009

0.039
0.004

0.0
0.422

BLACK

249.2

75+300

1-2

75+325

0-1

0.057
0.010

0.765
0.011

2,654
82.08

0.0
0.247

BLACK

75+325

1-2

0.010
0.009

0.559
0.010

2.755
85.64

0.037
0.243

BLACK

75+350

0-1

0.009
0.008

0.738
0.013

6,807
203.8

0.252
0.225

BLACK

75+350

1-2

0.0
0.008

0.072
0.005

7,023
159.7

0.067
0.281

BLACK

75+375

0-1

0.063
0.010

0.784
0.014

5,364
174.8

0.0
0.287

BROWN

75+375

1-2

0.049
0.009

0.546
0.011

4,234
132.9

0.012
0.243

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DBS CRIP

75+400

0-1

0.079
0.010

0.786
0.014

2,712
91.80

0.123
0.223

BLACK

75+400

1-2

0.097
0.010

0.867
0.019

7,843
278.9

0.0
0.299

BROWN

754-425

0-1

0.039
0.009

0.560
0.011

1,719
56.17

0.373
0.209

BLACK

75+425

1-2

0.0
0.007

0.0
0.002

815.9
18.10

1.480
0.114

TAN

75+450

0-1

0.0
0.008

0.112
0.008

7,278
205.2

0.617
0.216

BLACK

75+450

1-2

0.016
0.009

0.347
0.007

1,202
33.78

1.304
0.122

BLACK

100+0

0-1

0.0
0.007

0.0
0.003

1,597
38.90

2.317
0.025

TAN

100+0

1-2

0.0
0.007

0.030
0.003

1,929
48.59

2.249
0.039

BLACK

100+25

0-1

0.0
0.007

0.0
0.003

1,532
37.40

2.306
0.029

TAN

100+25

1-2

0.0
0.007

0.0
0.002

1,189
28.95

2.066
0.061

TAN

100+50

0-1

0.01
0.008

0.301
0.004

1,642
44.15

1.742
0.063

BROWN

100+50

1-2

0.0
0.008

0.0
0.002

1,612
39.50

2.376
0.030

TAN

100+75

0-1

0.0
0.008

0.275
0.005

2,026
56.56

1,638
0.102

BLACK

100+75

1-2

0.0
0.007

0.0
0.002

2,368
55.96

2.615
0.024

TAN

100+100

0-1

0.007
0.008

0.283
0.005

2,213
61.32

1.722
0.093

BLACK

100+100

1-2

0.0
0.007

0.0
0.002

2,251
54.05

2.514
0.048

TAN

100+125

0-1

0.0
0.007

0.0
0.004

1,808
47.06

2.201
0.053

BLACK

100+125

1-2

0.0
0.008

0.0
0.003

23.06
60.03

2.284
0.067

BLACK

100+150

0-1

0.0
0.007

0.189
0.004

2,586
66.27

2.140
0.050

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

100+150

1-2

0.0
0.008

0.0
0.003

2,206
52.85

2.332
0.053

BLACK

100+175

0-1

0.0
0.008

0.558
0.008

2,153
61.56

1.079
0.146

BLACK

100+175

1-2

0.0
0.008

0.195
0.001

1,905
44.32

1.750
0.076

BLACK

100+200

0-1

0.0
0.008

0.391
0.008

1,933
59.23

1.343
0.130

BLACK

100+200

1-2

0.0
0.010

0.400
0.008

2.092
64.35

0.0
0.418

BLACK

109.7+225

0-1

0.101
0.009

0.499
0.010

1,885
61.37

1.381
0.111

BLACK

109.7+225

1-2

0.043
0.009

0.173
0.006

1,361
40.89

1.206
0.148

BLACK

100+275

0-1

0.0
0.007

0.0
0.003

1,507
38.01

2.345
0.016

BLACK

100+375

1-2

0.005
0.007

0.0
0.004

2,065
55.01

2.344
0.040

BLACK

100+400

0-1

0.0
0.007

0.0
0.003

2,340
56.11

2.521
0.033

BLACK

100+400

1-2

0.0
0.007

0.0
0.003

2,245
55.12

2.369
0.058

BLACK

100+425

0-1

0.0
0.007

0.0
0.003

2,111
52.57

2.518
0.024

BLACK

100+425

1-2

0.0
0.007

0.0
0.003

27.24
64.46

2.432
0.063

BLACK

100+450

0-1

0.006
0.008

0.0
0.004

2,202
60.02

2.187
0.062

BLACK

100+450

1-2

0.0
0.007

0.108
0.004

2,402
60.07

2.136
0.065

BLACK

111.5+250

0-1

0.007
0.008

0.028
0.003

3,448
74.77

2.212
0.107

BLACK

111.5+250

1-2

0.009
0.007

0.0
0.003

3,182
76.67

2.643
0.040

BLACK

113.4+300

0-1

0.005
0.007

0.0
0.004

2,525
66.42

2.309
0.066

113.4+300

1-2

0.0
0.007

0.0
0.003

1,346
38.18

2.250
0.024

BLACK
BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

113+275

0-1

0.0
0.007

0.0
0.003

2,202
56.06

2.344
0.061

BLACK

113+275

1-2

0.0
0.007

0.0
0.003

3,257
69.90

2.608
0.069

BLACK

116+325

0-1

0.0
0.007

0.0
0.003

2,601
66.86

2.407
0.068

BLACK

114.8+225

0-1

0.0
0.007

0.0
0.002

2,365
56.89

2.627
0.018

BLACK

116+350

1-2

0.0
0.007

0.0
0.003

2,474
65.13

2.377
0.065

BLACK

125+0

0-1

0.006
0.008

0.159
0.004

1,851
47.88

2.014
0.047

BLACK

125+100

0-1

0.006
0.009

0.362
0.004

3,059
77.70

1.257
0.145

BLACK

125+100

1-2

0.0
0.008

0.0
0.004

3,254
78.88

2.142
0.102

BLACK

125+125

0-1

0.0
0.008

0.242
0.003

3.029
74.94

1.852
0.097

BLACK

125+125

1-2

0.0
0.008

0.061
0.003

2,468
55.17

2.355
0.048

BLACK

125+150

0-1

0.033
0.008

0.652
0.011

2,471
77.95

1.211
0.133

BLACK

125+150

1-2

0.0
0.008

0.037
0.004

1,780
46.82

2.161
0.047

BLACK

125+175

0-1

0.010
0.009

0.635
0.009

1,944
36.38

0.537
0.193

BROWN

125+175

1-2

0.0
0.009

0.272
0.005

1,883
53.22

1.224
0.150

BLACK

125+200

0-1

0.003
0.007

0.009
0.004

2,283
61.40

2.204
0.061

BLACK

125+200

1-2

0.0
0.007

0.0
0.003

2,275
56.43

2.385
0.044

BLACK

125+225

0-1

0.0
0.007

0.0
0.004

3,262
81.43

2.167
0.100

BLACK

125+225

0-1

0.0
0.008

0.0
0.003

3,740
94.56

1.970
0.131

BLACK

125+250

0-1

0.0
0.007

0.0
0.003

2,856
74.37

2.161
0.100

BLACK

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

125+250

1-2

0.0
0.007

0.0
0.003

2,349
60.02

2.365
0.063

BLACK

125+275

0-1

0.0
0.008

0.0
0.003

2,065
35.58

2.315
0.059

BLACK

125+275

1-2

0.0
0.007

0.0
0.003

2,194
57.85

2.278
0.070

BLACK

125+300

0-1

0.0
0.007

0.0
0.003

1,812
44.52

2.439
0.017

BLACK

125+300

1-2

0.0
0.007

0.0
0.003

2,147
56.60

2.364
0.050

BLACK

125+325

0-1

0.0
0.007

0.0
0.003

1,522
37.52

2,306
0.031

TAN

125+325

1-2

0.0
0.007

0.0
0.002

1,706
41.77

2.417
0.025

BLACK

125+350

0-1

0.0
0.007

0.0
0.003

3,187
75.77

2.568
0.068

BLACK

125+350

1-2

0.0
0.007

0.0
0.003

2.088
56.50

2.296
0.062

BLACK

125+375

0-1

0.0
0.007

0.0
0.003

3,369
84.16

2.388
0.079

BLACK

125+375

1-2

0.0
0.007

0.0
0.003

2,885
80.01

2.173
0.094

BLACK

125+400

0-1

0.0
0.007

0.021
0.003

2,529
61.20

2.422
0.032

BLACK

125+400

1-2

0.0
0.007

0.023
0.004

2,857
69.24

2.289
0.074

BLACK

125+425

0-1

0.0
0.007

0.0
0.004

2,520
62.46

2.438
0.037

BLACK

125+425

1-2

0.0
0.008

0.0
0.003

2,299
56.90

2.323
0.052

BLACK

125+450

0-1

0.007
0.008

0.245
0.007

2,434
56.65

1.545
0.022

BLACK

125+450

1-2

0.053
0.010

0.0
0.156

6,202
91.03

0.0
0.71

BROWN

0+450

0-1

0.0
0.007

0.045
0.003

1,581
37.95

2.187
0.022

BLACK

0+450

1-2

0.0
0.007

0.0
0.003

1,426
34.11

2.213
0.043

BLACK

[

SAMPLE
COORDINATE

DEPTH
IN
FEET

CHROMIUM
IN %

LEAD
IN %

BARIUM
IN PPM

MERCURY
IN PPM

SAMPLE
DESCRIP

150+0

0-1

0.0
0.007

0.043
0.003

1,100
26.61

1.942
0.040

BLACK

150+0

1-2

0.0
0.007

0.0
0.002

1,407
34.55

2.293
0.034

TAN

APPENDIX D
SOIL SAMPLE PCB DATA FROM TAT FASP LABORATORY

22

SOIL SAMPLE PCS DATA FROM TAT FASP LABORATORY
KENOSHA IRON t METAL, KENOSEA, WISCONSIN
MAY 1994
LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

SI

50+0

0-1

ND

ND

S2

50+0

1-2

ND

ND

S3

75+0

0-1

1254/1260

1

S4

0+75

1-1.5

1248

31

S5

25+0

1-2

1260

(T)

56

0+25

0-1

ND

ND

S7

0-10

1-1.5

ND

ND

S8

0+50

1-1.5

ND

ND

S9

0+50

0-1

ND

ND

S10

0+0

0-1

ND

ND

Sll

75+0

1-2

ND

ND

S12

0+75

0-1

1248

(T)

S13

100+0

1-2

1254

(T)

S14

100+0

0-1

1254/1260

(T)

S15

125+0

1-2

1254

(T)

S16

25+0

0-1

ND

ND

S17

150+0

0-1

ND

ND

S18

0+25

1-1.5

ND

ND

S19

125+0

0-1

1254/1260

3

S20

150+0

1-2

ND

ND

S21

25+375

0-1

1254/1260

7

S22

25+400

0-1

1254/1260

18

S23

0+250

1-2

ND

ND

S24

0+225

0-1

ND

ND

S25

0+275

0-1

ND

ND

S26

25+225

1-2

ND

8

CONCENTRATION

(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

S27

0+100

0-1

1248

3

S28

0+100

1-2

ND

ND

S29

0+125

0-1

ND

ND

S30

0+125

1-2

ND

ND

S31

5+450

0-1

1254

12

S32

0+150

0-1

1254/1260

T

S33

25+200

1-2

ND

ND

S34

0+150

1-2

ND

ND

S35

25+125

0-1

1254

11

S36

0+275

0-1

1254/1260

(T)

S37

25+350

0-1

1254/1260

12

S38

25+200

0-1

1254/1260

(5-10)

S39

50+275

0-1

1248

16

S40

25-275

0-1

1248

25

S41

25+425

1-2

1254/1260

18

S42

0+250

0-1

ND

ND

S43

25+425

0-1

1254/1260

7

S44

50+400

0-1

1248/1260

16

S45

50+350

1-2

1254/1260

12

S46

50+375

0-1

1254/1260

21

S47

0-450

1-2

ND

ND

S48

0+300

0-1

ND

CONTAINS
CHLOROANE

S49

0+300

1-2

ND

ND

S50

50+350

0-1

1248/54/60

18

S51

25+275

1-2

1248

48

S52

50+300

0-1

1248

52

S53

25+225

0-1

1254/1260

10

S54

25-100

1-2

ND

ND

S55

25-100

' 0-1

1254/1260

7

CONCENTRATION
(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

S56

25+125

1-2

ND

ND

S57

0+175

0-1

ND

ND

S58

25+75

0-1

ND

ND

S59

25+75

1-2

ND

ND

S60

50+225

0-1

ND

ND

S61

0+225

1-2

ND

ND

S62

0+450

0-1

ND

ND

S63

0-200

0-1

ND

ND

S64

0+200

1-2

ND

ND

S65

0+175

1-2

ND

ND

S66

25+150

1-2

ND

ND

S67

25+150

0-1

ND

ND

S68

50-425

0-1

1248/1260

28

S69

25+400

1-2

1248/1260

30

S70

50+250

0-1

1254/1260

11

S71

25+325

0-1

1248

72

S72

25+375

1-2

1254/1260

18

S73

25+450

0-1

ND

ND

S74

25+300

0-1

1254/1260

40

S75

25-175

1-2

1254/1260

(T)

S76

50+325

0-1

1248/54/60

34

S77

50+300

1-2

1248

100+

S78

25+250

0-1

1248/54/60

(5-10)

S79

50-425

1-2

1254

15

S80

50-450

1-2

1248/1260

(5-10)

S81

25-50

1-2

ND

ND

S82

25+25

1-2

ND

ND

S83

25+350

.5-1

1248/54/60

36

S84

25+250

1-2

ND

ND

CONCENTRATION
(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

CONCENTRATION

S85

25+325

1-2

1248

37

S86

25+25

0-1

ND

ND

S87

25+175

0-1

1248/54/60

(5-10)

S88

25+450

1-2

ND

ND

S89

50-400

1-2

1248/1260

26

S90

25-300

.5-1

1248/54/60

54

S91

25-50

0-1

ND

ND

S92

125+450

0-1

ND

ND

S93

125+400

0-1

ND

ND

S94

125+400

1-2

ND

ND

S95

125+425

0-1

ND

ND

S96

125+425

1-2

ND

ND

S97

125+450

1-2

ND

ND

S98

100+450

1-2

ND

ND

S99

100+450

0-1

ND

ND

S100

75+400

0-1

1248/54/60

28

S101

75+400

1-2

1248/54/60

26

S102

75+450

1-2

1254

19

S103

75+425

1-2

1254/1260

18

S104

75+450

0-1

1248/54/60

8

S105

100+400

1-2

ND

ND

S106

100+425

1-2

ND

ND

S107

100+425

0-1

ND

ND

S108

100+400

0-1

ND

ND

S109

75+425

0-1

1254/1260

12

S110

75-100

0-1

1248/54/60

16

Sill

-25+200

0-.5

ND

ND

S112

75+325

1-2

1248/54/60

124

S113

75+200

1-2

1248/54/60

18

(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

S114

116+350

0-1

ND

ND

S115

100+125

0-1

1248/54/60

(5-10)

S116

-25+75

S117

75+125

1-2

1248/54/60

16

3118

-25+100

0-.5

ND

ND

S119

100+150

1-2

ND

ND

S120

75+250

0-1

1248/54/60

28

S121

100+375

1-2

ND

ND

S122

75+250

1-2

1248/54/60

34

S123

75+75

0-1

1254/1260

18

S124

75+25

1-2

ND

ND

S125

100+150

0-1

1248

26

S126

75+300

1-2

1248

49

S127

108+375

1-2

1254/1260

6

S128

75+300

0-1

1248/1260

92

S129

75-75

1-2

1254/1260

14

S130

75+50

1-2

ND

ND

S131

75-25

0-1

1248/54/60

(5-10)

S132

75-200

0-1

1248/54/60

38

S133

113.4+300

0-1

ND

ND

S134

114.8+325

1-2

ND

ND

S135

100+125

1-2

ND

ND

S136

100+100

1-2

ND

ND

S137

113+275

1-2

ND

ND

S138

75+325

0-1

1248/54/60

70

S139

75+275

0-1

1248/54/60

41

S140

75+350

0-1

1248/54/60

28

S141

100+375

0-1

ND

ND

S142

109.6+200

0-1

1248/54/60

32

CONCENTRATION
(IN PPM)

NO

CONCENTRATION

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FT)

SAMPLE
DEPTH
(IN FT)

PCB

S170

116+325

1-2

ND

ND

5/11/94

S171

125+350

0-1

ND

ND

5/11/94

S172

125+175

0-1

1254/1260

(T)

5/11/94

S173

50+50

1-2

ND

ND

5/10/94

S174

125+200

1-2

ND

ND

5/11/94

S175

100+25

0-1

ND

ND

5/11/94

S176

75+225

1-2

1248/54/60

37

5/10/94

S177

175+275

0-1

ND

ND

5/11/94

S178

75+375

0-1

1248/54/60

38

5/10/94

S179

100+100

0-1

1248/54/60

8

5/11/94

S180

75+350

1-2

1248

34

5/10/94

S181

125+100

0-1

1254/1260

23

5/11/94

S182

125+200

0-1

ND

ND

5/11/94

S183

125+325

1-2

ND

ND

5/11/94

S184

125+225

1-2

ND

ND

5/11/94

S185

50+125

0-1

1248/54/60

14

5/10/94

S186

50+200

1-2

ND

ND

5/10/94

S187

125+225

0-1

ND

ND

5/11/94

S188

50+100

1-2

ND

ND

5/10/94

S189

125+375

0-1

ND

ND

5/11/94

S190

50+150

1-2

ND

ND

5/10/94

S191

125+325

1-2

ND

ND

5/11/94

S192

50+75

0-1

1254/1260

26

5/10/94

S193

125+325

0-1

ND

ND

5/11/94

S194

125+150

1-2

ND

ND

5/11/94

S195

125+275

1-2

ND

ND

5/11/94

S196

125+100

1-2

1254/1260

5

5/11/94

S197

125+150

0-1

1248/54/60

16

5/11/94

DATE

(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FEET)

SAMPLE
DEPTH
(IN FEET)

PCB

S143

111.5+250

0-1

1248/54/60

(5-10)

S144

109.74-225

1-2

1254/1260

13

S145

109.7+225

0-1

1254/1260

11

S146

75+50

0-1

1254/1260

(5-10)

S147

-22+50

0-.5

ND

ND

S148

75+275

1-2

1254/1260

29

S149

75-175

0-1

1248/54/60

18

S150

75+375

1-2

1248/54/60

15

S151

109.6+200

1-2

1254/1260

25

S152

100+50

1-2

ND

ND

S153

75+225

0-1

1248/54/60

26

S154

75+150

0-1

1248/54/60

8

S155

100+75

0-1

1254/1260

15

S156

75+175

1-2

1248/54/60

25

S157

100+50

0-1

1248/54/60

(5-10)

S158

100+25

1-2

ND

ND

S159

108+175

0-1

1248/54/60

24

S160

100+75

1-2

ND

ND

S161

75+125

0-1

1254/1260

7

S162

-25+175

0-.5

0

ND

S163

113.4+300

1-2

0

ND

S164

75+150

1-2

1254/1260

4

S165

-25+150

0-.5

LOW
CHLOROANE

ND

S166

114.8+325

0-1

ND

ND

S167

115.5+250

1-2

ND

ND

S168

75+100

1-2

ND

ND

5169

114.8+325

1-2

ND

ND

ND = Non Detect

Trace <

CONCENTRATION
(IN PPM)

LAB
SAMPLE
NUMBER

SAMPLE
COORDINATES
(IN FT)

SAMPLE
DEPTH
(IN FT)

PCB

S198

50+175

0-1

1248/54/60

18

5/10/94

S199

50+200

0-1

1248

12

5/10/94

S200

50+25

1-2

ND

ND

5/10/94

S201

50+50

0-1

ND

ND

5/10/94

S202

50+25

0-1

ND

ND

5/10/94

S203

125+125

0-1

1248/54/60

(5-10)

5/11/94

S204

50+150

0-1

ND

ND

5/10/94

S205

125+275

0-1

ND

ND

5/11/94

S206

50+125

1-2

ND

ND

5/10/94

S207

125+375

1-2

ND

ND

5/11/94

S208

125+125

1-2

ND

ND

5/11/94

S209

125+175

1-2

1254/1260

23

5/11/94

S210

125+300

1-2

ND

ND

5/11/94

S211

125+250

0-1

ND

ND

5/11/94

S212

50+175

1-2

ND

ND

5/10/94

S213

125-250

1-2

ND

ND

5/11/94

S214

50+75

1-2

ND

ND

5/10/94

S215

50+100

0-1

ND

ND

5/10/94

125+300
S216
Non Detect
ND

0-1

ND

ND

5/11/94

CONCENTRATION

DATE

(IN PPM)

Trace < 5 PPM

APPENDIX E
RCMS 4,0 COST ESTIMATE

24

Summery Report
Initial Co»t Projection Scenario: KIHOSHA IRON t METAL
Projection ID Number: W10423SA
Cleanup Contractor: RES5 - Riedel Envirormntal

Page: 1

Date: 06/03/94
TAT Contractor: EOXOGYIENVIRON

Cost Projection Sunmery

Contractor Personnel
Contractor Equipment
Unit Rat* Materials
At Cost Materials
Subcontractors
Waste Transportation
Wast* Disposal

211,447.20
35,717.66
73,517.26
0.00
27,629.75
33,215.33
257,759.70

Cleanup Contractor Subtotal

639,286.90

Federal and State Agencies

0.00

Extramural Subtotal
20 X Extramural Contingency

639,286.90
127.857.38

Extramural Subtotal

767,144.28

TAT Personnel
TAT Special Projects
TAT Analytical Services

74,037.60
0.00
0.00

Total TAT Costs

74,037.60

Other Cost Items

0.00

Extramural Subtotal
IS X Project Contingency

841,181.88
126,177.28

Total Extramural Cost

967,359.16

EPA Regional Personnel

25,564.00

EPA Hon-imglonal Personnel
EPA Headquarters Direct
(10 X of Regional Hours)
EPA Indirect

0.00
2,160.00
38,160.00

EPA Total

65,880.00

Project Total

1,033,239.16

Page: 2

SuMary Report (com.)
Initial Cost Projection Scenario: KINOSHA IRON t METAL

Projection ID Huaber: W10423SA
Cleanup Contrector: RESS - Riedel EnvironMntel

Date: 06/03/94
TAT Contractor: ECOLOCYtEMVIROM

Project Scope

000

Step/Milestone

EstiMted
Duration

GENERAL SITE COSTS

90 Days

Co*t
1,033,239.16
1,033,239.16

DETAILED REPORT BY CATEGORY
REDACTED
4 PAGES
NOT RELEVANT TO THE SELECTION OF THE
REMOVAL ACTION